CN102433777B - Preparation method of cold migration printing gum and color paste thereof - Google Patents
Preparation method of cold migration printing gum and color paste thereof Download PDFInfo
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- CN102433777B CN102433777B CN201110364462.8A CN201110364462A CN102433777B CN 102433777 B CN102433777 B CN 102433777B CN 201110364462 A CN201110364462 A CN 201110364462A CN 102433777 B CN102433777 B CN 102433777B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
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Abstract
The invention discloses a preparation method of cold migration printing gum and color paste thereof. The gum contains starch oxide, printing oil and etherified starch. The cold migration printing gum has high water dissolving speed, and can be used for rapidly carrying a dye and transferring onto the surface of a fabric by being contacted with the fabric treated with a pretreatment liquid in the cold migration printing process. A film formed by drying color paste prepared from the gum has high elasticity, printing patterns can be effectively prevented from cracking, and meshes and ink cells are prevented from being blocked.
Description
Technical field
The printing gum that the present invention relates to use in textile industry, specifically refers to the compound method of a kind of cold-transfer printing thickener and mill base thereof.This cold-transfer printing is the carrier as dyestuff with thickener, the print paste that is modulated into REACTIVE DYES or ACID DYES can be printed on cold-transfer printing medium, and in transfer printing process, decalcomania is transferred on the textile fabric such as cotton, nylon from medium.
Background technology
Printing gum refers to and is added in the macromolecular compound that can play thickening power in print paste.First cold-transfer printing technique be printed on the print paste being made up of thickener and dyestuff on paper substrate, formation has the transfer printing paper of required pattern or word, then will on this transfer printing paper, there is the one side of dyestuff with closely sealed by seal fabric, make dyestuff depart from or peel off from paper substrate by pressure-acting, and by the pattern on transfer printing paper or words transfer printing to fabric.Thickener is a kind of liquid phase dispersion medium, is the carrier of dyestuff and stuffing, must have certain viscosity.The printing effect of thickener stamp has close relationship with the print paste that is printed fabric, printing method and be made up of thickener and dyestuff etc.And the key properties such as the rheological characteristic of print paste, shearing force, viscosity, viscosity, rate of drying depend on that former paste is the performance of thickener, therefore thickener plays vital effect in stamp process.Thickener in transfer printing, as a kind of thickener of print paste, should be given certain viscosity and Printing Characteristics, and after stamp, transfer, fixation process complete, thickener can be removed from fabric relatively easily.In addition, thickener also plays the decentralized medium of each component and the effect of diluent such as dyestuff in print paste, and the each component of printing gum can be evenly dispersed in former paste.The thickener of tradition application mainly contains: seaweeds, comprise sodium alginate and alginic acid ester, and starch and cellulose modified class, modification guar gum class, comprises oxidation guar gum, etherificate guar gum, and acrylic compounds synthetic thickening agent.In view of the feature of cold-transfer printing technique, require thickener to have water-soluble fast, so that facilitate dyestuff to transfer to fabric from paper fast in the time of transfer printing; In addition because cold-transfer printing technique is that flower type is printed on paper, therefore also require to have good printing characteristic.In order further to improve cold-transfer printing technique, improve the dyestuff rate of transform and Printing quality, and the cold-transfer printing thickener using now and the mill base of preparation thereof, what have has obtained patent right, the instructions for use that not too meets my company having, therefore need to develop a kind of novel cold-transfer printing thickener, and there is better printing and transferring properties.
Summary of the invention
In order to overcome the mill base of existing cold-transfer printing thickener and preparation thereof, what cause had has obtained patent right, and some cold-transfer printings do not meet my company's instructions for use with thickener, so, the invention provides the compound method of a kind of cold-transfer printing thickener and mill base thereof, can realize the rapid water dissolubility of cold-transfer printing thickener, and be suitable for being deployed into mill base and can be printed on paper, can shift smoothly to print to and printed on fabric.
The invention provides the compound method of a kind of cold-transfer printing thickener and mill base.
First aspect, provides a kind of cold-transfer printing thickener, and its formula according to percentage by weight is:
Oxidized starch 5-8%;
Stamp oil 0.5-1.5%;
Etherification starch 20-45%;
Adjust to 100% with deionized water.
Wherein said oxidized starch is hypochlorite oxidation starch or hydrogen peroxide oxidation starch or potassium permanganate oxidation starch or periodate oxidation starch; In dried starch, carboxyl mass fraction >=0.40% of described oxidized starch.Described stamp oil is the nonionic stamp oil taking prosparol as main component, selects the nonionic stamp oil of Ke Kai company, or similar stamp oil.Described etherification starch is low viscosity etherification starch, selects low viscosity hydroxyalkyl etherificate starch or low-viscosity carboxymethyl etherification starch; Described low viscosity is the former paste of etherification starch (10% etherification starch and 90% system after dried up abundant dissolving of going is called former paste) by 10% weight, under 25 DEG C of conditions, use Brookfield viscometer 20 transfer to tests per minute, its viscosity is 20,000-50,000mPas.
The compound method of described cold-transfer printing thickener is:
The oxidized starch of 5-8% weight is put into container, add 0.5-1.5% weight stamp oil and the etherification starch of 20-45% weight, add again deionized water to fully stirring after 100% weight, treat to dissolve completely with system color all for the moment, become cold-transfer printing thickener.
Second aspect of the present invention, provides the method for applying above-mentioned cold-transfer printing paste formulation print paste.
Described cold-transfer printing paste formula according to percentage by weight is:
Cold-transfer printing thickener 30-55%;
Dyestuff 0.2-15%;
Reservehao S 0.5-1%;
Dispersant 0.1-8%;
Levelling agent 0.05-0.5%;
Water adjusts to 100%.
Wherein dyestuff can be selected REACTIVE DYES or ACID DYES; Dispersant is selected from methanonaphthalene sulfonic acid dispersant, or phenolic condensation compound sulfonate dispersant, or fatty alcohol-polyoxyethylene ether silane type dispersant; Levelling agent is selected from the non-ionic surface active agent of alkane ether type, or aryl polyethenoxy ether sodium sulfate anion surfactant, or the two mixture.
The compound method of described cold-transfer printing mill base is:
Add the dyestuff of a small amount of cold water and 0.2-15% weight in container, and furnishing pasty state; Then add the mixed liquor of the levelling agent of dispersant, the 0.05-0.5% weight of reservehao S, the 0.1-8% weight of the 0.5-1% weight of having dissolved, add again 85 DEG C of left and right warm water that dyestuff is fully dissolved, join after filtering in the cold-transfer printing thickener of 30-55% weight, and water stirs after adjusting to 100% weight, make cold-transfer printing mill base.
Beneficial effect of the present invention is, oxidized starch has low viscosity, and high solid disperses property, minimum gelling.Because oxidized starch has been introduced carbonyl and carboxyl, make the retrogradation trend of amylose be down to bottom line, thereby keep the stability of viscosity.And apply cold-transfer printing thickener of the present invention and can form tough, clear, continuous film, more even than the film of acidified starch or ative starch thickener, the possibility of contraction and explosion still less.Apply cold-transfer printing thickener of the present invention, its water-soluble speed is fast, in cold-transfer printing technique, with the clothing in contact through pretreatment liquid processing, can carry fast dye transfer to fabric face.In addition the dry rear film forming of mill base of applying its allotment has good elasticity, can effectively avoid printing the crackle of design, and be applicable to the mode of printing of garden net, intaglio plate, soft version, can avoid the obstruction of mesh or ink cell.
Detailed description of the invention
Followingly further illustrate the present invention with non-limiting example, it should be noted, it is limitation of the present invention that these embodiment should not be considered as.
Embodiment 1
Be applicable to the cold-transfer printing thickener of vinyl-sulfone reactive dyes.
The percentage by weight that is applicable to the cold-transfer printing thickener each component of vinyl-sulfone reactive dyes is:
Hypochlorite oxidation starch accounts for 5% weight;
The triumphant PRINTOL S of section stamp oil accounts for 1.5% weight;
Low viscosity hydroxyalkyl etherificate starch accounts for 45% weight;
Adjust to 100% weight with deionized water.
The synthetic method of above-mentioned cold-transfer printing thickener:
Take above-mentioned 5% weight hypochlorite oxidation starch and put into container, add again stamp oil and the 45% weight low viscosity hydroxyalkyl etherificate starch of 1.5% weight Ke Kai company, add after deionized water is adjusted to 100% weight and fully stir, treat to dissolve completely with system color all for the moment, become the cold-transfer printing thickener that is applicable to vinyl-sulfone reactive dyes.
Apply the method for the above-mentioned cold-transfer printing paste formulation print paste that is applicable to vinyl-sulfone reactive dyes.
Cold-transfer printing paste formula according to percentage by weight is:
Above-mentioned cold-transfer printing thickener accounts for 55% weight;
Vinyl-sulfone reactive dyes accounts for 15% weight;
Reservehao S accounts for 1% weight;
Dispersant accounts for 7.5% weight;
Levelling agent accounts for 0.5% weight;
Water is adjusted to 100% weight.
Wherein REACTIVE DYES consumption should be according to the allotment of the flower type design colours depth, the vinyl-sulfone reactive dyes of now selecting accounts for 15% weight, reservehao S is 1% weight, dispersant dosage is 1/2nd of REACTIVE DYES consumption, be 7.5% weight, dispersant is selected methanonaphthalene sulfonic acid dispersant, and levelling agent is selected aryl polyethenoxy ether sodium sulfate anion surfactant, is 0.5% weight.
The compound method of above-mentioned cold-transfer printing mill base is:
Add the vinyl-sulfone reactive dyes furnishing pasty state of a small amount of cold water and 15% weight, then add the mixed liquor of the aryl polyethenoxy ether sodium sulfate anion surfactant of methanonaphthalene sulfonic acid dispersant, 0.5% weight of the 1% weight reservehao S that dissolved, 7.5% weight, add again 85 DEG C of left and right warm water that dyestuff is fully dissolved, join after filtering in the cold-transfer printing thickener of 55% weight, and water stirs after adjusting to 100% weight, make the cold-transfer printing mill base of vinyl-sulfone reactive dyes.
Embodiment 2
Be applicable to the cold-transfer printing thickener of symmetrical three pyridine type REACTIVE DYES.
Be applicable to the percentage by weight of the cold-transfer printing thickener each component of symmetrical three pyridine type REACTIVE DYES:
Hydrogen peroxide oxidation starch accounts for 6% weight;
The triumphant PRINTOL S-C of section stamp oil accounts for 1.2 % by weight;
Low-viscosity carboxymethyl etherification starch accounts for 40% weight;
Adjust to 100% weight with deionized water.
The synthetic method of above-mentioned cold-transfer printing thickener:
Take above-mentioned 6% weight hydrogen peroxide oxidation starch, add again the Ke Kai company of 1.2% weight to produce stamp oil and 40% weight low-viscosity carboxymethyl etherification starch, add after deionized water is adjusted to 100% weight and fully stir, treat to dissolve completely with system color all for the moment, become the cold-transfer printing thickener that is applicable to symmetrical three pyridine type REACTIVE DYES.
Apply the method for the above-mentioned cold-transfer printing paste formulation print paste that is applicable to symmetrical three pyridine type REACTIVE DYES.Cold-transfer printing paste formula according to percentage by weight is:
Above-mentioned cold-transfer printing thickener accounts for 30% weight;
Symmetrical three pyridine type REACTIVE DYES account for 5% weight;
Reservehao S accounts for 0.5% weight;
Dispersant accounts for 2.5% weight;
Levelling agent accounts for 0.3% weight;
Water is adjusted to 100% weight.
Wherein REACTIVE DYES consumption should be according to the allotment of the flower type design colours depth, the symmetry three pyridine type REACTIVE DYES of now selecting are 5% weight, reservehao S is 0.5% weight, dispersant dosage is 1/2nd of REACTIVE DYES consumption, be 2.5% weight, dispersant is selected phenolic condensation compound sulfonate dispersant, and levelling agent is 0.3% weight, selects the non-ionic surface active agent of alkane ether type and the mixture that aryl polyethenoxy ether sodium sulfate anion surfactant was modulated by weight 2: 1.
The compound method of above-mentioned cold-transfer printing mill base is:
Add the symmetry three pyridine type REACTIVE DYES furnishing pasty states of a small amount of cold water and 5% weight, then add the reservehao S of 0.5% weight of having dissolved, the phenolic condensation compound sulfonate dispersant of 2.5% weight, the non-ionic surface active agent of the alkane ether type of 0.3% weight and aryl polyethenoxy ether sodium sulfate anion surfactant are by weight the mixture of modulation in 2: 1, add again 85 DEG C of left and right warm water that dyestuff is fully dissolved, join after filtering in the cold-transfer printing thickener of 30% weight, and water stirs after adjusting to 100% weight, make the cold-transfer printing mill base of symmetrical three pyridine type REACTIVE DYES.
Embodiment 3
Be applicable to the cold-transfer printing thickener of ACID DYES.
Be applicable to the percentage by weight of the cold-transfer printing thickener each component of ACID DYES:
Potassium permanganate oxidation starch accounts for 8% weight;
The middle work printing and dyeing ZG-338 of Chemical Co., Ltd. stamp oil accounts for 0.5% weight;
Low-viscosity carboxymethyl etherification starch accounts for 20% weight;
Adjust to 100% weight with deionized water.
The synthetic method of the above-mentioned cold-transfer printing thickener that is applicable to ACID DYES:
Take above-mentioned 8% weight potassium permanganate oxidation starch and put into container, add again the middle work printing and dyeing ZG-338 of Chemical Co., Ltd. stamp oil and the 20% weight low-viscosity carboxymethyl etherification starch of 0.5% weight, add after deionized water is adjusted to 100% weight and fully stir, treat to dissolve completely with system color all for the moment, become the cold-transfer printing thickener that is applicable to vinyl-sulfone reactive dyes.
Apply the method for the above-mentioned preparation print paste that is applicable to ACID DYES.Cold-transfer printing paste formula according to percentage by weight is:
Above-mentioned cold-transfer printing thickener accounts for 45% weight;
ACID DYES accounts for 10% weight;
Reservehao S accounts for 0.8% weight;
Dispersant accounts for 5% weight;
Levelling agent accounts for 0.2% weight;
Water is adjusted to 100% weight.
Wherein ACID DYES consumption is according to the allotment of the flower type design colours depth, the ACID DYES of now selecting is 10% weight, reservehao S is 0.5% weight, dispersant dosage is 1/2nd of ACID DYES consumption, be 5% weight, select fatty alcohol-polyoxyethylene ether silane type dispersant, levelling agent accounts for 0.2% weight, selects the non-ionic surface active agent of alkane ether type.
The compound method of above-mentioned cold-transfer printing mill base is:
Add the ACID DYES furnishing pasty state of a small amount of cold water and 10% weight, then add the mixed liquor of the alkane ether type non-ionic surface active agent of fatty alcohol-polyoxyethylene ether silane type dispersant, 0.2% weight of the 0.8% weight reservehao S that dissolved, 5% weight, add again 85 DEG C of left and right warm water that dyestuff is fully dissolved, join after filtering in the cold-transfer printing thickener of 45% weight, and water stirs after adjusting to 100% weight, make the cold-transfer printing mill base of vinyl-sulfone reactive dyes.
In above-described embodiment 1, embodiment 2 and embodiment 3, carboxyl mass fraction >=0.40% of selected oxidized starch; Selected low viscosity etherification starch, its low viscosity is the former paste of etherification starch by 10% weight, under 25 DEG C of conditions, with Brookfield viscometer, with 20 transfer to tests per minute, its viscosity is 20,000-50,000mPas.
Claims (6)
1. a color paste formulation method for cold-transfer printing thickener, is characterized in that:
The mill base of described cold-transfer printing paste formulation according to the content of the each component of percentage by weight is:
Cold-transfer printing thickener accounts for 30-55% weight, and dyestuff accounts for 0.2-15% weight, and reservehao S accounts for 0.5-1% weight, and dispersant accounts for 0.1-8% weight, and levelling agent accounts for 0.05-0.5% weight, and water is adjusted to 100% weight; Add the dyestuff of a small amount of water and 0.2-15% weight in container, and furnishing pasty state; Then add the mixed liquor of the levelling agent of dispersant, the 0.05-0.5% weight of reservehao S, the 0.1-8% weight of the 0.5-1% weight of having dissolved, add again 85 DEG C of left and right warm water that dyestuff is fully dissolved, after filtration, join in the cold-transfer printing thickener of 30-55% weight, water stirs after adjusting to 100% weight again, makes cold-transfer printing mill base; Wherein, described cold-transfer printing thickener is made up of oxidized starch, stamp oil, etherification starch and deionized water; Described cold-transfer printing thickener according to the each constituent content of percentage by weight is: oxidized starch accounts for 5-8% weight, and stamp oil accounts for 0.5-1.5% weight, and etherification starch accounts for 20-45% weight, adjusts to 100% weight with deionized water; Concrete grammar is that the oxidized starch of 5-8% weight is put into container, add the stamp oil of 0.5-1.5% weight and the etherification starch of 20-45% weight, add again deionized water to fully stirring after 100% weight, treat to dissolve completely with system color all for the moment, become cold-transfer printing thickener.
2. the color paste formulation method of cold-transfer printing thickener according to claim 1, is characterized in that: described dyestuff is selected REACTIVE DYES or ACID DYES.
3. the color paste formulation method of cold-transfer printing thickener according to claim 1, is characterized in that: described dispersant is selected from methanonaphthalene sulfonic acid dispersant or phenolic condensation compound sulfonate dispersant or fatty alcohol-polyoxyethylene ether silane type dispersant.
4. the color paste formulation method of cold-transfer printing thickener according to claim 1, is characterized in that: described levelling agent is selected from the non-ionic surface active agent of alkane ether type, or aryl polyethenoxy ether sodium sulfate anion surfactant, or the two mixture.
5. the color paste formulation method of cold-transfer printing thickener according to claim 1, Ji Tezheng is: carboxyl mass fraction >=0.40% of described oxidized starch; Described oxidized starch is hypochlorite oxidation starch, hydrogen peroxide oxidation starch, potassium permanganate oxidation starch or periodate oxidation starch.
6. cold-transfer printing thickener according to claim 1, is characterized in that: described stamp oil is the nonionic stamp oil taking prosparol as main component.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110364462.8A CN102433777B (en) | 2011-11-17 | 2011-11-17 | Preparation method of cold migration printing gum and color paste thereof |
| TW101142940A TWI481761B (en) | 2011-11-17 | 2012-11-16 | Cold-transfer printing thicker and producing method for color paste thereof |
| PCT/CN2012/084758 WO2013071881A1 (en) | 2011-11-17 | 2012-11-16 | Cold transferring printing thickener and preparation method of color paste thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110364462.8A CN102433777B (en) | 2011-11-17 | 2011-11-17 | Preparation method of cold migration printing gum and color paste thereof |
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| CN102433777A CN102433777A (en) | 2012-05-02 |
| CN102433777B true CN102433777B (en) | 2014-07-23 |
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| CN201110364462.8A Active CN102433777B (en) | 2011-11-17 | 2011-11-17 | Preparation method of cold migration printing gum and color paste thereof |
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| Country | Link |
|---|---|
| CN (1) | CN102433777B (en) |
| TW (1) | TWI481761B (en) |
| WO (1) | WO2013071881A1 (en) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102433777B (en) * | 2011-11-17 | 2014-07-23 | 长胜纺织科技发展(上海)有限公司 | Preparation method of cold migration printing gum and color paste thereof |
| CN103243582A (en) * | 2013-04-16 | 2013-08-14 | 杜芳莉 | Acidic levelling agent and preparation method thereof |
| CN104278565A (en) * | 2014-09-24 | 2015-01-14 | 无锡市东北塘宏良染色厂 | Transfer printing paste |
| CN105442355A (en) * | 2015-12-25 | 2016-03-30 | 罗莱生活科技股份有限公司 | Novel eight-color-separation fabric printing method |
| CN106245378A (en) * | 2016-08-17 | 2016-12-21 | 朱维 | A kind of polyhexamethylene adipamide compositions thickening agent |
| CN108239887B (en) * | 2016-12-27 | 2020-07-31 | 长胜纺织科技发展(上海)有限公司 | Pretreatment method for plate-alignment liquid feeding |
| CN108239888B (en) * | 2016-12-27 | 2020-07-14 | 长胜纺织科技发展(上海)有限公司 | Paperless transfer printing method |
| CN107385978A (en) * | 2017-08-11 | 2017-11-24 | 李月仙 | A kind of two-sided overlay film method for transfer printing |
| CN107869075A (en) * | 2017-12-20 | 2018-04-03 | 苏州润弘贸易有限公司 | Textile printing paste |
| CN115947923B (en) * | 2023-02-17 | 2023-08-04 | 广州山木新材料科技有限公司 | Water-based polyurethane resin and digital hot-dip painting ink containing same |
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| US20070149657A1 (en) * | 2002-11-22 | 2007-06-28 | Roman Skuratowicz | Corrugating adhesives for bonding coated papers and methods for bonding coated papers |
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- 2012-11-16 WO PCT/CN2012/084758 patent/WO2013071881A1/en active Application Filing
- 2012-11-16 TW TW101142940A patent/TWI481761B/en active
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Also Published As
| Publication number | Publication date |
|---|---|
| CN102433777A (en) | 2012-05-02 |
| TW201323683A (en) | 2013-06-16 |
| WO2013071881A1 (en) | 2013-05-23 |
| TWI481761B (en) | 2015-04-21 |
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