CN102373628A - Environment-friendly coloring agent composition and production method thereof - Google Patents
Environment-friendly coloring agent composition and production method thereof Download PDFInfo
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- CN102373628A CN102373628A CN2010102623776A CN201010262377A CN102373628A CN 102373628 A CN102373628 A CN 102373628A CN 2010102623776 A CN2010102623776 A CN 2010102623776A CN 201010262377 A CN201010262377 A CN 201010262377A CN 102373628 A CN102373628 A CN 102373628A
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Abstract
The invention provides an environment-friendly coloring agent composition and a production method thereof. The environment-friendly coloring agent composition is prepared from various dyeing raw materials, aids, a leveling agent and a penetrating agent, wherein the dyeing raw materials are commercial raw materials; and the penetrating agent is fatty alcohol polyoxypropylene ether or cis-glutaconic acid, di-secondary octyl ester potassium sulfonate, belongs to a non-ionic surfactant, has a strong penetrating effect, also has fixed hydrophilic and oleophilic groups, can be directionally arranged on the surface of a solution, and can obviously reduce surface tension.
Description
Technical field
The present invention relates to the textile dyeing technical field, relate in particular to a kind of environmental protection coloring composition and production method.
Background technology
Affinity between the color of dyestuff and it and tissue is by the molecular structure decision of dyestuff itself, colorific chromophoric group and and tissue between the auxochrome group of generation affinity determined the dyeing property of coloring agent jointly.As dye substance, except chromophoric group is arranged, also need a kind of auxochrome group that makes compound generation ionization.As in the dye composition often by nitro (NO2), azo group (N=N-), vinyl etc. formed chromophoric group, and by-OH ,-SO3H ,-acidic-group such as COOH and-NH2 ,-NHCH3 ,-basic groups such as N (CH3) 2 have constituted auxochrome group.Their existence makes the dye substance ionization, and polarity strengthens, and promotes to have an effect between dyestuff and tissue, produces Color.We call acidity or basic stain to the dyestuff that has acidity or basic group in the auxochrome group respectively.
Dyeing is the important steps of printing and dyeing in the production process, can use ACID DYES to dye usually, and the height of dye level is directly restricting the quality of fabric quality.Also there are many technical problems that are worth solution at present in the prior art.
Summary of the invention
The objective of the invention is to provides a kind of good stability to the problems referred to above, and firm environmental protection coloring composition and production method dye.
Technical scheme of the present invention is following: a kind of environmental protection coloring composition, form by weight percentage by following prescription:
Dyeing raw material 25~35%
Levelling agent 15~35%
Bleeding agent 5~10%
Auxiliary agent 3~10%
Water surplus %.
As a kind of optimal way of coloring composition according to the invention, said auxiliary agent is an acetic acid, and said levelling agent is prepared by weight percentage and comprised: lignosulfonates 25-35%, carboxymethyl cellulose 5-8%, and urea 6-8%, surplus is a water.
As a kind of optimal way of coloring composition according to the invention, said bleeding agent is the mixture of fatty alcohol polyoxypropylene ether and suitable glutaconate di-sec-octyl potassium sulfonate, and ratio between two is 1: 1~4.
As a kind of optimal way of coloring composition according to the invention, comprise the steps: steps A, normal temperature and pressure preparation dyeing raw material and levelling agent down; Step B, in having the agitated reactor of agitator, add entry; Add auxiliary agent, bleeding agent and levelling agent after water temperature is controlled at 50-70 ℃; Stir operation and add said dyeing raw material after 15~30 minutes, turning round began to be warming up to 100 ℃ after 1~2 hour, reacted and filtered discharging after 2~3 hours.
Fabric provided by the present invention is used coloring agent, adopts multiple dyeing raw material, auxiliary agent, levelling agent and bleeding agent formulated in combination to form, and the raw material that wherein dyes is commercially available raw material; Bleeding agent is fatty alcohol polyoxypropylene ether or suitable glutaconate di-sec-octyl potassium sulfonate; Belong to non-ionic surface active agent, have stronger osmosis, also have fixing hydrophilic and oleophilic group; Surface energy at solution aligns, and the material that surface tension is significantly descended.The composition of these components has good result, the quality of lining can significantly be provided the dyeing of cotton textiles, BLENDED FABRIC, polyester-cotton fabric.
The specific embodiment
Embodiment 1
1, takes by weighing 1 part of acid violet, 2 parts of acid reds, 2 parts of allotments of Indian yellow and form the dyeing raw material; Get 0.1 part of di-2-ethylhexylphosphine oxide naphthalene sulfonate, 0.5 part of lignosulfonates, 0.1 part of carboxymethyl cellulose, 0.15 part in urea, 7 parts in water, it is subsequent use to make levelling agent under the normal temperature and pressure;
2, take by weighing 2 parts of dyeing raw materials, 0.1 part of acetic acid, 0.2 part of levelling agent, 1 part of fatty alcohol polyoxypropylene ether, 6.5 parts in water;
3, in having the agitated reactor of agitator, add 6.5 parts of water; And add 0.2 part of 0.1 part of acetic acid, 1 part of fatty alcohol polyoxypropylene ether and levelling agent after making water temperature rise to 60 ℃; Stir operation and add 2 parts of dyeing raw materials after 15 minutes; Turning round begins after 30 minutes to heat up, and in 50 minutes, begins to be warming up to 90 ℃, be incubated filtration discharging in 2 hours and promptly gets fabric and use coloring agent.
Embodiment 2:
1, with embodiment 1;
2, take by weighing 3 parts of dyeing raw materials, 0.5 part in sulfuric acid, 0.5 part of levelling agent is along 1.8 parts of glutaconate di-sec-octyl potassium sulfonates, 7 parts in water;
3, in having the agitated reactor of agitator, add 7 parts of water; And add 0.51 part in sulfuric acid after making water temperature rise to 55 ℃, along 0.5 part of 1.8 parts of glutaconate di-sec-octyl potassium sulfonates and levelling agent; Stir operation and add 3 parts of dyeing raw materials after 20 minutes; Turning round begins after 35 minutes to heat up, and in 60 minutes, begins to be warming up to 95 ℃, is incubated discharging in 3 hours and promptly gets fabric and use coloring agent.
What should explain is; Above embodiment is only unrestricted in order to technical scheme of the present invention to be described; Although with reference to preferred embodiment the present invention is specified, those of ordinary skill in the art should be appreciated that and can make amendment or be equal to replacement technical scheme of the present invention; And not breaking away from the spirit and the scope of technical scheme of the present invention, it all should be encompassed in the middle of the claim scope of the present invention.
Claims (4)
1. environmental protection coloring composition is characterized in that: be made up of by weight percentage following prescription:
Dyeing raw material 25~35%
Levelling agent 15~35%
Bleeding agent 5~10%
Auxiliary agent 3~10%
Water surplus %.
2. according to the said coloring composition of claim 1, it is characterized in that: said auxiliary agent is an acetic acid, and said levelling agent is prepared by weight percentage and comprised: lignosulfonates 25-35%, carboxymethyl cellulose 5-8%, and urea 6-8%, surplus is a water.
3. according to the said coloring composition of claim 1, it is characterized in that: said bleeding agent is the mixture of fatty alcohol polyoxypropylene ether and suitable glutaconate di-sec-octyl potassium sulfonate, and ratio between two is 1: 1~4.
4. according to the said coloring composition production method of claim 1, it is characterized in that: comprise the steps: steps A, normal temperature and pressure preparation dyeing raw material and levelling agent down; Step B, in having the agitated reactor of agitator, add entry; Add auxiliary agent, bleeding agent and levelling agent after water temperature is controlled at 50-70 ℃; Stir operation and add said dyeing raw material after 15~30 minutes, turning round began to be warming up to 100 ℃ after 1~2 hour, reacted and filtered discharging after 2~3 hours.
Priority Applications (1)
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CN2010102623776A CN102373628A (en) | 2010-08-24 | 2010-08-24 | Environment-friendly coloring agent composition and production method thereof |
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CN2010102623776A CN102373628A (en) | 2010-08-24 | 2010-08-24 | Environment-friendly coloring agent composition and production method thereof |
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CN102373628A true CN102373628A (en) | 2012-03-14 |
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CN2010102623776A Pending CN102373628A (en) | 2010-08-24 | 2010-08-24 | Environment-friendly coloring agent composition and production method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104532617A (en) * | 2014-12-24 | 2015-04-22 | 常熟市淼泉盛达助剂厂 | Leveling agent for fabrics |
CN113328204A (en) * | 2021-04-20 | 2021-08-31 | 惠州锂威电子科技有限公司 | Lithium ion battery isolating membrane and preparation method thereof |
-
2010
- 2010-08-24 CN CN2010102623776A patent/CN102373628A/en active Pending
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104532617A (en) * | 2014-12-24 | 2015-04-22 | 常熟市淼泉盛达助剂厂 | Leveling agent for fabrics |
CN113328204A (en) * | 2021-04-20 | 2021-08-31 | 惠州锂威电子科技有限公司 | Lithium ion battery isolating membrane and preparation method thereof |
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Application publication date: 20120314 |