CN102388920B - Organic and inorganic composite pesticide and preparation method thereof - Google Patents
Organic and inorganic composite pesticide and preparation method thereof Download PDFInfo
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- CN102388920B CN102388920B CN2011103108122A CN201110310812A CN102388920B CN 102388920 B CN102388920 B CN 102388920B CN 2011103108122 A CN2011103108122 A CN 2011103108122A CN 201110310812 A CN201110310812 A CN 201110310812A CN 102388920 B CN102388920 B CN 102388920B
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses an organic and inorganic composite pesticide and a preparation method thereof. The preparation method comprises the following steps of: weighing the following components in parts by weight: 6-10 parts of diammonium phosphate, 3-5 parts of ammonium chloride, 2-4 parts of sodium chloride, 2-4 parts of sodium sulfate, 3-5 parts of phenol, 3-5 parts of alkali, 0.5-2 parts of carbendazim, 0.2-0.5 part of bacteriostatic mildewcide and the balance of distilled water; respectively adding the components into a stirrer and stirring, and then putting in a reaction kettle; stirring for 10-30 minutes at 60-90 DEG C; and cooling and filtering to finally obtain the organic and inorganic composite pesticide. The organic and inorganic composite pesticide has the advantage of good effect, and the preparation process is simple and can be put into industrial application.
Description
Technical field
The present invention relates to a kind of organic and inorganic composite pesticide, particularly relate to a kind of organic and inorganic composite pesticide and preparation method thereof.
Background technology
Organic agricultural chemicals is to take the class agricultural chemicals that the compounds such as organochlorine, organic phosphor, Organic fluoride, organic sulfur, organic copper are active ingredient.This class agricultural chemicals has insecticide, bactericide, miticide, weed killer herbicide, nematocide and rodenticide, such as chlorophos, parathion etc.To use maximum class agricultural chemicals.
Inorganic pesticide mainly contains calcium arsenate, lead arsenate, aluminum phosphate, lime sulfur mixture, copper sulphate, bordeaux mixture etc.This class action of agricultural chemicals is more single, and kind is few, and drug effect is low, and easily poisoning occurs, so current most kind is replaced by synthetic organic pesticide.
Summary of the invention
The defect existed in order to overcome above-mentioned prior art, the invention provides a kind of organic and inorganic composite pesticide, and the preparation method of this agricultural chemicals is provided simultaneously, and this agricultural chemicals is effective, and the preparation method is simple.
For achieving the above object, concrete scheme of the present invention is:
Scheme one: a kind of organic and inorganic composite pesticide comprises diammonium phosphate, ammonium chloride, sodium chloride, sodium sulphate, phenol, alkali, carbendazim, bacteria mildew-proof agent, all the other are distilled water; Count by weight: the bacteria mildew-proof agent of the alkali of the sodium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the sodium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are for distilled water.
Scheme two: a kind of organic and inorganic composite pesticide comprises diammonium phosphate, ammonium chloride, potassium chloride, potassium sulphate, phenol, alkali, carbendazim, bacteria mildew-proof agent, all the other are distilled water; Count by weight: the bacteria mildew-proof agent of the alkali of the potassium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the potassium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are for distilled water.
A kind ofly prepare organic and method inorganic composite pesticide, the method concrete steps are:
Step 1, each component adds in agitator and stirs respectively according to the parts by weight ratio;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 10-30 minute, temperature is 60-90 ℃;
Step 4, cooling, filter.
In the present invention, described phenol is a kind of in cresols, orthoresol.
In the present invention, described alkali is organic base; Described organic base is a kind of in sodium methoxide, potassium ethoxide.
In the present invention, described bacteria mildew-proof agent is a kind of in benzimidazolyl-2 radicals-aminocarbamic acid methyl esters, copper 8-quinolinolate.
The invention has the beneficial effects as follows: efficient, safety, environmental protection, cost are low, effective; Technique of the present invention is simple, convenient and swift, has greatly improved operating efficiency, and device therefor, for process equipment commonly used, can be realized industrial applications.
Embodiment:
Be easy to understand understanding in order to make technological means of the present invention, creation characteristic and to reach purpose, below in conjunction with specific embodiment, further set forth the present invention
Embodiment 1.
Step 1, distilled water by the benzimidazolyl-2 radicals of the carbendazim of the sodium methoxide of the cresols of the sodium sulphate of the sodium chloride of the ammonium chloride of the diammonium phosphate of 6KG, 3KG, 2KG, 2KG, 3KG, 3KG, 0.5KG, 0.2KG-aminocarbamic acid methyl esters, 50KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 10 minutes, temperature is 60 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 2.
Step 1, by the copper 8-quinolinolate of the carbendazim of the potassium ethoxide of the orthoresol of the sodium sulphate of the sodium chloride of the ammonium chloride of the diammonium phosphate of 10KG, 5KG, 4KG, 4KG, 5KG, 5KG, 2KG, 0.5KG, the distilled water of 60KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 30 minutes, temperature is 90 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 3.
Step 1, by the copper 8-quinolinolate of the carbendazim of the potassium ethoxide of the orthoresol of the sodium sulphate of the sodium chloride of the ammonium chloride of the diammonium phosphate of 8KG, 4KG, 3KG, 3KG, 4KG, 4KG, 1KG, 0.3KG, the distilled water of 55KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 20 minutes, temperature is 75 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 4.
Step 1, distilled water by the benzimidazolyl-2 radicals of the carbendazim of the sodium methoxide of the cresols of the potassium sulphate of the potassium chloride of the ammonium chloride of the diammonium phosphate of 6KG, 3KG, 2KG, 2KG, 3KG, 3KG, 0.5KG, 0.2KG-aminocarbamic acid methyl esters, 50KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 10 minutes, temperature is 60 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 5.
Step 1, by the copper 8-quinolinolate of the carbendazim of the potassium ethoxide of the orthoresol of the potassium sulphate of the potassium chloride of the ammonium chloride of the diammonium phosphate of 10KG, 5KG, 4KG, 4KG, 5KG, 5KG, 2KG, 0.5KG, the distilled water of 60KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 30 minutes, temperature is 90 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 6.
Step 1, by the copper 8-quinolinolate of the carbendazim of the ethanol potash of the orthoresol of the potassium sulphate of the potassium chloride of the ammonium chloride of the diammonium phosphate of 8KG, 4KG, 3KG, 3KG, 4KG, 4KG, 1KG, 0.4KG, the distilled water of 55KG, add in agitator and stir respectively;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 20 minutes, temperature is 75 ℃;
Step 4, cooling, filter, make a kind of organic and inorganic composite pesticide.
Embodiment 7
Adopt respectively organic and inorganic composite pesticide prepared by embodiment 1-6 to be suppressed the insect test, survey it to pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hide from, the inhibiting rate of Americal rice leaf miner.
Get respectively organic and inorganic composite pesticide 100 grams prepared by embodiment 1-6, substep adds water 300 grams, 500 grams, 1000 grams, stir well with agitator, can evenly be sprayed onto melon, really, on leaf, leguminous vegetables, medication 10min, insect is slow in reacting, occurs curling and dead, its curling and lethality increases and rises with product design, and it suppresses pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hides from, its efficiency of Americal rice leaf miner is in Table 1.
Table 1 for the organic and inorganic composite pesticide getting respectively embodiment 1-6 and prepare to insect inhibiting rate (slow in reacting+occur curling+lethality=inhibiting rate)
In such scheme, pickles pretty young woman, heart-eating worm, star caterpillar, scale insect, tortrix moth, cabbage caterpillar, wood louse, hide from, Americal rice leaf miner is melon, really, common insect on leaf, leguminous vegetables, traditional Chinese medicine, tealeaves, flowers, rape, cotton, tobacco and crops, the hairworm area is wide, breeding is fast, harm is large, usually causes the heavy losses such as fallen leaves, decayed fruit, the dead total crop failure of crops.As can be seen from Table 1, use organic and inorganic composite pesticide of the present invention significantly to suppress damage by disease and insect, prevent the pollution of chemical pesticide to environment; It has efficiently, safety, environmental protection, cost are low, effective; Technique of the present invention is simple, convenient and swift, has greatly improved operating efficiency, and device therefor, for process equipment commonly used, can be realized industrial applications.
Medicine of the present invention is suitable for before plant disease be about to occur or uses 1-2 time while occurring, and then according to plant disease, a situation arises every 5-9 days, re-uses 1-2 time, best results.
Above demonstration and described basic principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; that in above-described embodiment and specification, describes just illustrates principle of the present invention; the present invention also has various changes and modifications without departing from the spirit and scope of the present invention, and these changes and improvements all fall in the claimed scope of the invention.The claimed scope of the present invention is defined by appending claims and equivalent thereof.
Claims (2)
1. an organic and inorganic composite pesticide is characterized in that: it comprises diammonium phosphate, ammonium chloride, sodium chloride, sodium sulphate, phenol, alkali, carbendazim, bacteria mildew-proof agent, all the other are distilled water; Described organic and inorganic composite pesticide, count by weight: the bacteria mildew-proof agent of the alkali of the sodium sulphate of the ammonium chloride of the diammonium phosphate of 6-10 part, 3-5 part, the sodium chloride of 2-4 part, 2-4 part, the phenol of 3-5 part, 3-5 part, the carbendazim of 0.5-2 part, 0.2-0.5 part, all the other are for distilled water; Described phenol is a kind of in cresols, orthoresol; Described alkali is that organic base is a kind of in sodium methoxide, potassium ethoxide; Described bacteria mildew-proof agent is a kind of in benzimidazolyl-2 radicals-aminocarbamic acid methyl esters, copper 8-quinolinolate.
2. a method for preparing described a kind of organic and inorganic composite pesticide of claim 1, it is characterized in that: the concrete grammar step is:
Step 1, each component adds in agitator and stirs respectively according to the parts by weight ratio;
Step 2, after stirring, be placed in reactor;
Step 3, then stir, the time is 10-30 minute, temperature is 60-90 ℃;
Step 4, cooling, filter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103108122A CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011103108122A CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
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| Publication Number | Publication Date |
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| CN102388920A CN102388920A (en) | 2012-03-28 |
| CN102388920B true CN102388920B (en) | 2013-12-25 |
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| CN2011103108122A Expired - Fee Related CN102388920B (en) | 2011-10-14 | 2011-10-14 | Organic and inorganic composite pesticide and preparation method thereof |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN103444778A (en) * | 2012-05-30 | 2013-12-18 | 天津绿动植物营养技术开发有限公司 | Inorganic agricultural chemical and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063599A (en) * | 1992-03-16 | 1992-08-19 | 江苏省农业科学院 | A kind of compound disinfectant |
| CN1065772A (en) * | 1992-05-04 | 1992-11-04 | 江苏省农业科学院 | A kind of complex killing insect and germ agent |
-
2011
- 2011-10-14 CN CN2011103108122A patent/CN102388920B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1063599A (en) * | 1992-03-16 | 1992-08-19 | 江苏省农业科学院 | A kind of compound disinfectant |
| CN1065772A (en) * | 1992-05-04 | 1992-11-04 | 江苏省农业科学院 | A kind of complex killing insect and germ agent |
Non-Patent Citations (4)
| Title |
|---|
| 复合生物制剂防治苹果轮纹病;张丽萍等;《农药》;20060325(第03期);201-203页 * |
| 张丽萍等.复合生物制剂防治苹果轮纹病.《农药》.2006,(第03期), |
| 杀菌杀虫复合型多功能烟剂――农用烟剂发展方向;董奇伟等;《中国农资》;20060820(第10期);36-37页 * |
| 董奇伟等.杀菌杀虫复合型多功能烟剂――农用烟剂发展方向.《中国农资》.2006,(第10期), |
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| CN102388920A (en) | 2012-03-28 |
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