CN102376534A - Manufacturing method of standard sheet for silicon epitaxial film thickness test - Google Patents

Manufacturing method of standard sheet for silicon epitaxial film thickness test Download PDF

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Publication number
CN102376534A
CN102376534A CN2010102653146A CN201010265314A CN102376534A CN 102376534 A CN102376534 A CN 102376534A CN 2010102653146 A CN2010102653146 A CN 2010102653146A CN 201010265314 A CN201010265314 A CN 201010265314A CN 102376534 A CN102376534 A CN 102376534A
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silicon
deielectric
coating
thickness
manufacture method
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刘继全
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Shanghai Huahong Grace Semiconductor Manufacturing Corp
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Shanghai Hua Hong NEC Electronics Co Ltd
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Abstract

The invention discloses a manufacturing method of a standard sheet for a silicon epitaxial film thickness test, which comprises the following steps of: (1) depositing a layer of dielectric film on a silicon substrate; (2) patterning and etching the dielectric film so as to form a pattern formed by the dielectric film on the silicon substrate; (3) selectively growing a silicon epitaxial layer on the silicon substrate; (4) removing the dielectric film; and (5) measuring the depth of a groove formed by the silicon epitaxial layer after the dielectric film is removed, wherein the depth is used as a standard thickness of an adjacent silicon epitaxial layer. Through the invention, the silicon epitaxial measurement accuracy can be improved.

Description

The manufacture method of silicon epitaxy thickness testing standard sheet
Technical field
The present invention relates to the semiconductor integrated circuit field, particularly relate to a kind of manufacture method of silicon epitaxy thickness testing standard sheet.
Background technology
Silicon epitaxy thickness method of testing mainly adopts fourier infrared (FTIR) method of testing; The method is that the doping content according to silicon epitaxy layer and substrate layer has evident difference to demarcate the thickness of epitaxial loayer (substrate generally has high doping content, for example highly doped P type or N type substrate).But (generally being higher than 1000 ℃) carried out in epitaxial growth under hot conditions; The dopant of substrate can spread in epitaxial loayer in epitaxial process; Thereby cause moving on the interface of substrate and epitaxial loayer and thickening; The degree of moving on the different epitaxial growth condition interfaces is different, causes existing than mistake with the result that preceding method is measured, so need calibration with preceding method.
Summary of the invention
The technical problem that the present invention will solve provides a kind of manufacture method of silicon epitaxy thickness testing standard sheet, improves silicon epitaxy and measures accuracy.
For solving the problems of the technologies described above, the manufacture method of silicon epitaxy thickness testing standard sheet of the present invention comprises the steps:
Step 1, the layer dielectric of on silicon base, growing;
Step 2, carry out graphical and etching, on silicon base, form the figure that constitutes by said deielectric-coating said deielectric-coating;
Step 3, on said silicon base the selective growth silicon epitaxy layer;
Step 4, remove said deielectric-coating;
Step 5, measure to remove behind the deielectric-coating the degree of depth, with the standard thickness of this degree of depth as the adjacent silicon epitaxial loayer by the formed groove of said silicon epitaxy layer.
Because silicon epitaxy layer and deielectric-coating all grow on silicon base, the bottom of formed groove was the interface of silicon base after deielectric-coating was removed, and the degree of depth of groove is the thickness of epitaxial loayer.Therefore method of the present invention can obtain accurately to demarcate the silicon epitaxy standard film of epitaxy layer thickness, effectively solves silicon epitaxy thickness measurement problem.
Description of drawings
Below in conjunction with accompanying drawing and embodiment the present invention is done further detailed explanation:
Fig. 1-the 6th, method one embodiment process flow diagram of the present invention;
Fig. 7 is method one an embodiment control flow chart of the present invention.
Embodiment
Referring to shown in Figure 7, in one embodiment, the manufacture method of said silicon epitaxy thickness testing standard sheet comprises the steps:
Step 1, combine shown in Figure 1, growth one layer dielectric 2 on silicon base 1.Said silicon base 1 is P+ silicon base or N+ silicon base, for example adopts P type heavy doping silicon chip (resistivity<0.01ohm.cm).The dielectric film 2 is a silicon oxide film having a thickness of
Figure BSA00000246998400021
Of course, the medium may be a silicon oxide film 2 other than the dielectric film, such as silicon nitride or silicon oxynitride; wherein the thickness of the dielectric film 2 is not limited to Yu
Figure BSA00000246998400022
For example in the 500 -
Step 2, combine Fig. 2, shown in 3, said deielectric-coating 2 carried out graphical and etching, on silicon base 1, form the ring-shaped figure that constitutes by said deielectric-coating 2.Fig. 2 is the sectional drawing of formed figure after deielectric-coating is etched, and Fig. 3 is the vertical view of formed figure after deielectric-coating is etched.The deielectric-coating 2 that behind over etching, circularizes is concentric with silicon base 1, and the width of annular is 10-100 μ m; The deielectric-coating of annular can be a ring or equally spaced a plurality of ring.
Step 3, combine shown in Figure 4, selective growth silicon epitaxy layer 3 on said silicon base 1.Be that silicon epitaxy layer 3 is only grown on silicon base, on silicon oxide film, do not grow.The thickness of silicon epitaxy layer 3 is about
Figure BSA00000246998400031
.The thickness of silicon epitaxy layer 3 is less than the thickness of deielectric-coating 2 in this step.
Step 4, combine Fig. 5, shown in 6, remove the deielectric-coating 2 on the said silicon base 1, groove 4 appearance that formed by silicon epitaxy layer 3 are just arranged on said silicon base 1 like this.Said deielectric-coating 2 can adopt wet method or dry etching to remove.Fig. 5 is the sectional drawing of the formed figure after deielectric-coating 2 is removed, and Fig. 6 is the vertical view that deielectric-coating is removed the formed figure in back.
Step 5, measure the degree of depth that deielectric-coating 2 is removed the formed groove 4 in back with the scan-probe method.Because groove 4 bottoms are the interface of silicon base 1, so the degree of depth of groove 4 is the thickness of silicon epitaxy layer 3.The degree of depth of the groove of measuring with the scan-probe method 4 can be used as the standard thickness (standard thickness of adjacent position silicon epitaxy layer 3) of this epitaxial wafer, can demarcate the FTIR assay method with this epitaxial wafer.
More than through embodiment the present invention has been carried out detailed explanation, but these are not to be construed as limiting the invention.Under the situation that does not break away from the principle of the invention, those skilled in the art also can make many distortion and improvement, and these also should be regarded as protection scope of the present invention.

Claims (6)

1. the manufacture method of a silicon epitaxy thickness standard film is characterized in that, comprises the steps:
Step 1, on silicon base deposit one layer dielectric;
Step 2, carry out graphical and etching, on silicon base, form the figure that constitutes by said deielectric-coating said deielectric-coating;
Step 3, on said silicon base the selective growth silicon epitaxy layer;
Step 4, remove said deielectric-coating;
The degree of depth of the groove that is formed by said silicon epitaxy layer behind step 5, the mensuration removal deielectric-coating is with the standard thickness of this degree of depth as the adjacent silicon epitaxial loayer.
2. manufacture method as claimed in claim 1 is characterized in that: the resistivity of silicon base is less than or equal to 0.05ohm.cm.
3. manufacture method as claimed in claim 1; It is characterized in that: deielectric-coating described in the step 1 is at least a in silica, silicon nitride or the silicon oxynitride, and thickness is 500-
Figure FSA00000246998300011
4. manufacture method as claimed in claim 1 is characterized in that: the figure described in the step 2 is annular and concentric with said silicon base, and annular width is 1-100 μ m; Said figure is a ring or equally spaced a plurality of ring.
5. manufacture method as claimed in claim 1 is characterized in that: selective growth described in the step 3, and grown silicon epitaxial loayer on said silicon base only, grown silicon epitaxial loayer not on said deielectric-coating, and the thickness of silicon epitaxy layer is less than the thickness of deielectric-coating.
6. manufacture method as claimed in claim 1 is characterized in that: the mensuration in the step 5 adopts the scan-probe method to measure the degree of depth of groove.
CN2010102653146A 2010-08-26 2010-08-26 Manufacturing method of standard sheet for silicon epitaxial film thickness test Pending CN102376534A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103412272A (en) * 2013-06-17 2013-11-27 上海晶盟硅材料有限公司 Standard sheet for calibrating mercury-probe resistivity measuring instrument and mercury-probe resistivity measuring instrument calibration method
WO2014180132A1 (en) * 2013-05-10 2014-11-13 京东方科技集团股份有限公司 Film thickness testing method and device
CN115727774A (en) * 2022-12-02 2023-03-03 河北普兴电子科技股份有限公司 Calibration method for measuring thickness of epitaxial layer by infrared spectrometer and calibration sheet

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02105438A (en) * 1988-10-13 1990-04-18 Nec Corp Measurement of film thickness of epitaxial growth layer
KR20080048703A (en) * 2006-11-29 2008-06-03 동부일렉트로닉스 주식회사 Measurement method of a thickness in an epitaxial process using a surface step

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH02105438A (en) * 1988-10-13 1990-04-18 Nec Corp Measurement of film thickness of epitaxial growth layer
KR20080048703A (en) * 2006-11-29 2008-06-03 동부일렉트로닉스 주식회사 Measurement method of a thickness in an epitaxial process using a surface step

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014180132A1 (en) * 2013-05-10 2014-11-13 京东方科技集团股份有限公司 Film thickness testing method and device
CN103412272A (en) * 2013-06-17 2013-11-27 上海晶盟硅材料有限公司 Standard sheet for calibrating mercury-probe resistivity measuring instrument and mercury-probe resistivity measuring instrument calibration method
CN115727774A (en) * 2022-12-02 2023-03-03 河北普兴电子科技股份有限公司 Calibration method for measuring thickness of epitaxial layer by infrared spectrometer and calibration sheet

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