CN102388920A - Organic and inorganic composite pesticide and preparation method thereof - Google Patents
Organic and inorganic composite pesticide and preparation method thereof Download PDFInfo
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- CN102388920A CN102388920A CN2011103108122A CN201110310812A CN102388920A CN 102388920 A CN102388920 A CN 102388920A CN 2011103108122 A CN2011103108122 A CN 2011103108122A CN 201110310812 A CN201110310812 A CN 201110310812A CN 102388920 A CN102388920 A CN 102388920A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses an organic and inorganic composite pesticide and a preparation method thereof. The preparation method comprises the following steps of: weighing the following components in parts by weight: 6-10 parts of diammonium phosphate, 3-5 parts of ammonium chloride, 2-4 parts of sodium chloride, 2-4 parts of sodium sulfate, 3-5 parts of phenol, 3-5 parts of alkali, 0.5-2 parts of carbendazim, 0.2-0.5 part of bacteriostatic mildewcide and the balance of distilled water; respectively adding the components into a stirrer and stirring, and then putting in a reaction kettle; stirring for 10-30 minutes at 60-90 DEG C; and cooling and filtering to finally obtain the organic and inorganic composite pesticide. The organic and inorganic composite pesticide has the advantage of good effect, and the preparation process is simple and can be put into industrial application.
Description
Technical field
The present invention relates to a kind of organic and inorganic compounding agricultural chemicals, particularly relate to a kind of organic and inorganic compounding agricultural chemicals and preparation method thereof.
Background technology
Organic agricultural chemicals is to be one type of agricultural chemicals of active ingredient with compounds such as organochlorine, organic phosphor, Organic fluoride, organic sulfur, organic copper.This type agricultural chemicals has insecticide, bactericide, miticide, weed killer herbicide, nematocide and rodenticide, for example chlorophos, parathion etc.Be to use one type of maximum agricultural chemicals.
Inorganic pesticide mainly contains calcium arsenate, lead arsenate, aluminum phosphate, lime sulfur mixture, copper sulphate, bordeaux mixture etc.This type action of agricultural chemicals is more single, and kind is few, and drug effect is low, and is prone to poisoning takes place, so present most kind is replaced by synthetic organic pesticide.
Summary of the invention
In order to overcome the defective that above-mentioned prior art exists, the present invention provides a kind of organic and inorganic compounding agricultural chemicals, and the preparation method of this agricultural chemicals is provided simultaneously, and this agricultural chemicals is effective, and the preparation method is simple.
For realizing above-mentioned purpose, concrete scheme of the present invention is:
Scheme one: a kind of organic and inorganic compounding agricultural chemicals comprise diammonium phosphate, ammonium chloride, sodium chloride, sodium sulphate, phenol, alkali, carbendazim, antibacterial mould inhibitor, all the other are distilled water; Count by weight: the antibacterial mould inhibitor of the alkali of the sodium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the sodium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are for distilled water.
Scheme two: a kind of organic and inorganic compounding agricultural chemicals comprise diammonium phosphate, ammonium chloride, potassium chloride, potassium sulphate, phenol, alkali, carbendazim, antibacterial mould inhibitor, all the other are distilled water; Count by weight: the antibacterial mould inhibitor of the alkali of the potassium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the potassium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are for distilled water.
A kind ofly prepare organic and the method inorganic compounding agricultural chemicals, these method concrete steps are:
Step 1, each component add in the agitator respectively according to the parts by weight ratio and stir;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 10-30 minute, and temperature is 60-90 ℃;
Step 4, cooling is filtered.
Among the present invention, said phenol is a kind of in cresols, the orthoresol.
Among the present invention, said alkali is organic base; Said organic base is a kind of in sodium methoxide, the potassium ethoxide.
Among the present invention, said antibacterial mould inhibitor is a kind of in benzimidazolyl-2 radicals-aminocarbamic acid methyl esters, the copper 8-quinolinolate.
The invention has the beneficial effects as follows: efficient, safety, environmental protection, cost are low, effective; Technology of the present invention is simple, and is convenient and swift, greatly improved operating efficiency, and device therefor can be realized industrial applications for process equipment commonly used.
Embodiment:
Be easy to understand understanding in order to make technological means of the present invention, creation characteristic and to reach purpose, further set forth the present invention below in conjunction with specific embodiment
Embodiment 1.
Step 1; With the diammonium phosphate of 6KG, the ammonium chloride of 3KG, the sodium chloride of 2KG, the sodium sulphate of 2KG, the cresols of 3KG, the sodium methoxide of 3KG, the carbendazim of 0.5KG, benzimidazolyl-2 radicals-aminocarbamic acid methyl esters of 0.2KG, the distilled water of 50KG, add in the agitator respectively and stir;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 10 minutes, and temperature is 60 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 2.
Step 1 with the diammonium phosphate of 10KG, the ammonium chloride of 5KG, the sodium chloride of 4KG, the sodium sulphate of 4KG, the orthoresol of 5KG, the potassium ethoxide of 5KG, the carbendazim of 2KG, the copper 8-quinolinolate of 0.5KG, the distilled water of 60KG, adds in the agitator respectively and stirs;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 30 minutes, and temperature is 90 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 3.
Step 1 with the diammonium phosphate of 8KG, the ammonium chloride of 4KG, the sodium chloride of 3KG, the sodium sulphate of 3KG, the orthoresol of 4KG, the potassium ethoxide of 4KG, the carbendazim of 1KG, the copper 8-quinolinolate of 0.3KG, the distilled water of 55KG, adds in the agitator respectively and stirs;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 20 minutes, and temperature is 75 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 4.
Step 1; With the diammonium phosphate of 6KG, the ammonium chloride of 3KG, the potassium chloride of 2KG, the potassium sulphate of 2KG, the cresols of 3KG, the sodium methoxide of 3KG, the carbendazim of 0.5KG, benzimidazolyl-2 radicals-aminocarbamic acid methyl esters of 0.2KG, the distilled water of 50KG, add in the agitator respectively and stir;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 10 minutes, and temperature is 60 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 5.
Step 1 with the diammonium phosphate of 10KG, the ammonium chloride of 5KG, the potassium chloride of 4KG, the potassium sulphate of 4KG, the orthoresol of 5KG, the potassium ethoxide of 5KG, the carbendazim of 2KG, the copper 8-quinolinolate of 0.5KG, the distilled water of 60KG, adds in the agitator respectively and stirs;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 30 minutes, and temperature is 90 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 6.
Step 1 with the diammonium phosphate of 8KG, the ammonium chloride of 4KG, the potassium chloride of 3KG, the potassium sulphate of 3KG, the orthoresol of 4KG, the ethanol potash of 4KG, the carbendazim of 1KG, the copper 8-quinolinolate of 0.4KG, the distilled water of 55KG, adds in the agitator respectively and stirs;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 20 minutes, and temperature is 75 ℃;
Step 4, cooling is filtered, and promptly makes a kind of organic and inorganic compounding agricultural chemicals.
Embodiment 7
Adopt the organic and inorganic compounding agricultural chemicals of embodiment 1-6 preparation to suppress the insect test respectively, survey it to pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hide from, the inhibiting rate of Americal rice leaf miner.
Get organic and inorganic compounding agricultural chemicals 100 grams of embodiment 1-6 preparation respectively, substep adds entry 300 grams, 500 grams; 1000 grams stir well with agitator, can evenly be sprayed onto melon, really, on the leaf, leguminous vegetables; Medication 10min, insect is slow in reacting, occurs curling and dead; Its curl with lethality with the increasing and rise of product design, it suppresses pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hides from, its efficient of Americal rice leaf miner is seen table 1.
Table 1 is to get the organic and inorganic compounding agricultural chemicals of embodiment 1-6 preparation respectively to insect inhibiting rate (slow in reacting+as to occur curling+lethality=inhibiting rate)
In the such scheme; Pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hide from, Americal rice leaf miner is melon, really, common insect on leaf, leguminous vegetables, traditional Chinese medicine, tealeaves, flowers, rape, cotton, tobacco and the crops; The hairworm area is wide, breeding is fast, harm is big, usually causes heavy losses such as fallen leaves, decayed fruit, the dead total crop failure of crops.Can find out by table 1, use organic and inorganic compounding agricultural chemicals of the present invention significantly to suppress damage by disease and insect, prevent the pollution of chemical pesticide environment; It has efficiently, safety, environmental protection, cost are low, effective; Technology of the present invention is simple, and is convenient and swift, greatly improved operating efficiency, and device therefor can be realized industrial applications for process equipment commonly used.
Medicine of the present invention is suitable for before plant disease be about to take place or uses 1-2 time when taking place, and a situation arises re-used best results 1-2 time in separated 5-9 days according to plant disease then.
More than show and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; The present invention is not restricted to the described embodiments; That describes in the foregoing description and the specification just explains principle of the present invention; The present invention also has various changes and modifications under the prerequisite that does not break away from spirit and scope of the invention, and these variations and improvement all fall in the scope of the invention that requires protection.The present invention requires protection domain to be defined by appending claims and equivalent thereof.
Claims (9)
1. organic and inorganic compounding agricultural chemicals is characterized in that: it comprises diammonium phosphate, ammonium chloride, sodium chloride, sodium sulphate, phenol, alkali, carbendazim, antibacterial mould inhibitor, all the other are distilled water.
2. a kind of organic and inorganic compounding agricultural chemicals according to claim 1 is characterized in that: count by weight: the antibacterial mould inhibitor of the alkali of the sodium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the sodium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are distilled water.
3. organic and inorganic compounding agricultural chemicals is characterized in that: it comprises diammonium phosphate, ammonium chloride, potassium chloride, potassium sulphate, phenol, alkali, carbendazim, antibacterial mould inhibitor, all the other are distilled water.
4. a kind of organic and inorganic compounding agricultural chemicals according to claim 3 is characterized in that: count by weight: the antibacterial mould inhibitor of the alkali of the potassium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the potassium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are distilled water.
5. according to claim 1 to 4 any described a kind of organic and an inorganic compounding agricultural chemicals, it is characterized in that: said phenol is a kind of in cresols, the orthoresol.
6. according to any described a kind of organic and inorganic compounding agricultural chemicals of claim 1 to 4, it is characterized in that: said alkali is organic base.
7. a kind of organic and inorganic compounding agricultural chemicals according to claim 6 is characterized in that: said organic base is a kind of in sodium methoxide, the potassium ethoxide.
8. according to claim 1 to 4 any described a kind of organic and an inorganic compounding agricultural chemicals, it is characterized in that: said antibacterial mould inhibitor is a kind of in benzimidazolyl-2 radicals-aminocarbamic acid methyl esters, the copper 8-quinolinolate.
9. method for preparing any said a kind of organic and an inorganic compounding agricultural chemicals of claim 1 to 4, it is characterized in that: the concrete grammar step is:
Step 1, each component add in the agitator respectively according to the parts by weight ratio and stir;
Step 2 after the stirring, places agitated reactor;
Step 3 stirs again, and the time is 10-30 minute, and temperature is 60-90 ℃;
Step 4, cooling is filtered.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103108122A CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103108122A CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
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| Publication Number | Publication Date |
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| CN102388920A true CN102388920A (en) | 2012-03-28 |
| CN102388920B CN102388920B (en) | 2013-12-25 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN2011103108122A Expired - Fee Related CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103444778A (en) * | 2012-05-30 | 2013-12-18 | 天津绿动植物营养技术开发有限公司 | Inorganic agricultural chemical and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063599A (en) * | 1992-03-16 | 1992-08-19 | 江苏省农业科学院 | A kind of compound disinfectant |
| CN1065772A (en) * | 1992-05-04 | 1992-11-04 | 江苏省农业科学院 | A kind of complex killing insect and germ agent |
-
2011
- 2011-10-14 CN CN2011103108122A patent/CN102388920B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063599A (en) * | 1992-03-16 | 1992-08-19 | 江苏省农业科学院 | A kind of compound disinfectant |
| CN1065772A (en) * | 1992-05-04 | 1992-11-04 | 江苏省农业科学院 | A kind of complex killing insect and germ agent |
Non-Patent Citations (3)
| Title |
|---|
| 《中国农资》 20060820 董奇伟等 杀菌杀虫复合型多功能烟剂__农用烟剂发展方向 , 第10期 * |
| 张丽萍等: "复合生物制剂防治苹果轮纹病", 《农药》 * |
| 董奇伟等: "杀菌杀虫复合型多功能烟剂――农用烟剂发展方向", 《中国农资》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103444778A (en) * | 2012-05-30 | 2013-12-18 | 天津绿动植物营养技术开发有限公司 | Inorganic agricultural chemical and preparation method thereof |
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| CN102388920B (en) | 2013-12-25 |
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