CN102391680A - Disperse dye composite for dyeing and printing polyester spandex fiber - Google Patents
Disperse dye composite for dyeing and printing polyester spandex fiber Download PDFInfo
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- CN102391680A CN102391680A CN201110211817XA CN201110211817A CN102391680A CN 102391680 A CN102391680 A CN 102391680A CN 201110211817X A CN201110211817X A CN 201110211817XA CN 201110211817 A CN201110211817 A CN 201110211817A CN 102391680 A CN102391680 A CN 102391680A
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- 0 C*(C)N(*)C(C=C1)=CC(*)[C@]1N=Nc(cc1)c(*)cc1[N+]([O-])=O Chemical compound C*(C)N(*)C(C=C1)=CC(*)[C@]1N=Nc(cc1)c(*)cc1[N+]([O-])=O 0.000 description 3
- RTSFYDHMSFFZTI-WCWDXBQESA-N CN(Cc1ccccc1)c(cc1)ccc1/N=N/c(c(Cl)cc([N+]([O-])=O)c1)c1Cl Chemical compound CN(Cc1ccccc1)c(cc1)ccc1/N=N/c(c(Cl)cc([N+]([O-])=O)c1)c1Cl RTSFYDHMSFFZTI-WCWDXBQESA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
- D06P1/18—Azo dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/24—Polyamides; Polyurethanes
- D06P3/26—Polyamides; Polyurethanes using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
Abstract
The invention discloses a disperse dye composite for dyeing and printing polyester spandex fiber; the disperse dye composite mainly comprises the following components in percentage by weight: 34%-88% of component A, 2.5%-23% of component B, 6.5%-47% of component C, 3%-38% of component D, 0%-3% of component E and 0%-3.5% of component F. The disperse dye composite of the invention is particularly suitable for dyeing and printing the polyester spandex fiber, has very excellent compatibility, high dye-uptake, various excellent fastnesses such as solarization resistance fastness, rubbing resistance fastness, sublimation resistance fastness and the like for dyeing the polyester spandex textiles, and particularly very good washing resistance fastness and is one of 'extra-high washing fastness' products.
Description
Technical field
The present invention relates to a kind of disperse dye composition, particularly a kind of disperse dye composition of washing spandex fibre dyeing and stamp that is applicable to.
Background technology
Dyestuff is pieced together the technology of mixing exquisiteness day by day, and various composite assembly union dyeing material make rapid progress, and deep color dispersion dyes occupies maximum ratio, especially black, blue dye species.To this, industry has been released the black dyes that multiple composite assembly mixes.Though and each item dyeing behavior on polyster fibre of black disperse dye in the market is all excellent, remain further to be improved in the dyeing behavior of washing on the spandex fibre of gained popularity.Therefore, dyeing is badly in need of seeking one at the economical dispersed dye of washing each item dyeing behavior excellence on the spandex fibre.
Summary of the invention
The invention provides a kind of being applicable to and wash spandex fibre dyeing and stamp, coloured light is bright-coloured, compatibleness good, the economical disperse dye composition that light fastness, washing fastness are all high.
A kind of disperse dye composition that is used to wash spandex fibre dyeing and stamp, its weight percent is formed and is mainly comprised:
Component A 34%～88%
B component 2.5%～23%
Component C 6.5%～47%
Component D 3%～38%
Component E 0%～3%
Component F 0%～3.5%
Described component A is one or more in the compound shown in the formula (1):
In the formula (1), X
1Be cyanic acid or halogen; R
1, R
2Independent separately is C
1～C
4Alkyl ,-CH
2COOR
5,-C
2H
4COOR
6Or-C
2H
4OCOCH
3, R
3, R
4Independent separately is C
1～C
4Alkyl, R wherein
5, R
6Independent separately is C
1～C
4Alkyl;
Described B component is one or more in the compound shown in the formula (2):
In the formula (2), X
2Be cyanic acid or nitro; R
7Be C
1～C
4Alkyl, phenyl or C
1～C
4Alkoxyl group, R
8, R
9Independent separately is C
1～C
4Alkyl, n is 1 or 2;
Described component C is one or more in the compound shown in the formula (3):
In the formula (3), X
3Be nitro or hydrogen: work as X
3During for nitro, X
4Be hydrogen or methoxyl group; Work as X
3During for hydrogen, X
4For
R
10Be C
1～C
4Alkyl;
Described component D is one or more in the compound shown in the formula (4):
In the formula (4), R
11Be hydrogen or C
1～C
4Alkoxyl group, R
12Be C
1～C
4Alkyl, R
13, R
14Independent separately is C
1～C
4Alkyl, m is 1 or 2;
Described component E is the compound shown in the formula (5):
Described component F is the compound shown in the formula (6):
When the dye composite of selecting for use mainly was made up of component A, B component, component C and component D, the weight percent of preferred disperse dye composition was formed and is comprised:
Component A 45%～88%
B component 2.5%～12%
Component C 6.5%～31%
Component D 3%～25%.
In order to improve light fastness, available dye composite mainly is made up of component A, B component, component C, component D and component E, this moment disperse dye composition, by weight percentage, component comprises:
Component A 34%～79.5%
B component 5%～23%
Component C 10%～40%
Component D 5%～38%
Component E 0.5%～2%.
In order further to improve washing fastness, available dye composite also can be made up of component A, B component, component C, component D and component F, disperse dye composition at this moment, and by weight percentage, component comprises:
Component A 34%～79.5%
B component 5%～23%
Component C 10%～40%
Component D 5%～38%
Component F 0.5%～2.5%.
In addition, all more excellent when needs each item fastness ability, when washing fastness significantly improved, preferred disperse dye composition also can be made up of component A, B component, component C, component D, component E and component F, and by weight percentage, component comprises:
Component A 36%～78.5%
B component 4.5%～20%
Component C 10%～36%
Component D 6%～28%
Component E 0.5%～3%
Component F 0.5%～3.5%.
Take all factors into consideration being easy to get property of raw material and dyeing behavior, described component A is preferably the mixture of one or more in the compound shown in the formula (1-1) to (1-5):
Described B component is preferably the mixture of one or both in the compound shown in formula (2-1), (2-2):
Described component C is preferably the mixture of one or more in the compound shown in the formula (3-1) to (3-6):
Described component D be preferably formula (4-1) (4-2) shown in one or both mixture in the compound:
The disperse dye composition that is used to wash spandex fibre dyeing and stamp of the present invention needs to add auxiliary agent when reality is used, said auxiliary agent is dispersion agent, diffusant and other tensio-active agents etc. that dispersed dye are used always when composite.Preferred auxiliary agent comprises one of following or its mixture: naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, alkyl naphthalene sulfonic acid formaldehyde condensation products.Like condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF), naphthalene sulfonic acidformaldehyde condensation product (dispersing agent NNO), benzyl naphthalene sulfonic formaldehyde condensation compound (dispersing agent CNF), sodium lignosulfonate (xylogen 83A, 85A) etc.The ratio of the weight that the weight that usually, adds auxiliary agent and dye component A～F are total is 0.6～4.8: 1.
Disperse dye composition of the present invention can be used following method preparation:
With component A, B component and component C and component D, component E, component F, after mixing by said ratio, in the presence of auxiliary agent, water or other tensio-active agent, carry out the particlized processing with kibblers such as sand mill or shredders; Also can the former dyestuff of component A, B component, component C, component D, component E, component F be carried out micropartical with kibblers such as sand mill or shredders respectively in the presence of auxiliary agent, water or other tensio-active agent, mix by said ratio again.
Disperse dye composition of the present invention, aqueous with can be after sand mill or the shredder grinding, can be powdery, particulate state after the spraying drying.
Described component A, B component, component C, component D, component E, component F all can adopt the commercially available prod.
Disperse dye composition of the present invention; Be very suitable for washing/spandex fibre on dyeing and stamp; Compatibleness is splendid, and dye uptake is high, and washing/spandex fabric on each item fastness such as painted sun-resistant fastness, fastness to rubbing, fastness to sublimation excellent; Extraordinary washing fastness is particularly arranged, be one of " extra-high-speed washing fastness series " product.
Embodiment
Below in conjunction with specific embodiment the present invention is further described, but protection scope of the present invention is not limited to this.
Embodiment 1～15
According to the data in the table 1, component A, B component, component C, component D, component E, component F, auxiliary agent and water mixture are ground dispersion with sand mill, carry out spraying drying then.Component A wherein, B component, component C, component D, component E, component F all can adopt the dispersed dye of Zhejiang Province Runtu intercalated Co., Ltd's production or prepared voluntarily by existing method.
Structural formula (1-1) preparation method is: after 2,4 dinitro 6 bromo aniline diazotization, again with 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (1-2) preparation method is: by 2, after 4-dinitrobenzene-6-chloroaniline diazotization, again with 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (1-3) preparation method is: by 2, after 4-dinitrobenzene-6-cyano-aniline diazotization, again with 2-oxyethyl group-5-acetylaminohydroxyphenylarsonic acid N, the coupling of N-dimethoxy phosphinylidyne MEA forms;
Structural formula (1-4) preparation method is: after 2,4 dinitro 6 bromo aniline diazotization, again with 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N, the coupling of N-dimethoxy phosphinylidyne MEA forms;
Structural formula (1-5) preparation method is: after 2,4 dinitro 6 bromo aniline diazotization, form with 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N-ethyl-N-methoxy phosphinylidyne monomethylaniline coupling again;
Structural formula (2-1) preparation method is: by 2, after the 4-dinitraniline diazotization, again with m-acetamino-N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (2-2) preparation method is: after 2 cyano 4 nitro aniline diazotization, again with m-acetamino-N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (3-1) by 2-nitro-4-anisidine diazotization after, again with 1-ethyl-6-hydroxy-4-methyl-2-oxo-1,2-dihydro-3-pyridine nitrile coupling forms;
The DISPERSE YELLOW 126# that structural formula (3-2) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce;
The DISPERSE YELLOW 119# that structural formula (3-3) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce;
The DISPERSE YELLOW 114# that structural formula (3-4) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce;
Structural formula (3-5) by methylsulphonic acid aniline diazotization after, again with 1,4-dimethyl--3-cyanic acid-6-hydroxyl-2-pyridone coupling forms;
Structural formula (3-6) by a N-benzoylaniline diazotization after, again with 1,4-dimethyl--3-cyanic acid-6-hydroxyl-2-pyridone coupling forms;
Structural formula (4-1) preparation method is: by 2, after the 4-dinitro thiophene diazotization, again with 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (4-2) preparation method is: by 2, after the 4-dinitro thiophene diazotization, again with m-acetamino-N, the coupling of N-dimethoxy phosphinylidyne monomethylaniline forms;
Structural formula (5) preparation method is: by 2, after the 6-two chloro-4-N-methyl-p-nitroaniline diazotization, form with N-methyl-Phenhenzamine coupling again;
The Disperse Blue-60 # that structural formula (6) can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce;
Table 1
Performance test
The dye mixture that the foregoing description 1～15 is made carries out performance test, and testing method is following:
According to the GB/T2394-2003 similar methods, it is 1% dispersed dye suspension-s that the disperse dye composition that will be made by embodiment 1～15, water are mixed with mass percent concentration respectively; Draw 20ml dispersed dye suspension-s and mix, regulate dye bath pH to 5, be warmed up to 60 ℃ then with acetic acid with the water of 80m; Put into 2g simultaneously respectively to wash/the spandex trevira carries out high-temperature pressure dyeing; In 35 minutes, be warmed up to 130 ℃, be incubated 30 minutes, be cooled to 80 ℃ of samplings.
Observe cloth specimen coloured light and adopt GB/T3921-1997, GB/T8427-1998, GB/T5718-1997, GB/T3920-1997 to measure its dyefastness, measure the result and see table 2.
Table 2 (unit: level)
Can know by last table, this disperse dye composition washing/spandex on painted each item fastness all very excellent, particularly washing fastness is significantly improved.
Claims (10)
1. disperse dye composition that is used to wash spandex fibre dyeing and stamp, its weight percent composition mainly comprises:
Component A 34%～88%
B component 2.5%～23%
Component C 6.5%～47%
Component D 3%～38%
Component E 0%～3%
Component F 0%～3.5%
Described component A is one or more in the compound shown in the formula (1):
In the formula (1), X
1Be cyanic acid or halogen; R
1, R
2Independent separately is C
1～C
4Alkyl ,-CH
2COOR
5,-C
2H
4COOR
6Or-C
2H
4OCOCH
3, R
3, R
4Independent separately is C
1～C
4Alkyl, R wherein
5, R
6Independent separately is C
1～C
4Alkyl;
Described B component is one or more in the compound shown in the formula (2):
In the formula (2), X
2Be cyanic acid or nitro; R
7Be C
1～C
4Alkyl, phenyl or C
1～C
4Alkoxyl group, R
8, R
9Independent separately is C
1～C
4Alkyl, n is 1 or 2;
Described component C is one or more in the compound shown in the formula (3):
In the formula (3), X
3Be nitro or hydrogen: work as X
3During for nitro, X
4Be hydrogen or methoxyl group; Work as X
3During for hydrogen, X
4For
R
10Be C
1～C
4Alkyl;
Described component D is one or more in the compound shown in the formula (4):
In the formula (4), R
11Be hydrogen or C
1～C
4Alkoxyl group, R
12Be C
1～C
4Alkyl, R
13, R
14Independent separately is C
1～C
4Alkyl, m is 1 or 2;
Described component E is the compound shown in the formula (5):
Described component F is the compound shown in the formula (6):
2. the disperse dye composition that is used to wash spandex fibre dyeing and stamp according to claim 1 is characterized in that described weight percent is formed and comprised:
Component A 45%～88%
B component 2.5%～12%
Component C 6.5%～31%
Component D 3%～25%.
3. the disperse dye composition that is used to wash spandex fibre dyeing and stamp according to claim 1 is characterized in that described weight percent is formed and comprised:
Component A 34%～79.5%
B component 5%～23%
Component C 10%～40%
Component D 5%～38%
Component E 0.5%～2%.
4. the disperse dye composition that is used to wash spandex fibre dyeing and stamp according to claim 1 is characterized in that described weight percent is formed and comprised:
Component A 34%～79.5%
B component 5%～23%
Component C 10%～40%
Component D 5%～38%
Component F 0.5%～2.5%.
5. the disperse dye composition that is used to wash spandex fibre dyeing and stamp according to claim 1 is characterized in that described weight percent is formed and comprised:
Component A 36%～78.5%
B component 4.5%～20%
Component C 10%～36%
Component D 6%～28%
Component E 0.5%～3%
Component F 0.5%～3.5%.
6. according to the described disperse dye composition that is used to wash spandex fibre dyeing and stamp of the arbitrary claim of claim 1～5, it is characterized in that described component A is the mixture of one or more in the compound shown in the formula (1-1) to (1-5):
7. according to the described disperse dye composition that is used to wash spandex fibre dyeing and stamp of the arbitrary claim of claim 1～5, it is characterized in that described B component is the mixture of one or both in the compound shown in formula (2-1), (2-2):
8. according to the described disperse dye composition that is used to wash spandex fibre dyeing and stamp of the arbitrary claim of claim 1～5, it is characterized in that described component C is the mixture of one or more in the compound shown in the formula (3-1) to (3-6):
9. according to the described disperse dye composition that is used to wash spandex fibre dyeing and stamp of the arbitrary claim of claim 1～5, it is characterized in that described component D is the mixture of one or both in the compound shown in formula (4-1), (4-2):
10. according to the described disperse dye composition that is used to wash spandex fibre dyeing and stamp of the arbitrary claim of claim 1～5; It is characterized in that; Described disperse dye composition need add auxiliary agent when using, and the weight that auxiliary agent adds is 0.6～4.8 times of dye component A～F gross weight; Described auxiliary agent comprises one or more in naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, the alkyl naphthalene sulfonic acid formaldehyde condensation products.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310537347.5A CN103554992B (en) | 2011-07-27 | 2011-07-27 | A kind of disperse dye composition for washing spandex fibre dyeing and stamp |
| CN201110211817.XA CN102391680B (en) | 2011-07-27 | 2011-07-27 | Disperse dye composite for dyeing and printing polyester spandex fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110211817.XA CN102391680B (en) | 2011-07-27 | 2011-07-27 | Disperse dye composite for dyeing and printing polyester spandex fiber |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310537347.5A Division CN103554992B (en) | 2011-07-27 | 2011-07-27 | A kind of disperse dye composition for washing spandex fibre dyeing and stamp |
| CN201310535081.0A Division CN103554991B (en) | 2011-07-27 | 2011-07-27 | Disperse dye composition for polyester/spandex fiber dyeing and printing |
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| Publication Number | Publication Date |
|---|---|
| CN102391680A true CN102391680A (en) | 2012-03-28 |
| CN102391680B CN102391680B (en) | 2014-11-05 |
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| CN201110211817.XA Active CN102391680B (en) | 2011-07-27 | 2011-07-27 | Disperse dye composite for dyeing and printing polyester spandex fiber |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102942806A (en) * | 2012-11-17 | 2013-02-27 | 江苏德旺化工工业有限公司 | Dispersing blue dyestuff |
| CN103073921A (en) * | 2012-12-30 | 2013-05-01 | 浙江龙盛集团股份有限公司 | Dispersed dark dye composition |
| CN103421347A (en) * | 2013-09-02 | 2013-12-04 | 杭州福莱蒽特精细化工有限公司 | High washing fastness dispersed dark blue dye composition |
| CN103525125A (en) * | 2013-10-23 | 2014-01-22 | 江苏德旺化工工业有限公司 | Disperse dye |
| EP2754696A1 (en) * | 2013-01-15 | 2014-07-16 | DyStar Colours Distribution GmbH | AOX-free navy and black disperse dye mixtures |
| WO2014108357A1 (en) * | 2013-01-14 | 2014-07-17 | Dystar Colours Distribution Gmbh | High wet-fast disperse dye mixtures |
| CN104710839A (en) * | 2013-12-31 | 2015-06-17 | 江苏吉华化工有限公司 | Disperse dye mixture |
| CN104744964A (en) * | 2013-12-29 | 2015-07-01 | 浙江龙盛集团股份有限公司 | Disperse blue dye monomeric compound and disperse dye |
| CN114213872A (en) * | 2021-12-27 | 2022-03-22 | 维昂(山东)纺织科技有限公司 | Disperse dye composition, disperse dye product and application thereof |
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- 2011-07-27 CN CN201310537347.5A patent/CN103554992B/en active Active
- 2011-07-27 CN CN201110211817.XA patent/CN102391680B/en active Active
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|---|---|---|---|---|
| EP0675174A1 (en) * | 1994-02-04 | 1995-10-04 | Nippon Kayaku Kabushiki Kaisha | Dye composition and method of dyeing hydrophobic fiber therewith |
| CN1235625A (en) * | 1996-11-01 | 1999-11-17 | 日本化药株式会社 | Dye composition and method for dyeing hydrophobic fiber with the same |
| JP2004339252A (en) * | 2003-05-12 | 2004-12-02 | Dystar Japan Ltd | Disperse dye mixture suitable for dyeing composite material of polyurethane and polyester |
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Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102942806A (en) * | 2012-11-17 | 2013-02-27 | 江苏德旺化工工业有限公司 | Dispersing blue dyestuff |
| CN103073921A (en) * | 2012-12-30 | 2013-05-01 | 浙江龙盛集团股份有限公司 | Dispersed dark dye composition |
| CN103073921B (en) * | 2012-12-30 | 2014-11-26 | 浙江龙盛集团股份有限公司 | Dispersed dark dye composition |
| CN111423743A (en) * | 2013-01-14 | 2020-07-17 | 德司达染料分销有限公司 | AOX-free navy blue and black disperse dyes |
| US9534118B2 (en) | 2013-01-14 | 2017-01-03 | Dystar Colours Distribution Gmbh | High wet fast disperse dye mixtures |
| WO2014108357A1 (en) * | 2013-01-14 | 2014-07-17 | Dystar Colours Distribution Gmbh | High wet-fast disperse dye mixtures |
| US9493657B2 (en) | 2013-01-14 | 2016-11-15 | Dystar Colours Distribution Gmbh | AOX-free navy and black disperse dyes |
| CN104919006A (en) * | 2013-01-14 | 2015-09-16 | 德司达染料分销有限公司 | AOX-free navy and black disperse dye mixtures |
| JP2016516097A (en) * | 2013-01-14 | 2016-06-02 | ダイスター・カラーズ・ディストリビューション・ゲゼルシャフト・ミト・ベシュレンクテル・ハフツング | Highly wet fast disperse dye mixture |
| EP2754696A1 (en) * | 2013-01-15 | 2014-07-16 | DyStar Colours Distribution GmbH | AOX-free navy and black disperse dye mixtures |
| CN103421347A (en) * | 2013-09-02 | 2013-12-04 | 杭州福莱蒽特精细化工有限公司 | High washing fastness dispersed dark blue dye composition |
| CN103421347B (en) * | 2013-09-02 | 2014-08-27 | 杭州福莱蒽特精细化工有限公司 | High washing fastness dispersed dark blue dye composition |
| CN103525125A (en) * | 2013-10-23 | 2014-01-22 | 江苏德旺化工工业有限公司 | Disperse dye |
| CN104744964A (en) * | 2013-12-29 | 2015-07-01 | 浙江龙盛集团股份有限公司 | Disperse blue dye monomeric compound and disperse dye |
| CN104744964B (en) * | 2013-12-29 | 2017-04-05 | 浙江龙盛集团股份有限公司 | A kind of dispersed blue dye monomeric compound and disperse dyes |
| CN104710839A (en) * | 2013-12-31 | 2015-06-17 | 江苏吉华化工有限公司 | Disperse dye mixture |
| CN104710839B (en) * | 2013-12-31 | 2016-09-14 | 江苏吉华化工有限公司 | A kind of admixture of disperse dyes |
| CN114213872A (en) * | 2021-12-27 | 2022-03-22 | 维昂(山东)纺织科技有限公司 | Disperse dye composition, disperse dye product and application thereof |
| CN114213872B (en) * | 2021-12-27 | 2023-12-22 | 维昂(山东)纺织科技有限公司 | Disperse dye composition, disperse dye product and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103554992A (en) | 2014-02-05 |
| CN102391680B (en) | 2014-11-05 |
| CN103554992B (en) | 2015-08-12 |
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