CN102423119A - Additive for increasing cigarette smoke moisture and application thereof - Google Patents
Additive for increasing cigarette smoke moisture and application thereof Download PDFInfo
- Publication number
- CN102423119A CN102423119A CN2011102994111A CN201110299411A CN102423119A CN 102423119 A CN102423119 A CN 102423119A CN 2011102994111 A CN2011102994111 A CN 2011102994111A CN 201110299411 A CN201110299411 A CN 201110299411A CN 102423119 A CN102423119 A CN 102423119A
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- Prior art keywords
- additive
- cigarette
- moisture
- smoke
- fiber
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Links
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 83
- 239000000779 smoke Substances 0.000 title claims abstract description 54
- 239000000654 additive Substances 0.000 title claims abstract description 45
- 230000000996 additive effect Effects 0.000 title claims abstract description 42
- 239000000835 fiber Substances 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 17
- -1 polysiloxane Polymers 0.000 claims abstract description 12
- 230000008569 process Effects 0.000 claims abstract description 12
- 125000000753 cycloalkyl group Chemical group 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 8
- 229920001296 polysiloxane Polymers 0.000 claims abstract description 8
- 238000002360 preparation method Methods 0.000 claims abstract description 5
- 239000000126 substance Substances 0.000 claims abstract description 3
- HMDDXIMCDZRSNE-UHFFFAOYSA-N [C].[Si] Chemical group [C].[Si] HMDDXIMCDZRSNE-UHFFFAOYSA-N 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 2
- 125000001183 hydrocarbyl group Chemical group 0.000 claims description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- 125000000962 organic group Chemical group 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 2
- 229920001921 poly-methyl-phenyl-siloxane Polymers 0.000 claims description 2
- 238000006116 polymerization reaction Methods 0.000 claims description 2
- 238000005507 spraying Methods 0.000 claims description 2
- 230000000638 stimulation Effects 0.000 abstract description 6
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 238000000465 moulding Methods 0.000 abstract 1
- 230000001953 sensory effect Effects 0.000 description 11
- 241000208125 Nicotiana Species 0.000 description 9
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 9
- 230000000391 smoking effect Effects 0.000 description 7
- 229920006221 acetate fiber Polymers 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 4
- 238000013441 quality evaluation Methods 0.000 description 4
- 230000008859 change Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 230000007794 irritation Effects 0.000 description 3
- 230000009467 reduction Effects 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 229920002301 cellulose acetate Polymers 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 239000003906 humectant Substances 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 1
- 206010013789 Dry throat Diseases 0.000 description 1
- 241000219000 Populus Species 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 239000012496 blank sample Substances 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000013068 control sample Substances 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 238000004868 gas analysis Methods 0.000 description 1
- 230000005802 health problem Effects 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 229960002715 nicotine Drugs 0.000 description 1
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 1
- 239000008041 oiling agent Substances 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000000523 sample Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention relates to an additive for increasing cigarette smoke moisture and application thereof, belonging to the technical field of cigarette production. The additive disclosed by the invention is while oil, cyclic hydrocarbon oil, polysiloxane or a mixture of while oil and cyclic hydrocarbon oil, wherein the mixture of the while oil and cyclic hydrocarbon oil has the mixed proportion that the two substances are mixed at random in the range of 5-95 percent by weight. In the application of the additive, the additive which accounts for 0.5-5.0 percent of filter tip fiber is uniformly added into the filter tip fiber, namely the additive is uniformly coated on the surface of the fiber in the preparation process of filter tip fiber bundles; or the additive is uniformly sprayed onto the surface of the opened fibers in the moulding process of a filter tip. The additive has the advantages of effectively increasing cigarette smoke moisture, softening smoke, increasing smoke moist feeling, reducing stimulation and improving comfort of the throat and cigarette sense quality and is suitable for various types of cigarettes, especially low-tar cigarettes.
Description
The technical field is as follows:
the invention relates to an additive for improving cigarette smoke moisture and application thereof, belonging to the technical field of cigarette production.
Background art:
with the increasing attention and importance of society on smoking and health problems, harm reduction and tar reduction become core technologies competing in the tobacco industry, but with the reduction of tar content of cigarettes, a great deal of fragrance loss is inevitably caused, and the style and smoking quality of the cigarettes are seriously affected. Particularly for low-tar cigarettes, the development of the low-tar cigarettes is restricted by the problems of thin aroma, dry smoke, increased stimulation, reduced throat comfort and the like. Therefore, how to maintain the aroma of the cigarettes, reduce the irritation and improve the comfort of the throat becomes an urgent problem to be solved in the tobacco industry.
The reasons for the problems of dry smoke, increased stimulation, reduced throat comfort and the like are very complicated, wherein the moisture of the mainstream smoke is a very important factor influencing the problems, and the content of the moisture directly influences the sensory quality of the cigarettes. In view of the importance of cigarette smoke moisture, how to adjust and improve the cigarette mainstream smoke moisture has become an important subject of domestic and foreign research. In recent years, many technologists have studied how to control, maintain and improve the moisture of cigarettes through production processes and external additives, and influence of the moisture on the taste of cigarettes. Xiaowenping (Chinese character)[1]The relation between the moisture of the cigarette and the taste of the cigarette is researched by the people, and the change rule of the influence of the moisture change of the tobacco shreds on the taste of the cigarette is discussed. The cigarette evaluation results show that the moisture of the tobacco shreds has an influence on the smoking taste. The influence is in irregular normal distribution, and the normal distribution tends to move towards the direction of small moisture along with the increase of the cigarette quality. The influence of the moisture change of the cigarettes on the moisture of the smoke is not obvious. Chinese patent 98113287.1 discloses a novel humectant[2]And the moisture of the tobacco shreds can be effectively kept. However, the research work is only limited to the moisture in the tobacco shreds, and the research on the moisture of cigarette smoke is not related. Chinese patent CN100593980C[3]A composite additive for increasing the water content of cigarette smoke is disclosed, which can increase the water content of main stream smoke of cigarette after it is used in cigarette.
The invention improves the moisture content of the mainstream smoke by modifying the acetate fiber tows. The cigarette filter rod material (acetate fiber tow) contains hydroxyl, is easy to be compatible with water due to the action of hydrogen bonds and Van der Waals force, and when cigarette smoke passes through the filter rod, moisture in the smoke is easy to be adsorbed by the tow. At present, the improvement technology of acetate fiber tows for cigarettes for regulating and improving the main stream smoke moisture of the cigarettes and the new material and new technology of filter rods are not reported.
Reference to the literature
[1] Experiments on the effect of moisture on smoking taste of cigarettes were studied [ J ]. yunnan tobacco, 2002 (1): 39-41.
[2] Luscochang, luruilin, a novel tobacco humectant: china, CN1204482[ P ], 1999-01-13.
[3] Poplar leaf Queen, Wangbaoxing, a gem, Xulan, and Yizhimin, a composite additive for improving the smoke moisture of cigarettes and application thereof: china, ZL 200610048649.6[ P ], 2006-8-31.
The invention content is as follows:
the invention aims to provide an additive capable of effectively regulating and improving the moisture of mainstream smoke of cigarettes, keeping the style of the cigarettes unchanged, increasing the moisture of the smoke, reducing the stimulation and improving the comfort of the throat and application thereof.
The purpose of the invention is realized as follows:
an additive for improving the moisture of cigarette smoke is characterized in that the additive is white oil, cyclic hydrocarbon oil, polysiloxane or a mixture of the white oil and the cyclic hydrocarbon oil.
A filter tip additive for increasing the moisture content in the smoke of cigarette features that the polysiloxane has a general formula
Wherein,
r represents an organic group, which may be the same or different, and represents a monovalent hydrocarbon group having 1 to 18 carbon atoms, silicon-carbon bonded, optionally substituted, such as methyl, phenyl, etc.;
n is the degree of polymerization (n is not less than 2);
R1represents a hydrogen atom or an OH group or R.
An additive for improving the moisture of cigarette smoke is characterized in that the polysiloxane mainly comprises the following components: polydimethylsiloxane, polymethylphenylsiloxane.
The additive for improving the moisture of the cigarette smoke is characterized in that the mixing proportion of the mixture of the white oil and the cyclic hydrocarbon oil is as follows: the two substances are respectively mixed randomly within the range of 5-95% by weight.
The application of the additive of the invention is as follows:
the additive has wide application range, is suitable for various types of cigarettes, and is particularly suitable for low-tar cigarettes. The application method comprises two methods:
firstly, taking 0.5-5.0% of additive accounting for the weight ratio of the filter rod fibers, and uniformly coating the additive on the surfaces of the fibers in the preparation process of a fiber tow, namely: in the oiling procedure, the additive is evenly coated on the surface of the fiber, and then the prepared fiber is made into the acetate fiber filter tip according to the common forming process.
Secondly, taking 0.5-5.0% of additive accounting for the weight ratio of the fibers of the filter rod to be added into the fibers in the process of forming the filter rod, namely: uniformly spraying the mixture into opened fiber tows, and preparing the acetate fiber filter tip according to a common forming process.
The invention has the advantages that: (1) through modifying the acid-vinegar fiber tows, the hydrophobicity of the tows is increased, and the adsorption and interception of the filter tip to smoke moisture are reduced, so that the moisture content of mainstream smoke is improved, the comfort of the smoke is improved, the irritation is reduced, and the comfort of the throat is improved. (2) Sufficient raw material sources, simple preparation process and low cost. (3) The application range is wide, and the cigarette filter tip can be applied to different types of cigarettes. (4) The addition process is simple.
The specific implementation mode is as follows:
the present invention will be further clearly understood by the following specific examples. They are not intended to limit the invention.
Mainstream smoke analysis of cigarette samples:
the method adopts GB/T19609, YC/T29-30 and YC/T156-157-2001 standards to detect the total particulate matter, tar content, carbon monoxide content, smoke nicotine content and smoke moisture of the cigarette smoke.
Sensory quality evaluation of cigarette samples:
adjusting cigarette samples according to the national standard GB/T16447 + 1996 atmosphere environment for adjusting and testing tobacco and tobacco products, and performing cigarette sensory quality evaluation by an evaluation expert group according to the regulation of GB 5606.4-2005 cigarette sensory technical requirement.
Examples 1 to 2:
a, B cigarettes were selected, and the cigarettes were respectively attached to a filter rod containing 1% white oil, and the blank sample was not supplemented with additives. The cigarette smoke analysis and detection results and the smoking evaluation results are shown in tables 1 and 2. From the flue gas analysis data it can be seen that: the additive has obvious effect of improving the moisture of the main stream smoke of the cigarette after being applied to the filter tip. The mainstream smoke moisture of the cigarettes was increased by 26.7% and 20%, respectively, compared to the control sample. The results of the smoke panel test in Table 2 show that the compound additive added into the cigarette can soften smoke, increase the moist feeling, reduce the irritation, obviously reduce the dry throat and improve the sensory quality of the cigarette. Meets the requirements of consumers on safety, comfort and mellowness of cigarettes.
TABLE 1 analysis result of cigarette smoke of different brands using filter tip additive
TABLE 2 Effect of mainstream Smoke moisture enhancement on sensory quality of cigarettes
Examples 3 to 6
The application method of the invention in cigarettes is as follows: the prepared additive is uniformly sprayed into the opened cellulose acetate tow according to the dosage of 0.5-1.5 percent (weight percentage) in the process of forming the filter tip, and the cellulose acetate filter tip is prepared according to the common forming process. Then the filter tip is connected with the cigarette according to the conventional cigarette process. And rolling the control cigarette sample according to the same cigarette process on the same production line. And (3) carrying out cigarette mainstream smoke analysis (specific results are shown in table 3) and cigarette sensory quality smoking evaluation.
As shown in Table 3, compared with the control cigarette without the additive, the cigarette containing the additive of the invention has obviously improved main stream smoke moisture, and the improvement rate has certain difference according to the different types and the different dosages of the additive, and the range is from 15.8 percent to 42.1 percent. . Sensory quality evaluation results show that the addition of the additive has no influence on the original style and taste of the cigarette, and can soften smoke, improve the smoothness of the smoke, increase the moisture of the smoke, reduce stimulation, improve the comfort of the throat and improve the sensory quality of the cigarette.
Examples 7 to 9
In the preparation process of the filter tip fiber, namely the oiling treatment process, the additive white oil, the cyclic hydrocarbon oil and the polysiloxane are added into the oiling agent and evenly coated on the surface of the fiber tows, and the prepared fiber is prepared into the acetate fiber filter tip according to the common forming process. After the filter tip is applied to cigarettes, the moisture of the main stream smoke of the cigarettes is respectively increased by 26.3%, 211% and 15.8%. The results are shown in Table 3. Sensory quality evaluation results show that the additive keeps the style of the cigarette unchanged, increases the moisture of smoke, reduces stimulation, improves the throat comfort and improves the sensory smoking quality of the cigarette.
TABLE 3 application effect of additives for increasing cigarette smoke moisture
Claims (5)
1. An additive for improving the moisture of cigarette smoke is characterized in that the additive is white oil, cyclic hydrocarbon oil, polysiloxane or a mixture of the white oil and the cyclic hydrocarbon oil.
2. The additive for increasing the moisture content of cigarette smoke according to claim 1, wherein the polysiloxane has the general formula
Wherein,
r represents an organic group, which may be the same or different, and represents a monovalent hydrocarbon group having 1 to 18 carbon atoms, silicon-carbon bonded, optionally substituted, such as methyl, phenyl, etc.;
n is the degree of polymerization (n is not less than 2);
R1represents a hydrogen atom or a 0H group or R.
3. The additive for increasing the moisture content of cigarette smoke according to claim 1, wherein the polysiloxane is mainly selected from the group consisting of: polydimethylsiloxane, polymethylphenylsiloxane.
4. The additive for improving the moisture of the smoke of the cigarettes according to claim 1, wherein the mixture of the white oil and the cyclic hydrocarbon oil is prepared from the following components in percentage by weight: the two substances are respectively mixed randomly within the range of 5-95% by weight.
5. The use of the additive for increasing the moisture content of cigarette smoke according to claim 1, wherein the additive comprises: uniformly adding an additive accounting for 0.5-5.0% of the weight of the filter rod fiber into the filter rod fiber, namely: in the preparation process of the filter rod fiber tows, the fiber tows are uniformly coated on the surface of the fiber; or uniformly spraying the mixture on the surface of the opened fiber in a filter tip forming process.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011102994111A CN102423119A (en) | 2011-09-29 | 2011-09-29 | Additive for increasing cigarette smoke moisture and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011102994111A CN102423119A (en) | 2011-09-29 | 2011-09-29 | Additive for increasing cigarette smoke moisture and application thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102423119A true CN102423119A (en) | 2012-04-25 |
Family
ID=45957221
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011102994111A Pending CN102423119A (en) | 2011-09-29 | 2011-09-29 | Additive for increasing cigarette smoke moisture and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102423119A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
| CN103504474A (en) * | 2013-10-16 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick capable of effectively improving water absorption of filter element |
| CN105852195A (en) * | 2015-01-22 | 2016-08-17 | 于杰 | Functional tobacco shreds |
| CN106723335A (en) * | 2016-12-09 | 2017-05-31 | 河南中烟工业有限责任公司 | A kind of strawberry aroma diacetate fiber and its application in ramuscule cigarette |
| CN108936804A (en) * | 2018-09-13 | 2018-12-07 | 广东中烟工业有限责任公司 | A kind of cigarette filter rod for improving flue gas and protecting fragrant effect |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3654934A (en) * | 1967-02-01 | 1972-04-11 | Joseph F Martin | Tobacco smoke filter |
| JPS5052296A (en) * | 1973-09-12 | 1975-05-09 | ||
| US4163453A (en) * | 1976-10-12 | 1979-08-07 | Liggett Group Inc. | 7-Alkoxy-1,2-benzopyrones as tobacco flavorants |
| US4194517A (en) * | 1976-10-06 | 1980-03-25 | B.A.T. Cigaretten-Fabriken Gmbh | Filter for cigarettes, cigarillos or pipes |
| CN1081082A (en) * | 1993-07-17 | 1994-01-26 | 姚广泉 | A kind of conditioner that is suitable for polypropylene fibre cigarette filter-tip production usefulness |
| JP2008289396A (en) * | 2007-05-23 | 2008-12-04 | Mitsubishi Rayon Co Ltd | Sheath/core-type cigarette filter |
| WO2010118122A1 (en) * | 2009-04-08 | 2010-10-14 | Oranjeway, Inc. | Smoke filtration device and method |
-
2011
- 2011-09-29 CN CN2011102994111A patent/CN102423119A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3654934A (en) * | 1967-02-01 | 1972-04-11 | Joseph F Martin | Tobacco smoke filter |
| JPS5052296A (en) * | 1973-09-12 | 1975-05-09 | ||
| US4194517A (en) * | 1976-10-06 | 1980-03-25 | B.A.T. Cigaretten-Fabriken Gmbh | Filter for cigarettes, cigarillos or pipes |
| US4163453A (en) * | 1976-10-12 | 1979-08-07 | Liggett Group Inc. | 7-Alkoxy-1,2-benzopyrones as tobacco flavorants |
| CN1081082A (en) * | 1993-07-17 | 1994-01-26 | 姚广泉 | A kind of conditioner that is suitable for polypropylene fibre cigarette filter-tip production usefulness |
| JP2008289396A (en) * | 2007-05-23 | 2008-12-04 | Mitsubishi Rayon Co Ltd | Sheath/core-type cigarette filter |
| WO2010118122A1 (en) * | 2009-04-08 | 2010-10-14 | Oranjeway, Inc. | Smoke filtration device and method |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103504475A (en) * | 2013-10-11 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
| CN103504475B (en) * | 2013-10-11 | 2015-06-17 | 红云红河烟草(集团)有限责任公司 | Hydrophobic moistening modifier for cigarette filter stick and application thereof |
| CN103504474A (en) * | 2013-10-16 | 2014-01-15 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick capable of effectively improving water absorption of filter element |
| CN103504474B (en) * | 2013-10-16 | 2015-06-17 | 红云红河烟草(集团)有限责任公司 | Cigarette filter stick capable of effectively improving water absorption of filter element |
| CN105852195A (en) * | 2015-01-22 | 2016-08-17 | 于杰 | Functional tobacco shreds |
| CN106723335A (en) * | 2016-12-09 | 2017-05-31 | 河南中烟工业有限责任公司 | A kind of strawberry aroma diacetate fiber and its application in ramuscule cigarette |
| CN108936804A (en) * | 2018-09-13 | 2018-12-07 | 广东中烟工业有限责任公司 | A kind of cigarette filter rod for improving flue gas and protecting fragrant effect |
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Application publication date: 20120425 |