CN102499463A - Plant essential oil, preparation method of plant essential oil, and application of plant essential oil to cigarettes - Google Patents
Plant essential oil, preparation method of plant essential oil, and application of plant essential oil to cigarettes Download PDFInfo
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- CN102499463A CN102499463A CN2011103334072A CN201110333407A CN102499463A CN 102499463 A CN102499463 A CN 102499463A CN 2011103334072 A CN2011103334072 A CN 2011103334072A CN 201110333407 A CN201110333407 A CN 201110333407A CN 102499463 A CN102499463 A CN 102499463A
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Abstract
The invention discloses plant essential oil, a preparation method of the plant essential oil, and application of the plant essential oil to cigarettes. The preparation method includes: cleaning plants prior to drying, and crushing to obtain plant powder; and distilling the plant powder in sodium chloride solution at 80 DEGC to 100 DEG C for 8 hours to 12 hours, collecting volatiles to obtain light yellow essential oil, and processing the light yellow essential oil to obtain the plant essential oil, wherein a mass ratio of the plant powder to the sodium chloride is 1:10-20, and the plants belong to oriental blueberry, herba lycopi, anaphalis sinica hance or rosa laevigata michx. The preparation method is simple in operation, easy in control, low in cost, low in environment pollution and applicable to industrial production, while existing cigarette processing technics need no change. The plant essential oil is applicable to cigarettes, and the cigarettes with the plant essential oil are more fragrant in smoking, have smell of herbs, are unique and rich in fragrance, and are more flowing, harmonious, penetrating and comfortable.
Description
Technical field
The present invention relates to the preparation and the application of essential oil, be specifically related to a kind of plants essential oil and preparation method thereof and the application in cigarette.
Background technology
Developing the rich-fragrance reduced-harmfulness cigarette, can satisfy numerous smokers' demand, can ensure their healthy again, is a difficult task of tobacco business.Commonly used at present falls burnt technology when reducing tarry matters in smoke content; Some fragrance components in the flue gas have also been reduced; Cause people to feel " cigarette is not fragrant ", the physiology satisfaction is not enough, therefore presses for to add certain essence and flavoring agent and keep and compensate the fragrant jealous of tobacco.
China such as Zhejiang Province's characteristic plant resources are abundant; Contain abundant aroma component in some natural plants; These compositions can well compensate the fragrance of low-coke tar cigarette, can reduce that tar also can strengthen the physiology satisfaction when burning and sucking to the harm of human body when burning and sucking; Like application number disclosed grape biology extract for tobacco in 200710053675.2 the one Chinese patent application, disclosed gadol extract etc. among the Chinese patent ZL200610063556.0.Because plant resources is abundant; China particularly has advantageous advantage aspect the utilization of Chinese herbal medicine at natural plants; Can utilize this advantage; In conjunction with modern biochemical isolation technics, the extracts of some plants is carried out deep developmental research, performance and improve the effect of characteristic plant in actual production.
Blueberry Vaccinium bracteatum Thunb is an Ericaceae genus vaccinium plant.Its root, leaf, fruit all can be used as medicine, and have supplementing the kidney to control the nocturnal, strong muscle makes eye bright, removes the effect of sleeping, control chronic diarrhea and dysentery.Blueberry distributes very wide in China, reserves are very big, often is distributed in the hillside woods of hilly country or height above sea level 400m～1400m or in the bushes.Main chemical compositions is Quercetin, leukotrienes, freidelin, hydroxycinnamic acid etc. in its branches and leaves.Exploitation to blueberry at present mainly concentrates on its melanic research, as: the extraction of flavonoids monomer, separation, purifying and evaluation in the disclosed oriental blueberry melanin among the Chinese patent ZL200610040413.8; Also have some to the blueberry STUDY ON POLYSACHAROSE, like the disclosed method of from blueberry leaf, extracting soluble polysaccharide among the Chinese patent ZL200710067653.1; But separation and purification and development and use to the blueberry aroma component also do not appear in the newspapers.
Herba Lycopi Eupatorium japonicum Thunb. is the herb of Labiatae herbaceos perennial ground bamboo shoot (lycopus lucidus) Lycopus lu-cidus Turcz. or bristle ground bamboo shoot (hair leaf lycopus lucidus) L.lucidus Turcz.var.hirtus Regel..Tapped when summer, autumn, cauline leaf was luxuriant, dry.Contain volatile oil, glycoside, tannin and resin; Also contain flavonoids, phenols. amino acid, organic acid, saponin, various saccharides.Has promoting blood circulation, the effect of diuresis detumescence.Can be used for amenorrhea due to stagnation of blood, disease purplish or white patches on the skin, postpartum stasis of blood pain, oedema, traumatic injury.
Fragrant blue or green Anaphalis sinica Hance, another name: reed, an ancient musical pipe vertical bamboo flute or Japanese Raspberry Root are composite family anaphalis plant.Perennial herb.Root-like stock is thin or sturdy, and is wooden, and stolon is very thin.Stem is upright, and is sturdy, and high 20-50 centimetre, by white or canescence wool.The leaf stockless, little armful of stem is all tightr in the upper and lower arrangement of complete stool; The blade Long Circle, drape over one's shoulders the needle-like Long Circle to linear, the bottom leaf is withered at the florescence, and long 2-9 centimetre, wide 0.5-1.3 centimetre; The short gradually point or blunt of tip, the anxious tip of tool, base portion is gradually narrow; Decurrence is narrow wing on stem, full edge, and the surface is by thinner spider's thread shape wool; The back side is close by pale asphyxia or yellowish green thick wool, and assorted glandular hairs is arranged, usually in veinclearing show or the base portion leaf sometimes for going out arteries and veins from base three.Purposes: kobadrin, relieving asthma.
Fruit of Cherokee rose Rosa laevigata Michx., another name: hemiplelea davidii, thorn pear, golden small-mouthed jar etc. are rosaceous plant.Evergreen climing property shrub does not have hair; Sprig except that hook-shaped prickle is arranged, close living spinelet.Leaflet 3, minority 5, ellipticity is avette or to drape over one's shoulders needle-like avette, long 2-7 centimetre, wide 1.5-4.5 centimetre, there is serration at the edge, the two sides does not have hair, the back side along in arteries and veins spinelet is arranged; Petiole, rachis have little prickle or spinelet; Stipule is linear, separates with petiole, and is caducous.Hua Dan gives birth to side shoot top, white, diameter 5-9 centimetre; The close living spinelet of anthocaulus and calyx tube outside.Subsphaeroidal or the obovate of cynarrhodion, long 2-4 centimetre, spinelet is arranged, the top has long and outer anti-persistent calyx sheet.May at florescence, the fruit phase 9-10 month.The root skin is obtained through refining tannin extract; Fruit medicine has diuresis, kidney tonifying effect; Leaf has the removing toxicity for detumescence effect; Root is medicinal, can promoting blood circulation to remove blood stasis, the convergence of drawing out pus by applying a plaster to the affected part, dispel the wind that it is wet to drive.Fruit contains vitamin C, malic acid, citric acid, tannin, saponin etc.
At present, blueberry essential oil, Herba Lycopi's essential oil, fragrant blue or green essential oil or the application of fruit of Cherokee rose essential oil in cigarette also do not appear in the newspapers.
Summary of the invention
The invention provides a kind of plants essential oil that can be applicable in the cigarette.
The present invention also provides a kind of preparation method of plants essential oil, and this method is simple to operate, be easy to control.
The present invention also provides the application of a kind of plants essential oil in cigarette, and plants essential oil is applied in the cigarette, can significantly improve the perfume quantity of cigarette and the comfort level when sucking.
A kind of preparation method of plants essential oil may further comprise the steps:
A. it is dry plant to be cleaned the back, obtains the plant powder through pulverizing;
B. the plant powder was distilled 8 hours-12 hours down in 80 ℃-100 ℃ in sodium chloride (NaCl) aqueous solution, collect volatile matter and obtain faint yellow essential oil, obtain plants essential oil through post processing;
Wherein, the mass ratio of plant powder and sodium-chloride water solution is 1: 10-20;
Described plant is blueberry, Herba Lycopi, fragrant green grass or young crops or the fruit of Cherokee rose.
The branches and leaves of described blueberry, Herba Lycopi complete stool, fragrant blue or green complete stool or fruit of Cherokee rose complete stool all are applicable to the present invention and pluck conveniently that therefore described blueberry is the branches and leaves of blueberry; Perhaps, described Herba Lycopi is the Herba Lycopi complete stool; Perhaps, described fragrant green grass or young crops is fragrant blue or green complete stool; Perhaps, the described fruit of Cherokee rose is a fruit of Cherokee rose complete stool.
Among the step a, dry mode is varied, can dry naturally, dry in the shade, and also can pass through oven for drying, and from saving time and avoiding destroying active component two aspects and take all factors into consideration, the condition of described drying is preferably: 20 ℃ of-40 ℃ of air dried.
Be the effect that further guarantees to extract, preferred:
The order number of described plant powder is 20 orders-100 orders.
Among the step b, the mass fraction of described sodium-chloride water solution is 2%-5%.
Described post processing comprises: use anhydrous sodium sulfate dehydration.
Described plants essential oil can be applicable in the cigarette, need not change the original processing technology of cigarette during application, but can increase the perfume quantity of cigarette and the comfort level when sucking.
The consumption of described plants essential oil is preferably 0.005 ‰-0.05 ‰ of cigarette shreds quality.
The application process of described plants essential oil in cigarette; Comprise: plants essential oil is used the ethanol water dissolving of volume fraction as 60%-80%; Be mixed with the solution that plants essential oil concentration is 0.02mg/ml-0.2mg/ml, be sprayed onto on the cigarette shreds, obtain containing the pipe tobacco of plants essential oil.Adopt existing cigarette preparation method as after mixing operations such as silk, balance, cigarette, the pipe tobacco that will contain plants essential oil is processed cigarette.
The present invention also provides a kind of steam distillation system, can improve the productive rate of plants essential oil when being used to prepare plants essential oil.
A kind of steam distillation system comprises the container that is used to hold raw material of being with opening, is used for heater that container is heated and the condensing unit that is communicated with vessel port, is communicated with through the determination of volatile matter device between described condensing unit and the vessel port;
Described condensing unit comprises spherical condensation tube and the serpentine condenser that is communicated with successively;
Described determination of volatile matter device comprises that the intersection of three passages that are interconnected and every two passes is provided with outlet, and wherein two outlets are communicated with vessel port, spherical condensation tube respectively, and the residue outlet is provided with switch.
Compared with prior art, the present invention has following advantage:
The preparation method of plants essential oil of the present invention; Adopt dry, the faint yellow essential oil of pulverizings → distillation → collection after post processing, to make plants essential oil, simple to operate, be easy to control and raw material sources enrich, cost is low; Energy consumption is low; Environmentally safe need not to change the processing technology that has cigarette now, is suitable for suitability for industrialized production.
Plants essential oil of the present invention may be used in the cigarette, adds the cigarette of plants essential oil of the present invention, and perfume quantity increases when sucking, and the herbal medicine note is arranged, and fragrance has uniqueness, and rich and elegant sense increases, and hamony is better, and it is good to send out property thoroughly, and comfort level strengthens.Quality defect such as improved China's cigarette product insufficient fragrance to a certain extent, comfort level is not high, excitement is strong has good actual production meaning and value.
Steam distillation of the present invention system can improve the productive rate of target product.
Description of drawings
Fig. 1 is the structural representation of steam distillation of the present invention system;
Among the figure: 1 is serpentine condenser; 2 is spherical condensation tube; 3 is the determination of volatile matter device; 4 is container; 5 is heater.
The specific embodiment
The present invention does below in conjunction with embodiment and further describes.
Embodiment 1
As shown in Figure 1; Steam distillation of the present invention system; The heater 5 that comprise the container 4 that is used to hold raw material of being with opening, is used for container 4 is heated and with the condensing unit of container 4 open communication, be communicated with through determination of volatile matter device 3 between condensing unit and container 4 openings; Condensing unit comprises the spherical condensation tube 2 and serpentine condenser 1 that is communicated with successively; Determination of volatile matter device 3 comprises that the intersection of three passages that are interconnected and every two passes is provided with outlet, and wherein two outlets are communicated with container 4 openings, spherical condensation tube 2 respectively, and the residue outlet is provided with switch.
During small-scale test, container 4 can be selected flask for use, heater 5 optional electricity consumption heating jackets.
Embodiment 2
Adopt the steam distillation system of embodiment 1.
A, fresh blueberry branches and leaves are cleaned back 40 ℃ of air dried 48h, be crushed to 60 orders again, obtain the blueberry powder;
B, the blueberry powder of getting step a gained are put into the 5L flask; In the mass ratio of the blueberry powder and the NaCl aqueous solution is that to add mass fraction be 2.5% the NaCl aqueous solution for 1: 10 ratio; Keep 100 ℃ of distillation 8h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes the blueberry essential oil.The amount of gained blueberry essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the blueberry essential oil of equal conditions gained: with 10g blueberry powder is example; Adopt the steam distillation system of embodiment 1 to obtain 0.1g blueberry essential oil, adopt conventional Distallation systm to obtain 0.35g blueberry essential oil.
0.01 ‰ usefulness microsyringe according to tobacco quality is drawn the blueberry essential oil; Using volume fraction is that 70% ethanol water is made into blueberry essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 2 as cigarette) as the spray solution of 0.04mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, and sensory evaluating smoking result is: (note is propped up A as cigarette with the Cigarette that does not add the blueberry essential oil; It is 2 identical that pipe tobacco and cigarette prop up) relatively; Perfume quantity strengthens, rich slightly increase, and elegant sense strengthens; Hamony and high conformity, fragrance has uniqueness.
Embodiment 3
Adopt the steam distillation system of embodiment 1.
A, fresh blueberry branches and leaves are cleaned back 30 ℃ of air dried 60h, be crushed to 20 orders again, obtain the blueberry powder;
B, the blueberry powder of getting step a gained are put into the 5L flask; In the mass ratio of the blueberry powder and the NaCl aqueous solution is that to add mass fraction be 3% the NaCl aqueous solution for 1: 20 ratio; Keep 90 ℃ of distillation 10h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes the blueberry essential oil.The amount of gained blueberry essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the blueberry essential oil of equal conditions gained.
0.05 ‰ usefulness microsyringe according to tobacco quality is drawn the blueberry essential oil; Using volume fraction is that 70% ethanol water is made into blueberry essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 3 as cigarette) as the spray solution of 0.2mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, sensory evaluating smoking result is: compare with the Cigarette that does not add the blueberry essential oil (note is propped up A as cigarette), perfume quantity strengthens; Rich slightly increase; Elegant sense strengthens, hamony and high conformity, and fragrance has uniqueness.
Embodiment 4
Adopt the steam distillation system of embodiment 1.
A, be placed on 40 ℃ of dry 48h down after fresh blueberry branches and leaves are cleaned, be crushed to 80 orders again, obtain the blueberry powder;
B, the blueberry powder of getting step a gained are put into the 5L flask; In the mass ratio of the blueberry powder and the NaCl aqueous solution is that to add mass fraction be 2.5% the NaCl aqueous solution for 1: 10 ratio; Keep 80 ℃ of distillation 12h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes the blueberry essential oil.The amount of gained blueberry essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the blueberry essential oil of equal conditions gained.
0.005 ‰ usefulness microsyringe according to tobacco quality is drawn the blueberry essential oil; Using volume fraction is that 70% ethanol water is made into blueberry essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 4 as cigarette) as the spray solution of 0.12mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, sensory evaluating smoking result is: compare with the Cigarette that does not add the blueberry essential oil (note is propped up A as cigarette), perfume quantity strengthens; Rich slightly increase; Elegant sense strengthens, hamony and high conformity, and fragrance has uniqueness.
Embodiment 5
Adopt the steam distillation system of embodiment 1.
A, fresh blueberry branches and leaves are cleaned back 20 ℃ of air-dry 70h, be crushed to 100 orders again, obtain the blueberry powder;
B, the blueberry powder of getting step a gained are put into the 5L flask; In the mass ratio of the blueberry powder and the NaCl aqueous solution is that to add mass fraction be 5% the NaCl aqueous solution for 1: 18 ratio; 86 ℃ are distilled 11h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes the blueberry essential oil.The amount of gained blueberry essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the blueberry essential oil of equal conditions gained.
0.03 ‰ usefulness microsyringe according to tobacco quality is drawn the blueberry essential oil; Using volume fraction is that 60% ethanol water is made into blueberry essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 5 as cigarette) as the spray solution of 0.02mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add the blueberry essential oil (note is propped up A as cigarette), perfume quantity strengthens, rich slightly increase, and elegant sense strengthens, hamony and high conformity, fragrance has uniqueness.
Embodiment 6
Adopt the steam distillation system of embodiment 1.
A, fresh blueberry branches and leaves are cleaned back 35 ℃ of air-dry 30h, be crushed to 40 orders again, obtain the blueberry powder;
B, the blueberry powder of getting step a gained are put into the 5L flask; In the mass ratio of the blueberry powder and the NaCl aqueous solution is that to add mass fraction be 2% the NaCl aqueous solution for 1: 12 ratio; 95 ℃ are distilled 9h down, and essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes the blueberry essential oil.The amount of gained blueberry essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the blueberry essential oil of equal conditions gained.
0.02 ‰ usefulness microsyringe according to tobacco quality is drawn the blueberry essential oil; Using volume fraction is that 80% ethanol water is made into blueberry essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 6 as cigarette) as the spray solution of 0.08mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add the blueberry essential oil (note is propped up A as cigarette), perfume quantity strengthens, rich slightly increase, and elegant sense strengthens, hamony and high conformity, fragrance has uniqueness.
Embodiment 7
Adopt the steam distillation system of embodiment 1.
A, fresh Herba Lycopi complete stool is cleaned back 40 ℃ of air dried 48h, be crushed to 60 orders again, obtain Herba Lycopi's powder;
B, Herba Lycopi's powder of getting step a gained are put into the 5L flask; In the mass ratio of the Herba Lycopi's powder and the NaCl aqueous solution is that to add mass fraction be 2.5% the NaCl aqueous solution for 1: 15 ratio; Keep 100 ℃ of distillation 8h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes Herba Lycopi's essential oil.The amount of gained Herba Lycopi essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at Herba Lycopi's essential oil of equal conditions gained: with 10g Herba Lycopi's powder is example; Adopt the steam distillation system of embodiment 1 to obtain 1.35g Herba Lycopi's essential oil, adopt conventional Distallation systm to obtain 0.48g Herba Lycopi's essential oil.
0.05 ‰ usefulness microsyringe according to tobacco quality is drawn Herba Lycopi's essential oil; Using volume fraction is that 70% ethanol water is made into Herba Lycopi's essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 7 as cigarette) as the spray solution of 0.2mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, sensory evaluating smoking result is: compare with the Cigarette that does not add Herba Lycopi's essential oil (note is propped up A as cigarette), perfume quantity strengthens; Rich slightly increase; Elegant sense strengthens, hamony and high conformity, and fragrance has uniqueness.
Embodiment 8
Adopt the steam distillation system of embodiment 1.
A, fresh Herba Lycopi complete stool is cleaned back 30 ℃ of air dried 60h, be crushed to 20 orders again, obtain Herba Lycopi's powder;
B, Herba Lycopi's powder of getting step a gained are put into the 5L flask; In the mass ratio of the Herba Lycopi's powder and the NaCl aqueous solution is that to add mass fraction be 3.5% the NaCl aqueous solution for 1: 20 ratio; Keep 90 ℃ of distillation 12h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes Herba Lycopi's essential oil.The amount of gained Herba Lycopi essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at Herba Lycopi's essential oil of equal conditions gained.
0.01 ‰ usefulness microsyringe according to tobacco quality is drawn Herba Lycopi's essential oil; Using volume fraction is that 70% ethanol water is made into Herba Lycopi's essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 8 as cigarette) as the spray solution of 0.04mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, sensory evaluating smoking result is: compare with the Cigarette that does not add Herba Lycopi's essential oil (note is propped up A as cigarette), perfume quantity strengthens; Rich slightly increase; Elegant sense strengthens, hamony and high conformity, and fragrance has uniqueness.
Embodiment 9
Adopt the steam distillation system of embodiment 1.
A, be placed on 40 ℃ of air dried 48h after fresh Herba Lycopi complete stool cleaned, be crushed to 40 orders again, obtain Herba Lycopi's powder;
B, Herba Lycopi's powder of getting step a gained are put into the 5L flask; In the mass ratio of the Herba Lycopi's powder and the NaCl aqueous solution is that to add mass fraction be 5% the NaCl aqueous solution for 1: 20 ratio; Keep 100 ℃ of distillation 10h down, essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes Herba Lycopi's essential oil.The amount of gained Herba Lycopi essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at Herba Lycopi's essential oil of equal conditions gained.
0.005 ‰ usefulness microsyringe according to tobacco quality is drawn Herba Lycopi's essential oil; Using volume fraction is that 70% ethanol water is made into Herba Lycopi's essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 9 as cigarette) as the spray solution of 0.02mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h, sensory evaluating smoking result is: compare with the Cigarette that does not add Herba Lycopi's essential oil (note is propped up A as cigarette), perfume quantity strengthens; Rich slightly increase; Elegant sense strengthens, hamony and high conformity, and fragrance has uniqueness.
Embodiment 10
Adopt the steam distillation system of embodiment 1.
A, fresh Herba Lycopi complete stool is cleaned back 20 ℃ of air-dry 70h, be crushed to 100 orders again, obtain Herba Lycopi's powder;
B, Herba Lycopi's powder of getting step a gained are put into the 5L flask; In the mass ratio of the Herba Lycopi's powder and the NaCl aqueous solution is that to add mass fraction be 2% the NaCl aqueous solution for 1: 10 ratio; 80 ℃ are distilled 10h down, and essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes Herba Lycopi's essential oil.The amount of gained Herba Lycopi essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at Herba Lycopi's essential oil of equal conditions gained.
0.03 ‰ usefulness microsyringe according to tobacco quality is drawn Herba Lycopi's essential oil; Using volume fraction is that 60% ethanol water is made into Herba Lycopi's essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 10 as cigarette) as the spray solution of 0.1mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add Herba Lycopi's essential oil (note is propped up A as cigarette), perfume quantity strengthens, rich slightly increase, and elegant sense strengthens, hamony and high conformity, fragrance has uniqueness.
Embodiment 11
Adopt the steam distillation system of embodiment 1.
A, fresh Herba Lycopi complete stool is cleaned back 35 ℃ of air-dry 30h, be crushed to 80 orders again, obtain Herba Lycopi's powder;
B, Herba Lycopi's powder of getting step a gained are put into the 5L flask; In the mass ratio of the Herba Lycopi's powder and the NaCl aqueous solution is that to add mass fraction be 4% the NaCl aqueous solution for 1: 12 ratio; 95 ℃ are distilled 9h down, and essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes Herba Lycopi's essential oil.The amount of gained Herba Lycopi essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at Herba Lycopi's essential oil of equal conditions gained.
0.02 ‰ usefulness microsyringe according to tobacco quality is drawn Herba Lycopi's essential oil; Using volume fraction is that 80% ethanol water is made into Herba Lycopi's essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 11 as cigarette) as the spray solution of 0.08mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add Herba Lycopi's essential oil (note is propped up A as cigarette), perfume quantity strengthens, rich slightly increase, and elegant sense strengthens, hamony and high conformity, fragrance has uniqueness.
Embodiment 12
Adopt the steam distillation system of embodiment 1.
A, fresh fragrant blue or green complete stool is cleaned back 40 ℃ of air dried 48h, be crushed to 60 orders again, obtain fragrant blue or green powder;
B, the fragrant blue or green powder of getting step a gained are put into the 5L flask; In the mass ratio of the blue or green powder of perfume (or spice) and the NaCl aqueous solution is that to add mass fraction be 2.5% the NaCl aqueous solution for 1: 15 ratio; Keep 100 ℃ of distillation 8h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fragrant blue or green essential oil.The amount of the fragrant blue or green essential oil of gained is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fragrant blue or green essential oil of equal conditions gained: with the fragrant blue or green powder of 10g is example; Adopt the steam distillation system of embodiment 1 to obtain the fragrant blue or green essential oil of 1.28g, adopt conventional Distallation systm to obtain the fragrant blue or green essential oil of 0.35g.
0.05 ‰ usefulness microsyringe according to tobacco quality is drawn fragrant blue or green essential oil; Using volume fraction is that 70% ethanol water is made into fragrant blue or green essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 12 as cigarette) as the spray solution of 0.2mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add fragrant blue or green essential oil (note is propped up A as cigarette), perfume quantity increases, elegant sense and rich enhancing; Hamony and high conformity, fragrance has uniqueness.
Embodiment 13
Adopt the steam distillation system of embodiment 1.
A, fresh fragrant blue or green complete stool is cleaned back 35 ℃ of air dried 60h, be crushed to 20 orders again, obtain fragrant blue or green powder;
B, the fragrant blue or green powder of getting step a gained are put into the 5L flask; In the mass ratio of the blue or green powder of perfume (or spice) and the NaCl aqueous solution is that to add mass fraction be 3.5% the NaCl aqueous solution for 1: 20 ratio; Keep 90 ℃ of distillation 12h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fragrant blue or green essential oil.The amount of the fragrant blue or green essential oil of gained is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fragrant blue or green essential oil of equal conditions gained.
0.01 ‰ usefulness microsyringe according to tobacco quality is drawn fragrant blue or green essential oil; Using volume fraction is that 70% ethanol water is made into fragrant blue or green essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 13 as cigarette) as the spray solution of 0.04mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add fragrant blue or green essential oil (note is propped up A as cigarette), perfume quantity increases, elegant sense and rich enhancing; Hamony and high conformity, fragrance has uniqueness.
Embodiment 14
Adopt the steam distillation system of embodiment 1.
A, be placed on 30 ℃ of air dried 65h after fresh fragrant blue or green complete stool cleaned, be crushed to 40 orders again, obtain fragrant blue or green powder;
B, the fragrant blue or green powder of getting step a gained are put into the 5L flask; In the mass ratio of the blue or green powder of perfume (or spice) and the NaCl aqueous solution is that to add mass fraction be 4.5% the NaCl aqueous solution for 1: 20 ratio; Keep 100 ℃ of distillation 10h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fragrant blue or green essential oil.The amount of the fragrant blue or green essential oil of gained is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fragrant blue or green essential oil of equal conditions gained.
0.005 ‰ usefulness microsyringe according to tobacco quality is drawn fragrant blue or green essential oil; Using volume fraction is that 70% ethanol water is made into fragrant blue or green essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 14 as cigarette) as the spray solution of 0.02mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add fragrant blue or green essential oil (note is propped up A as cigarette), perfume quantity increases, elegant sense and rich enhancing; Hamony and high conformity, fragrance has uniqueness.
Embodiment 15
Adopt the steam distillation system of embodiment 1.
A, fresh fragrant blue or green complete stool is cleaned back 20 ℃ of air-dry 70h, be crushed to 100 orders again, obtain fragrant blue or green powder;
B, the fragrant blue or green powder of getting step a gained are put into the 5L flask; In the mass ratio of the blue or green powder of perfume (or spice) and the NaCl aqueous solution is that to add mass fraction be 2% the NaCl aqueous solution for 1: 10 ratio; 80 ℃ are distilled 10h down, and essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fragrant blue or green essential oil.The amount of the fragrant blue or green essential oil of gained is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fragrant blue or green essential oil of equal conditions gained.
0.03 ‰ usefulness microsyringe according to tobacco quality is drawn fragrant blue or green essential oil; Using volume fraction is that 60% ethanol water is made into fragrant blue or green essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 15 as cigarette) as the spray solution of 0.1mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add fragrant blue or green essential oil (note is propped up A as cigarette), perfume quantity increases, elegant sense and rich enhancing, and hamony and high conformity, fragrance has uniqueness.
Embodiment 16
Adopt the steam distillation system of embodiment 1.
A, fresh fragrant blue or green complete stool is cleaned back 25 ℃ of air-dry 68h, be crushed to 80 orders again, obtain fragrant blue or green powder;
B, the fragrant blue or green powder of getting step a gained are put into the 5L flask; In the mass ratio of the blue or green powder of perfume (or spice) and the NaCl aqueous solution is that to add mass fraction be 5% the NaCl aqueous solution for 1: 12 ratio; 95 ℃ are distilled 9h down, and essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fragrant blue or green essential oil.The amount of the fragrant blue or green essential oil of gained is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fragrant blue or green essential oil of equal conditions gained.
0.02 ‰ usefulness microsyringe according to tobacco quality is drawn fragrant blue or green essential oil; Using volume fraction is that 80% ethanol water is made into fragrant blue or green essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 16 as cigarette) as the spray solution of 0.08mg/ml, carries out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: compare with the Cigarette that does not add fragrant blue or green essential oil (note is propped up A as cigarette), perfume quantity increases, elegant sense and rich enhancing, and hamony and high conformity, fragrance has uniqueness.
Embodiment 17
Adopt the steam distillation system of embodiment 1.
A, fresh fruit of Cherokee rose complete stool is cleaned back 40 ℃ of air dried 48h, be crushed to 60 orders again, obtain fruit of Cherokee rose powder;
B, the fruit of Cherokee rose powder of getting step a gained are put into the 5L flask; In the mass ratio of the fruit of Cherokee rose powder and the NaCl aqueous solution is that to add mass fraction be 2.5% the NaCl aqueous solution for 1: 15 ratio; Keep 100 ℃ of distillation 8h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fruit of Cherokee rose essential oil.The amount of gained fruit of Cherokee rose essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fruit of Cherokee rose essential oil of equal conditions gained: with 10g fruit of Cherokee rose powder is example; Adopt the steam distillation system of embodiment 1 to obtain 1.5g fruit of Cherokee rose essential oil, adopt conventional Distallation systm to obtain 0.40g fruit of Cherokee rose essential oil.
0.05 ‰ usefulness microsyringe according to tobacco quality is drawn fruit of Cherokee rose essential oil; Using volume fraction is that 70% ethanol water is made into fruit of Cherokee rose essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 17 as cigarette) as the spray solution of 0.2mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: with the Cigarette that does not add fruit of Cherokee rose essential oil (note is propped up A as cigarette) relatively, perfume quantity increases, rich, sophistication, elegant degree and elegant sense strengthen; Hamony and high conformity, fragrance has uniqueness.
Embodiment 18
Adopt the steam distillation system of embodiment 1.
A, be placed on 20 ℃ of air dried 70h after fresh fruit of Cherokee rose complete stool cleaned, be crushed to 20 orders again, obtain fruit of Cherokee rose powder;
B, the fruit of Cherokee rose powder of getting step a gained are put into the 5L flask; In the mass ratio of the fruit of Cherokee rose powder and the NaCl aqueous solution is that to add mass fraction be 5% the NaCl aqueous solution for 1: 20 ratio; Keep 80 ℃ of distillation 10h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fruit of Cherokee rose essential oil.The amount of gained fruit of Cherokee rose essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fruit of Cherokee rose essential oil of equal conditions gained.
0.005 ‰ usefulness microsyringe according to tobacco quality is drawn fruit of Cherokee rose essential oil; Using volume fraction is that 60% ethanol water is made into fruit of Cherokee rose essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 18 as cigarette) as the spray solution of 0.02mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: with the Cigarette that does not add fruit of Cherokee rose essential oil (note is propped up A as cigarette) relatively, perfume quantity increases, rich, sophistication, elegant degree and elegant sense strengthen; Hamony and high conformity, fragrance has uniqueness.
Embodiment 19
Adopt the steam distillation system of embodiment 1.
A, be placed on 30 ℃ of air dried 60h after fresh fruit of Cherokee rose complete stool cleaned, be crushed to 100 orders again, obtain fruit of Cherokee rose powder;
B, the fruit of Cherokee rose powder of getting step a gained are put into the 5L flask; In the mass ratio of the fruit of Cherokee rose powder and the NaCl aqueous solution is that to add mass fraction be 2% the NaCl aqueous solution for 1: 10 ratio; Keep 90 ℃ of distillation 9h down; Essential oil is used anhydrous sodium sulfate dehydration in the collection determination of volatile matter device 3, makes fruit of Cherokee rose essential oil.The amount of gained fruit of Cherokee rose essential oil is than adopting conventional on the flask opening, to be communicated with a spherical condensation tube 2 or to be communicated with the amount showed increased of the Distallation systm of a serpentine condenser 1 at the fruit of Cherokee rose essential oil of equal conditions gained.
0.01 ‰ usefulness microsyringe according to tobacco quality is drawn fruit of Cherokee rose essential oil; Using volume fraction is that 80% ethanol water is made into fruit of Cherokee rose essential oil concentration and to pipe tobacco, rolls into Cigarette (note props up 19 as cigarette) as the spray solution of 0.1mg/ml; Carry out the sensory evaluating smoking behind constant temperature (22 ± 1 ℃) constant humidity (relative humidity 60 ± 2%) the balance 48h; Sensory evaluating smoking result is: with the Cigarette that does not add fruit of Cherokee rose essential oil (note is propped up A as cigarette) relatively, perfume quantity increases, rich, sophistication, elegant degree and elegant sense strengthen; Hamony and high conformity, fragrance has uniqueness.
The requirement of smokeing panel test: the smokeing panel test of each sample needs seven and the above persons to participate in, two judging panels of cigarette country, five and more than provincial judging panel; These qualifications all need pass qualification examinations.
Smoke panel test with reference to State Standard of the People's Republic of China (GB 5606.4-2005) " cigarette the 4th part: sense organ specification requirement " (Cigarettes-Part 4:Technical requirements for sense-evaluation); 2005-6-17 issue, 2006-1-1 implement, by General Administration of Quality Supervision, Inspection and Quarantine o of the People's Republic of China and Standardization Administration of China's issue.
The contrast cigarette props up sensory evaluating smoking result's (each item value is the mean value with 10 personnel's smoking results of smokeing panel test of qualification) that cigarette that (cigarette props up A) and embodiment of the invention 2-19 add plants essential oil props up 2-19 and sees the following form 1:
Table 1
Claims (10)
1. the preparation method of a plants essential oil may further comprise the steps:
A. it is dry plant to be cleaned the back, obtains the plant powder through pulverizing;
B. the plant powder was distilled 8 hours-12 hours down in 80 ℃-100 ℃ in sodium-chloride water solution, collect volatile matter and obtain faint yellow essential oil, obtain plants essential oil through post processing;
Wherein, the mass ratio of plant powder and sodium-chloride water solution is 1: 10-20;
Described plant is blueberry, Herba Lycopi, fragrant green grass or young crops or the fruit of Cherokee rose.
2. the preparation method of plants essential oil according to claim 1 is characterized in that, described blueberry is the branches and leaves of blueberry; Perhaps, described Herba Lycopi is the Herba Lycopi complete stool; Perhaps, described fragrant green grass or young crops is fragrant blue or green complete stool; Perhaps, the described fruit of Cherokee rose is a fruit of Cherokee rose complete stool.
3. the preparation method of plants essential oil according to claim 1 is characterized in that, among the step a, the condition of described drying is: 20 ℃ of-40 ℃ of air dried;
Perhaps, the order number of described plant powder is 20 orders-100 orders.
4. the preparation method of plants essential oil according to claim 1 is characterized in that, among the step b, the mass fraction of described sodium-chloride water solution is 2%-5%.
5. the preparation method of plants essential oil according to claim 1 is characterized in that, among the step b, described post processing comprises: use anhydrous sodium sulfate dehydration.
6. according to the plants essential oil of the preparation method of each described plants essential oil of claim 1-5 preparation.
7. the application of plants essential oil according to claim 6 in cigarette.
8. the application of plants essential oil according to claim 7 in cigarette is characterized in that, the consumption of plants essential oil is 0.005 ‰-0.05 ‰ of a cigarette shreds quality.
9. according to claim 7 or 8 application of described plants essential oil in cigarette; It is characterized in that; Described application process comprises: described plants essential oil is used the ethanol water dissolving of volume fraction as 60%-80%; The solution spray that is mixed with plants essential oil concentration and is 0.02mg/ml-O.2mg/ml is added on the cigarette shreds, the preparation cigarette.
10. steam distillation system; Comprise the container that is used to hold raw material of being with opening, be used for heater that container is heated and the condensing unit that is communicated with vessel port; It is characterized in that, be communicated with through the determination of volatile matter device between described condensing unit and the vessel port;
Described condensing unit comprises spherical condensation tube and the serpentine condenser that is communicated with successively;
Described determination of volatile matter device comprises that the intersection of three passages that are interconnected and every two passes is provided with outlet, and wherein two outlets are communicated with vessel port, spherical condensation tube respectively, and the residue outlet is provided with switch.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104977381A (en) * | 2015-06-01 | 2015-10-14 | 浙江工业大学 | Cherokee rose fruit essential oil and component analysis and identification method thereof |
| CN106281701A (en) * | 2016-08-17 | 2017-01-04 | 上海清轩生物科技有限公司 | Essential oil extraction device and plants essential oil extracting method |
| CN111171962A (en) * | 2020-03-20 | 2020-05-19 | 鲁南制药集团股份有限公司 | Novel volatile oil extractor |
| CN112481036A (en) * | 2020-11-20 | 2021-03-12 | 河北中烟工业有限责任公司 | Enzymolysis preparation method of high-aroma tobacco essential oil |
| CN112826767A (en) * | 2021-04-01 | 2021-05-25 | 广西大学 | Natural plant mask and preparation method thereof |
| CN115748303A (en) * | 2022-11-07 | 2023-03-07 | 云南中烟工业有限责任公司 | Glutinous rice fragrance type cigarette paper and application thereof |
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| CN1143671A (en) * | 1996-05-03 | 1997-02-26 | 云南省烟草工业研究所 | Natural perfume with health care action for cigarette |
| RO121080B1 (en) * | 2004-01-30 | 2006-12-29 | Farmacia Naturii S.R.L. | Therapeutic pillow |
| CN1986760A (en) * | 2006-12-22 | 2007-06-27 | 中国烟草总公司郑州烟草研究院 | Water vapor extracted and refined sophora flower oil and its application in perfuming cigarette |
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| CN1143671A (en) * | 1996-05-03 | 1997-02-26 | 云南省烟草工业研究所 | Natural perfume with health care action for cigarette |
| RO121080B1 (en) * | 2004-01-30 | 2006-12-29 | Farmacia Naturii S.R.L. | Therapeutic pillow |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104977381A (en) * | 2015-06-01 | 2015-10-14 | 浙江工业大学 | Cherokee rose fruit essential oil and component analysis and identification method thereof |
| CN106281701A (en) * | 2016-08-17 | 2017-01-04 | 上海清轩生物科技有限公司 | Essential oil extraction device and plants essential oil extracting method |
| CN111171962A (en) * | 2020-03-20 | 2020-05-19 | 鲁南制药集团股份有限公司 | Novel volatile oil extractor |
| CN112481036A (en) * | 2020-11-20 | 2021-03-12 | 河北中烟工业有限责任公司 | Enzymolysis preparation method of high-aroma tobacco essential oil |
| CN112826767A (en) * | 2021-04-01 | 2021-05-25 | 广西大学 | Natural plant mask and preparation method thereof |
| CN115748303A (en) * | 2022-11-07 | 2023-03-07 | 云南中烟工业有限责任公司 | Glutinous rice fragrance type cigarette paper and application thereof |
| CN115748303B (en) * | 2022-11-07 | 2023-11-10 | 云南中烟工业有限责任公司 | Glutinous rice fragrant cigarette paper and application thereof |
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| CN102499463B (en) | 2013-06-26 |
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