CN102345247A - Application method of flame retardant paint, as well as flame-retardant cigarette tipping paper and cigarette - Google Patents
Application method of flame retardant paint, as well as flame-retardant cigarette tipping paper and cigarette Download PDFInfo
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- CN102345247A CN102345247A CN2011102222243A CN201110222224A CN102345247A CN 102345247 A CN102345247 A CN 102345247A CN 2011102222243 A CN2011102222243 A CN 2011102222243A CN 201110222224 A CN201110222224 A CN 201110222224A CN 102345247 A CN102345247 A CN 102345247A
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Abstract
The invention relates to an application method of flame retardant paint, as well as flame-retardant cigarette tipping paper and a cigarette. The flame retardant paint is coated on the surface of the inner side of the cigarette tipping paper in contact with a filter rod, and the flame retardant paint cosists of the following ingredients by mass percent: 10 to 25 percent of flame retardant, 70 to 85 percent of auxiliaries and 1 to 5 percent of thickening agents, wherein the flame retardant comprises one or several kinds of materials in ammonium dihydrogen phosphate, diammonium phosphate, ammonium phosphate, monosodium orthophosphate, disodium hydrogen phosphate and water-soluble ammonium polyphosphate. All raw materials of the flame retardant paint belong to food additive type materials and are innoxious and harmless, the manufacture process is simple, the coiled cigarette has no peculiar smell, the smoking quality of the original cigarette can be maintained, when the unquenched cigarette is flamed to a position with the tipping paper, the stub can be automatically and completely extinguished in 1 to 2 min, and the self extinguishing rate is 100 percent, so fire hazards caused by the unquenched stub can be effectively prevented and reduced.
Description
Technical field
The present invention relates to technical field of cigarettes, is a kind of application process of BACN coating specifically, and cigarette tipping paper that obtains and the fire-retardant cigarette of stub.
Background technology
China is maximum in the world cigarette producing country, also is maximum in the world tobacco consumption state.Along with the tobacco development of science and technology, " smoking is with healthy ", " smoking and safety " become the main flow trend of tobacco business development gradually.This mainly considers from two aspects: the one, and cigarette props up infringement and the pollution of the flue gas of burning generation to human body and surrounding environment generation, and two are meant the fire that is caused by smoking.
The lighted cigarette butt surface temperature is 200 ℃～300 ℃, and central temperature is 700 ℃～800 ℃, apparently higher than the burning-point of other combustible materials.Like paper is 130 ℃, and cotton-wadded quilt, numb suede are 150 degree, and pine is 250 ℃.It is 4～15 minutes that the Linear Leaf Speedwell cigarette prolongs the burning time, inhales surplus cigarette end and generally can continue firing 1～4 minute, and in this time, many inflammability article all can be lighted.Sometimes cigarette end is thrown away in cotton-wadded quilt, wood shavings, wood chip or thick grass, and the dozens of minutes of glowing is not easy to be noted by the people that danger is bigger.
According to statistics, what smoking caused in the Japanese family fire accounts for 26%, and what smoking caused in the American family fire accounts for 29.1%.These countries are annual all to have many people because carelessness is died from smoking or thrown out without care in the fire that cigarette end causes.The fire that cigarette end causes in some cities of China accounts for 1/7th of fire sum, causes the news report of personnel and property loss to happen occasionally by house or the forest fire of throwing out the cigarette end initiation without care.
How to reduce the risk of inhaling surplus cigarette end initiation fire to greatest extent, reduce personnel and property loss that fire causes, designing and produce a kind of cigarette that the surplus cigarette end of suction is in time extinguished automatically is starting point of the present invention.
Summary of the invention
The application process that the purpose of this invention is to provide a kind of novel environment friendly retardants coatings; And the cigarette tipping paper that obtains and with the cigarette that it rolls, possess the end extinguishing function; Promptly when such cigarette was burned to the position of tipping paper, stub can all extinguish voluntarily.
A kind of application process of retardants coatings; With described retardants coatings be coated on be used on the cigarette tipping paper fire-retardant; Described retardants coatings is made up of following mass percent component: 10-25% fire retardant, 70-85% auxiliary agent and 1-5% thickener are formed, and described fire retardant comprises one or more in ammonium dihydrogen phosphate (ADP), diammonium hydrogen phosphate, ammonium phosphate, sodium dihydrogen phosphate, sodium hydrogen phosphate, the water-soluble poly ammonium phosphate.
Described auxiliary agent comprises the phosphoric acid,diluted aqueous solution of water or 1-5%, and described thickener comprises one or more in hydroxypropyl methylcellulose, starch phosphate sodium, sodium alginate, xanthans, chitin, tamarind seed polysaccharide glue, the titanium dioxide.
Described retardants coatings is coated on the face that cigarette tipping paper is inboard with filter rod contacts.Can be coated with into a fire-retardant endless belt, join with the junction of filter rod and pipe tobacco.Described fire-retardant endless belt width is the 5-6 millimeter.
A kind of fire-retardant cigarette tipping paper; Retardants coatings is coated on the face that cigarette tipping paper is inboard with filter rod contacts obtains; Described retardants coatings is made up of following mass percent component: 10-25% fire retardant, 70-85% auxiliary agent and 1-5% thickener are formed, and described fire retardant comprises one or more in ammonium dihydrogen phosphate (ADP), diammonium hydrogen phosphate, ammonium phosphate, sodium dihydrogen phosphate, sodium hydrogen phosphate, the water-soluble poly ammonium phosphate.Described auxiliary agent comprises the phosphoric acid,diluted aqueous solution of water or 1-5%, and described thickener comprises one or more in hydroxypropyl methylcellulose, starch phosphate sodium, sodium alginate, xanthans, chitin, tamarind seed polysaccharide glue, the titanium dioxide.
Described retardants coatings can be coated with into a fire-retardant endless belt, joins with the junction of filter rod and pipe tobacco.Described fire-retardant endless belt width is the 5-6 millimeter.
The fire-retardant cigarette of a kind of stub is the cigarette that is prepared from above-mentioned fire-retardant cigarette tipping paper.
Retardants coatings mainly is made up of one or more inorganic raw material fire retardants and proper assistant and thickener, and all raw material all belongs to the food additives class, nontoxic free from extraneous odour, safety and environmental protection.
Fire retardant mainly is made up of one or more inorganic raw materials in ammonium dihydrogen phosphate (ADP), diammonium hydrogen phosphate, ammonium phosphate, sodium dihydrogen phosphate, sodium hydrogen phosphate, the water-soluble poly ammonium phosphate etc.; Easy or more soluble in water; The no solid residue of aqueous solution clarification, its weight percentage accounts for 10～30% of whole retardants coatings.
The retardants coatings auxiliary agent mainly is the phosphoric acid,diluted aqueous solution of water or 1-5%, and its weight percentage accounts for 65～85% of whole retardants coatings.
The retardants coatings thickener mainly is to be made up of one or more raw materials such as hydroxypropyl methylcellulose, starch phosphate sodium, sodium alginate, xanthans, chitin, tamarind seed polysaccharide glue; Fully dissolving in the water or the phosphoric acid,diluted aqueous solution, the no solid residue of aqueous solution clarification.Its weight percentage accounts for 1～5% of whole retardants coatings.
The retardants coatings performance can keep stable in a long time like color, smell, Acidity of Aikalinity, viscosity etc.
The novel flame-retardant cigarette tipping paper rolls cigarette when propping up at last machine, and it rolls speed, cigarette quality etc. and the basic indifference of regular-size cigarette tipping paper.
The cigarette that the novel flame-retardant cigarette tipping paper is rolled can keep original suction quality of cigarette and taste, the basic no change of smoke chemistry index.
The cigarette that the novel flame-retardant cigarette tipping paper is rolled is when being burned to the position of tipping paper, and stub can all extinguish voluntarily in 1-2 minute, and the rate of putting out certainly is 100%.
Compared with the prior art the present invention has remarkable advantage:
A. the used retardants coatings safety and environmental protection of the present invention meets the requirement of food additives fully;
B. retardants coatings can be coated at present on commercially available any regular-size cigarette tipping paper and forms the novel flame-retardant cigarette tipping paper, and preparation technology is simple, need not do any change to cigarette machine;
C. the cigarette that is rolled by the novel flame-retardant cigarette tipping paper can keep original suction quality of cigarette and taste, the basic no change of smoke chemistry index;
D. the cigarette that rolled of novel flame-retardant cigarette tipping paper is when being burned to the position of tipping paper, and stub can all extinguish voluntarily in 1-2 minute, and the rate of putting out certainly is 100%.
Description of drawings
Fig. 1 is a cigarette structural representation of the present invention
1-cigarette tipping paper among the figure, 2-filter rod, the fire-retardant endless belt of 3-fire retardant coating, 4-pipe tobacco, 5-cigarette paper.
The specific embodiment
Adopt cigarette that above technology rolls when being burned to the position of tipping paper, stub can all extinguish voluntarily in 1-2 minute, and the rate of putting out certainly is 100%, therefore can effectively prevent and reduce because of not extinguishing the caused fire of stub.Combine case study on implementation to further specify at present, and can not form restriction the present invention:
The preparation of retardants coatings and novel flame-retardant cigarette tipping paper:
In 10 kg water, slowly add 200 gram hydroxypropyl methylcelluloses, be dissolved to clear solution, add 2500 gram ammonium dihydrogen phosphate (ADP)s again, be stirred to dissolving fully while stirring, retardants coatings; Be injected into then in cigarette tipping paper printing (gravure) the machine China ink groove, the inhibiting tape of coating one deck certain width at the regular-size cigarette tipping paper back side, the tipping paper after the coating is through drying, cutting into dish, and cigarette becomes cigarette to prop up on cigarette machine again.
Adopt above-mentioned novel flame-retardant cigarette tipping paper and common tipping paper, identical pipe tobacco and other auxiliary material respectively, become two kinds of cigarette samples by conventional production method cigarette.By specialty teacher of the smokeing panel test two kinds of cigarette sample qualities (fragrance, harmony, assorted gas, excitant, pleasant impression etc.) are estimated.By standard method two kinds of cigarette sample main flume conventional chemical indexs are carried out analyzing and testing simultaneously.
The cigarette sample quality evaluation is the result show, the cigarette that is rolled by novel flame-retardant cigarette tipping paper of the present invention can keep original suction quality of cigarette and taste.
Cigarette sample main flume conventional chemical index analysis testing result shows both basic indifferences.
The end extinguishing test:
E. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back horizontal positioned, and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 1.
F. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back and vertically place (combustion head-up), and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 1.
Table 1
| Light number | From putting out number | From putting out rate | |
| The regular-size cigarette tipping paper | 40 | 4 | 10％ |
| Novel flame-retardant cigarette tipping paper of the present invention | 40 | 40 | 100％ |
The preparation of retardants coatings and novel flame-retardant cigarette tipping paper:
In 10 kg water, slowly add 200 gram xanthans, be dissolved to clear solution, add 2000 gram ammonium dihydrogen phosphate (ADP)s and 1000 gram diammonium hydrogen phosphates again, be stirred to dissolving fully while stirring, retardants coatings; Be injected into then in cigarette tipping paper printing (gravure) the machine China ink groove, the inhibiting tape of coating one deck certain width at the regular-size cigarette tipping paper back side, the tipping paper after the coating is through drying, cutting into dish, and cigarette becomes cigarette to prop up on cigarette machine again.
Adopt above-mentioned novel flame-retardant cigarette tipping paper and common tipping paper, identical pipe tobacco and other auxiliary material respectively, become two kinds of cigarette samples by conventional production method cigarette.By specialty teacher of the smokeing panel test two kinds of cigarette sample qualities (fragrance, harmony, assorted gas, excitant, pleasant impression etc.) are estimated.By standard method two kinds of cigarette sample main flume conventional chemical indexs are carried out analyzing and testing simultaneously.
The cigarette sample quality evaluation is the result show, the cigarette that is rolled by novel flame-retardant cigarette tipping paper of the present invention can keep original suction quality of cigarette and taste.
Cigarette sample main flume conventional chemical index analysis testing result shows both basic indifferences.
The end extinguishing test:
G. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back horizontal positioned, and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 2.
H. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back and vertically place (combustion head-up), and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 2.
Table 2
The preparation of retardants coatings and novel flame-retardant cigarette tipping paper:
In 10 kg water, slowly add 150 Crow shop sign in the form of a streamer polysaccharide glue, be dissolved to clear solution, add 1000 gram ammonium dihydrogen phosphate (ADP)s, 1000 gram diammonium hydrogen phosphates and 1000 gram ammonium phosphate more respectively, be stirred to dissolving fully while stirring, retardants coatings; Be injected into then in cigarette tipping paper printing (gravure) the machine China ink groove, the inhibiting tape of coating one deck certain width at the regular-size cigarette tipping paper back side, the tipping paper after the coating is through drying, cutting into dish, and cigarette becomes cigarette to prop up on cigarette machine again.
Adopt above-mentioned novel flame-retardant cigarette tipping paper and common tipping paper, identical pipe tobacco and other auxiliary material respectively, become two kinds of cigarette samples by conventional production method cigarette.By specialty teacher of the smokeing panel test two kinds of cigarette sample qualities (fragrance, harmony, assorted gas, excitant, pleasant impression etc.) are estimated.By standard method two kinds of cigarette sample main flume conventional chemical indexs are carried out analyzing and testing simultaneously.
The cigarette sample quality evaluation is the result show, the cigarette that is rolled by novel flame-retardant cigarette tipping paper of the present invention can keep original suction quality of cigarette and taste.
Cigarette sample main flume conventional chemical index analysis testing result shows both basic indifferences.
The end extinguishing test:
I. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back horizontal positioned, and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 3.
J. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back and vertically place (combustion head-up), and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 3.
Table 3
| Light number | From putting out number | From putting out rate | |
| The regular-size cigarette tipping paper | 40 | 1 | 2.5％ |
| Novel flame-retardant cigarette tipping paper of the present invention | 40 | 40 | 100％ |
The preparation of retardants coatings and novel flame-retardant cigarette tipping paper:
In 10 kg water, slowly add 200 gram sodium alginates, be dissolved to clear solution, add 2000 gram water-soluble poly ammonium phosphate again, be stirred to dissolving fully while stirring, retardants coatings; Be injected into then in cigarette tipping paper printing (gravure) the machine China ink groove, the inhibiting tape of coating one deck certain width at the regular-size cigarette tipping paper back side, the tipping paper after the coating is through drying, cutting into dish, and cigarette becomes cigarette to prop up on cigarette machine again.
Adopt above-mentioned novel flame-retardant cigarette tipping paper and common tipping paper, identical pipe tobacco and other auxiliary material respectively, become two kinds of cigarette samples by conventional production method cigarette.By specialty teacher of the smokeing panel test two kinds of cigarette sample qualities (fragrance, harmony, assorted gas, excitant, pleasant impression etc.) are estimated.By standard method two kinds of cigarette sample main flume conventional chemical indexs are carried out analyzing and testing simultaneously.
The cigarette sample quality evaluation is the result show, the cigarette that is rolled by novel flame-retardant cigarette tipping paper of the present invention can keep original suction quality of cigarette and taste.
Cigarette sample main flume conventional chemical index analysis testing result shows both basic indifferences.
The end extinguishing test:
K. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back horizontal positioned, and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 4.
L. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back and vertically place (combustion head-up), and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 4.
Table 4
| Light number | From putting out number | From putting out rate | |
| The regular-size cigarette tipping paper | 40 | 0 | 0％ |
| Novel flame-retardant cigarette tipping paper of the present invention | 40 | 40 | 100％ |
The preparation of retardants coatings and novel flame-retardant cigarette tipping paper:
In 10 kg water, slowly add 200 gram xanthans, be dissolved to clear solution, add 2000 gram sodium dihydrogen phosphates and 1000 gram sodium hydrogen phosphates again, be stirred to dissolving fully while stirring, retardants coatings; Be injected into then in cigarette tipping paper printing (gravure) the machine China ink groove, the inhibiting tape of coating one deck certain width at the regular-size cigarette tipping paper back side, the tipping paper after the coating is through drying, cutting into dish, and cigarette becomes cigarette to prop up on cigarette machine again.
Adopt above-mentioned novel flame-retardant cigarette tipping paper and common tipping paper, identical pipe tobacco and other auxiliary material respectively, become two kinds of cigarette samples by conventional production method cigarette.By specialty teacher of the smokeing panel test two kinds of cigarette sample qualities (fragrance, harmony, assorted gas, excitant, pleasant impression etc.) are estimated.By standard method two kinds of cigarette sample main flume conventional chemical indexs are carried out analyzing and testing simultaneously.
The cigarette sample quality evaluation is the result show, the cigarette that is rolled by novel flame-retardant cigarette tipping paper of the present invention can keep original suction quality of cigarette and taste.
Cigarette sample main flume conventional chemical index analysis testing result shows both basic indifferences.
The end extinguishing test:
M. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back horizontal positioned, and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 5.
N. two kinds of cigarette samples are divided into two groups, respectively get 20 and light the back and vertically place (combustion head-up), and burning voluntarily when the position of firing to tipping paper, is observed it from putting out rate.The result sees the following form 5.
Table 5
| Light number | From putting out number | From putting out rate | |
| The regular-size cigarette tipping paper | 40 | 4 | 10％ |
| Novel flame-retardant cigarette tipping paper of the present invention | 40 | 40 | 100％ |
Claims (9)
1. the application process of a retardants coatings; It is characterized in that; With described retardants coatings be coated on be used on the cigarette tipping paper fire-retardant; Described retardants coatings is made up of following mass percent component: 10-25% fire retardant, 70-85% auxiliary agent and 1-5% thickener are formed, and described fire retardant comprises one or more in ammonium dihydrogen phosphate (ADP), diammonium hydrogen phosphate, ammonium phosphate, sodium dihydrogen phosphate, sodium hydrogen phosphate, the water-soluble poly ammonium phosphate.
2. application process according to claim 1; It is characterized in that; Described auxiliary agent comprises the phosphoric acid,diluted aqueous solution of water or 1-5%, and described thickener comprises one or more in hydroxypropyl methylcellulose, starch phosphate sodium, sodium alginate, xanthans, chitin, tamarind seed polysaccharide glue, the titanium dioxide.
3. application process according to claim 1 is characterized in that, described retardants coatings is coated on the face that cigarette tipping paper is inboard with filter rod contacts.
4. application process according to claim 3 is characterized in that, described retardants coatings is coated with into a fire-retardant endless belt, joins with the junction of filter rod and pipe tobacco.
5. application process according to claim 4 is characterized in that, described fire-retardant endless belt width is the 5-6 millimeter.
6. fire-retardant cigarette tipping paper; It is characterized in that; Retardants coatings is coated on the face that cigarette tipping paper is inboard with filter rod contacts obtains; Described retardants coatings is made up of following mass percent component: the 10-25% fire retardant; 70-85% auxiliary agent and 1-5% thickener are formed; Described fire retardant comprises ammonium dihydrogen phosphate (ADP); Diammonium hydrogen phosphate; Ammonium phosphate; Sodium dihydrogen phosphate; Sodium hydrogen phosphate; In the water-soluble poly ammonium phosphate one or more; Described auxiliary agent comprises the phosphoric acid,diluted aqueous solution of water or 1-5%, and described thickener comprises hydroxypropyl methylcellulose; Starch phosphate sodium; Sodium alginate; Xanthans; Chitin; Tamarind seed polysaccharide glue; In the titanium dioxide one or more.
7. fire-retardant cigarette tipping paper according to claim 6 is characterized in that, described retardants coatings is coated with into a fire-retardant endless belt, joins with the junction of filter rod and pipe tobacco.
8. fire-retardant cigarette tipping paper according to claim 7 is characterized in that, described fire-retardant endless belt width is the 5-6 millimeter.
9. the fire-retardant cigarette of stub is characterized in that, is the cigarette that is prepared from each described fire-retardant cigarette tipping paper of claim 6-7.
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| CN 201110222224 CN102345247B (en) | 2011-08-04 | 2011-08-04 | Application method of flame retardant paint, as well as flame-retardant cigarette tipping paper and cigarette |
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| CN102345247B CN102345247B (en) | 2013-08-14 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103031779A (en) * | 2012-12-11 | 2013-04-10 | 潍坊华港包装材料有限公司 | Cigarette tipping paper and production process thereof |
| CN108997846A (en) * | 2018-07-11 | 2018-12-14 | 甘灿新 | A kind of glue composite fireproof slurry and preparation method thereof |
| CN110924221A (en) * | 2018-09-19 | 2020-03-27 | 湖南中烟工业有限责任公司 | Flame retardant for fine cigarettes and application and preparation method thereof |
| CN112030605A (en) * | 2020-09-02 | 2020-12-04 | 云南中烟工业有限责任公司 | Microbial polysaccharide flame-retardant coating for cigarette paper and preparation method and application thereof |
| CN112080962A (en) * | 2020-09-04 | 2020-12-15 | 中国制浆造纸研究院有限公司 | Flame-retardant coating for cigarette paper, low-ignition-tendency cigarette paper and preparation method thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070458A (en) * | 2006-05-10 | 2007-11-14 | 许昌南 | Adhesive special for heat-insulation sound-absorbing heat-isolation fiber coating and preparing method |
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2011
- 2011-08-04 CN CN 201110222224 patent/CN102345247B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101070458A (en) * | 2006-05-10 | 2007-11-14 | 许昌南 | Adhesive special for heat-insulation sound-absorbing heat-isolation fiber coating and preparing method |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103031779A (en) * | 2012-12-11 | 2013-04-10 | 潍坊华港包装材料有限公司 | Cigarette tipping paper and production process thereof |
| CN108997846A (en) * | 2018-07-11 | 2018-12-14 | 甘灿新 | A kind of glue composite fireproof slurry and preparation method thereof |
| CN110924221A (en) * | 2018-09-19 | 2020-03-27 | 湖南中烟工业有限责任公司 | Flame retardant for fine cigarettes and application and preparation method thereof |
| CN112030605A (en) * | 2020-09-02 | 2020-12-04 | 云南中烟工业有限责任公司 | Microbial polysaccharide flame-retardant coating for cigarette paper and preparation method and application thereof |
| CN112080962A (en) * | 2020-09-04 | 2020-12-15 | 中国制浆造纸研究院有限公司 | Flame-retardant coating for cigarette paper, low-ignition-tendency cigarette paper and preparation method thereof |
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| CN102345247B (en) | 2013-08-14 |
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