CN102251392A - Fluffy softening treatment method for wool - Google Patents
Fluffy softening treatment method for wool Download PDFInfo
- Publication number
- CN102251392A CN102251392A CN2011101616360A CN201110161636A CN102251392A CN 102251392 A CN102251392 A CN 102251392A CN 2011101616360 A CN2011101616360 A CN 2011101616360A CN 201110161636 A CN201110161636 A CN 201110161636A CN 102251392 A CN102251392 A CN 102251392A
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- CN
- China
- Prior art keywords
- wool
- treatment method
- controlled
- weight
- described wool
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 210000002268 wool Anatomy 0.000 title claims abstract description 124
- 238000000034 method Methods 0.000 title claims abstract description 37
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000004902 Softening Agent Substances 0.000 claims abstract description 14
- HRZFUMHJMZEROT-UHFFFAOYSA-L sodium disulfite Chemical compound [Na+].[Na+].[O-]S(=O)S([O-])(=O)=O HRZFUMHJMZEROT-UHFFFAOYSA-L 0.000 claims abstract description 14
- 235000010262 sodium metabisulphite Nutrition 0.000 claims abstract description 14
- 238000006298 dechlorination reaction Methods 0.000 claims abstract description 12
- 239000012286 potassium permanganate Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 238000004061 bleaching Methods 0.000 claims abstract description 9
- 230000007935 neutral effect Effects 0.000 claims abstract description 6
- 150000004045 organic chlorine compounds Chemical class 0.000 claims abstract description 6
- 229960002163 hydrogen peroxide Drugs 0.000 claims description 12
- 229920001296 polysiloxane Polymers 0.000 claims description 12
- 239000003814 drug Substances 0.000 claims description 8
- 102000004169 proteins and genes Human genes 0.000 claims description 7
- 108090000623 proteins and genes Proteins 0.000 claims description 7
- 229940001584 sodium metabisulfite Drugs 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 5
- 238000004886 process control Methods 0.000 abstract description 3
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000006386 neutralization reaction Methods 0.000 abstract description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 2
- 229910052710 silicon Inorganic materials 0.000 abstract 2
- 239000010703 silicon Substances 0.000 abstract 2
- 230000002378 acidificating effect Effects 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000004383 yellowing Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 125000001309 chloro group Chemical group Cl* 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- FFBHFFJDDLITSX-UHFFFAOYSA-N benzyl N-[2-hydroxy-4-(3-oxomorpholin-4-yl)phenyl]carbamate Chemical compound OC1=C(NC(=O)OCC2=CC=CC=C2)C=CC(=C1)N1CCOCC1=O FFBHFFJDDLITSX-UHFFFAOYSA-N 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005660 chlorination reaction Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000004043 dyeing Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000009950 felting Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 238000002161 passivation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000005201 scrubbing Methods 0.000 description 1
- SUKJFIGYRHOWBL-UHFFFAOYSA-N sodium hypochlorite Chemical compound [Na+].Cl[O-] SUKJFIGYRHOWBL-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a fluffy softening treatment method for wool. The method comprises the following steps of: 1) applying organic chlorine compound and potassium permanganate to the wool on padding equipment under the condition of closing to neutral pH value, and then staying for 5 to 10 minutes so that the agents are fully reacted with the wool; 2) adding sodium pyrosulfite solution and performing neutralization and dechlorination treatment; 3) bleaching the wool by using clean water; 4) bleaching the wool by using hydrogen peroxide solution; 5) applying organic silicon softening agent to the wool under the acidic condition, wherein the applying amount of the organic silicon softening agent is 0.3 percent of the weight of the wool; and 6) drying the wool, and controlling the moisture regain of the dried wool at 8 to 10 percent. Compared with the prior art, the method has the advantages that: the treatment process is simplified, the process control is simple, the production efficiency can be remarkably improved, the method is convenient and reliable to use, the fluffy degree of the wool can be improved, the handfeel of the wool is improved remarkably, and the problem of yellowing after the wool is modified is effectively solved by bleaching treatment.
Description
Technical field
The invention belongs to the technical field that wool modifying is handled, specifically a kind of fluffy soft treatment method of wool.
Background technology
At present, along with improving constantly of people's living standard, the clothes of making as raw material with wool more and more are subjected to people's favor, and wool is a kind of natural protein fibre, it has many excellent characteristic,, better elastic soft as gloss, ABRASION RESISTANCE, hygroscopicity and warmth retention property etc.But the distinctive scale layer structure of wool easily makes woolen size felting distortion, weavy grain is smudgy, so limited the practicality of wool and the exploitation in market, therefore, on woolen industry, extensively adopt strong oxidation processes to reach the outward appearance feel of improving wool, present normally used oxidant mainly is chlorine and clorox, wool is after chloridized, can reach the effect of wool scale upgrading, and wool internal protein structure can produce a series of variation, improves the feel of wool after these processing procedures with the method that applies softener.Application number is the preparation method that 200610096303.3 Chinese invention patent discloses a kind of water scrubbing wool fabric and goods thereof, and employed in the chloridized in this patent promptly is chlorine.
But there is following defective in conventional chlorination processing method: in use medicament is violent to the wool reaction, and technology controlling and process requires high, and can not effectively improve the trend that wool after bulking intensity, the especially chloridized of wool feel has yellow.
Summary of the invention
The present invention is directed to deficiency of the prior art, provide a kind of work simplification, the fluffy soft treatment method of the simple wool of process control, the wool that uses this method to handle, its bulking intensity is greatly improved, and efficiently solves the phenomenon of flavescence behind the wool modifying.
In order to solve the problems of the technologies described above, the present invention is solved by following technical proposals: a kind of fluffy soft treatment method of wool, it is characterized in that may further comprise the steps: 1) organochlorine compound and potassium permanganate are being applied on the wool near padding on the equipment under the condition of neutral pH value, wherein, the applied amount of potassium permanganate is 0.5% to 1% of a described wool weight, potassium permanganate is to make the wool feel after the processing fluffy as the main effect of handling medicament, stops then medicament and described wool are fully reacted.Medicament carries out slowly and uniformly degrading to wool surface scale, when reaching the function needs, only give wool fibre MIN damage, and keep the primary characteristic of wool to greatest extent, wool is handled through the organic chloride long period, that relax, make wool surface scale angle uniform passivation, the organic matter in the oxidation processes combines the bulkiness that has increased wool with wool; 2) the interpolation sodium metabisulfite solution neutralizes and the dechlorination processing, and the addition of described sodium pyrosulfite is 1% of a described wool weight, and pH value is controlled at 4 in the dechlorination process, and temperature is controlled at 20-40 degree centigrade.Wool recovers true qualities after the sodium pyrosulfite dechlorination is handled, can judge the effect of neutralisation treatment with the situation of change of purple dot on the wool; 3) use clear water that described wool is carried out rinsing, remove the dirts such as protein that adhere on the described wool surface; 4) use hydrogenperoxide steam generator that described wool is bleached processing, the applied amount of hydrogen peroxide is 1% of a described wool weight, and the bleaching process pH value is controlled at 7-8, and temperature is 40 degrees centigrade.This step process can be improved the whiteness of wool, the peculiar smell after also but removal process 1 is handled simultaneously on the wool, after brightening processing, product dyeing back color and luster is more gorgeous, in being particularly suitable for dying, light color, wool product color effect when stamp will be more remarkable; 5) under acid condition described wool is applied silicone softening agent, the applied amount of described silicone softening agent is 0.3% of a described wool weight.After applying silicone softening agent, the feel of wool is with exquisiteness Paint Gloss; 6) described wool is dried processing, the regain of the described wool in baking back is controlled at 8-10%.The purpose of this step is to solidify fully in order to ensure silicone softening agent, to reach the effect of lasting softness.
In order to obtain better technique effect, further technical measures also comprise: the concentration of sodium metabisulfite solution described in the above-mentioned steps 2 is 80 to 120 grams per liters.
The use amount of clear water described in the above-mentioned steps 3 is 3 to 5 times of described wool weight.
The concentration of hydrogenperoxide steam generator described in the above-mentioned steps 4 is 80 to 120 grams per liters.
In the above-mentioned steps 6 described wool is dried when handling, its temperature is controlled at 50 to 60 degrees centigrade.
Compared with prior art, the present invention has following beneficial effect: treatment process is simplified, and process control is simple, production efficiency can be significantly improved, and is easy to use and reliable, can improve the bulking intensity of wool, it is remarkable to improve feel, the phenomenon of flavescence behind the effective solution of the bleaching processing wool modifying.
The specific embodiment
Below in conjunction with the specific embodiment the present invention is described in further detail: embodiment 1, a kind of fluffy soft treatment method of wool, it may further comprise the steps: 1) near padding on the equipment under the condition of neutral pH value organochlorine compound and potassium permanganate are being applied on the wool, wherein, the applied amount of potassium permanganate is 0.5% of a described wool weight, stops then medicament and described wool are fully reacted; 2) adding concentration is that the sodium metabisulfite solution of 80 grams per liters neutralizes and dechlorination is handled, and the addition of described sodium pyrosulfite is 1% of a described wool weight, and pH value is controlled at 4 in the dechlorination process, and temperature is controlled at 20 degrees centigrade; 3) use clear water that described wool is carried out rinsing, the use amount of clear water is 3 times of described wool weight, removes the dirts such as protein that adhere on the described wool surface; 4) working concentration is that the hydrogenperoxide steam generator of 80 grams per liters is bleached processing to described wool, and the applied amount of hydrogen peroxide is 1% of a described wool weight, and the bleaching process pH value is controlled at 7-8, and temperature is 40 degrees centigrade; 5) under acid condition described wool is applied silicone softening agent, the applied amount of described silicone softening agent is 0.3% of a described wool weight; 6) under temperature is 50 degrees centigrade condition described wool is dried processing, the regain of the described wool in baking back is controlled at 8%.
Embodiment 2, a kind of fluffy soft treatment method of wool, it may further comprise the steps: 1) near padding on the equipment under the condition of neutral pH value organochlorine compound and potassium permanganate are being applied on the wool, wherein, the applied amount of potassium permanganate is 1% of a described wool weight, stops then medicament and described wool are fully reacted; 2) adding concentration is that the sodium metabisulfite solution of 120 grams per liters neutralizes and dechlorination is handled, and the addition of described sodium pyrosulfite is 1% of a described wool weight, and pH value is controlled at 4 in the dechlorination process, and temperature is controlled at 40 degrees centigrade; 3) use clear water that described wool is carried out rinsing, the use amount of clear water is 5 times of described wool weight, removes the dirts such as protein that adhere on the described wool surface; 4) working concentration is that the hydrogenperoxide steam generator of 120 grams per liters is bleached processing to described wool, and the applied amount of hydrogen peroxide is 1% of a described wool weight, and the bleaching process pH value is controlled at 7-8, and temperature is 40 degrees centigrade; 5) under acid condition described wool is applied silicone softening agent, the applied amount of described silicone softening agent is 0.3% of a described wool weight; 6) under temperature is 60 degrees centigrade condition described wool is dried processing, the regain of the described wool in baking back is controlled at 10%.
Embodiment 3, a kind of fluffy soft treatment method of wool, it may further comprise the steps: 1) near padding on the equipment under the condition of neutral pH value organochlorine compound and potassium permanganate are being applied on the wool, wherein, the applied amount of potassium permanganate is 0.75% of a described wool weight, stops then medicament and described wool are fully reacted; 2) adding concentration is that the sodium metabisulfite solution of 100 grams per liters neutralizes and dechlorination is handled, and the addition of described sodium pyrosulfite is 1% of a described wool weight, and pH value is controlled at 4 in the dechlorination process, and temperature is controlled at 30 degrees centigrade; 3) use clear water that described wool is carried out rinsing, the use amount of clear water is 4 times of described wool weight, removes the dirts such as protein that adhere on the described wool surface; 4) working concentration is that the hydrogenperoxide steam generator of 100 grams per liters is bleached processing to described wool, and the applied amount of hydrogen peroxide is 1% of a described wool weight, and the bleaching process pH value is controlled at 7-8, and temperature is 40 degrees centigrade; 5) under acid condition described wool is applied silicone softening agent, the applied amount of described silicone softening agent is 0.3% of a described wool weight; 6) under temperature is 55 degrees centigrade condition described wool is dried processing, the regain of the described wool in baking back is controlled at 9%.
Claims (5)
1. the fluffy soft treatment method of a wool, it is characterized in that may further comprise the steps: 1) organochlorine compound and potassium permanganate are being applied on the wool near padding on the equipment under the condition of neutral pH value, wherein, the applied amount of potassium permanganate is 0.5% to 1% of a described wool weight, stops then medicament and described wool are fully reacted; 2) the interpolation sodium metabisulfite solution neutralizes and the dechlorination processing, and the addition of described sodium pyrosulfite is 1% of a described wool weight, and pH value is controlled at 4 in the dechlorination process, and temperature is controlled at 20-40 degree centigrade; 3) use clear water that described wool is carried out rinsing, remove the dirts such as protein that adhere on the described wool surface; 4) use hydrogenperoxide steam generator that described wool is bleached processing, the applied amount of hydrogen peroxide is 1% of a described wool weight, and the bleaching process pH value is controlled at 7-8, and temperature is 40 degrees centigrade; 5) under acid condition described wool is applied silicone softening agent, the applied amount of described silicone softening agent is 0.3% of a described wool weight; 6) described wool is dried processing, the regain of the described wool in baking back is controlled at 8-10%.
2. the fluffy soft treatment method of a kind of wool according to claim 1, it is characterized in that: the concentration of sodium metabisulfite solution described in the step 2 is 80 to 120 grams per liters.
3. the fluffy soft treatment method of a kind of wool according to claim 1, it is characterized in that: the use amount of clear water described in the step 3 is 3 to 5 times of described wool weight.
4. the fluffy soft treatment method of a kind of wool according to claim 1, it is characterized in that: the concentration of hydrogenperoxide steam generator described in the step 4 is 80 to 120 grams per liters.
5. the fluffy soft treatment method of a kind of wool according to claim 1 is characterized in that: in the step 6 described wool is dried when handling, its temperature is controlled at 50 to 60 degrees centigrade.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011101616360A CN102251392B (en) | 2011-06-16 | 2011-06-16 | Fluffy softening treatment method for wool |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2011101616360A CN102251392B (en) | 2011-06-16 | 2011-06-16 | Fluffy softening treatment method for wool |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102251392A true CN102251392A (en) | 2011-11-23 |
| CN102251392B CN102251392B (en) | 2013-04-24 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2011101616360A Expired - Fee Related CN102251392B (en) | 2011-06-16 | 2011-06-16 | Fluffy softening treatment method for wool |
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| Country | Link |
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| CN (1) | CN102251392B (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102943380A (en) * | 2012-11-21 | 2013-02-27 | 桐乡市濮院毛针织技术服务中心 | Formula and synthetic process of multifunctional fluffy additive |
| CN103243547A (en) * | 2013-04-24 | 2013-08-14 | 上海嘉麟杰纺织品股份有限公司 | Preparation method of humidity controlled wool blended knitted fabric |
| CN103850121A (en) * | 2014-02-21 | 2014-06-11 | 朱文潮 | Wool spinning softening agent |
| CN105113220A (en) * | 2015-09-29 | 2015-12-02 | 武汉纺织大学 | Method for removing scales on surface of wool |
| CN105795699A (en) * | 2016-05-13 | 2016-07-27 | 无为县荣华鬃刷制品有限公司 | Solution capable of improving weathering resistance of bristles |
| CN109023911A (en) * | 2018-09-13 | 2018-12-18 | 许昌市建安区东和畜牧养殖专业合作社 | The low damage wool of one kind tentatively cleans bleaching process |
| CN112981934A (en) * | 2019-12-17 | 2021-06-18 | 米歇尔（苏州）羊毛工业有限公司 | Wool heat preservation quilt |
| CN113005777A (en) * | 2019-12-20 | 2021-06-22 | 米歇尔（苏州）羊毛工业有限公司 | Washable shrinkage-proof wool quilt |
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| JPH01124677A (en) * | 1987-11-09 | 1989-05-17 | Seiji Kubo | Shrinkproof processing of knitted/woven fabric by spun wool yarn |
| CN1117099A (en) * | 1994-07-16 | 1996-02-21 | 张海燕 | Surface modification treatment of sheep wool |
| CN1414170A (en) * | 2002-10-25 | 2003-04-30 | 泰安康平纳毛纺织有限公司 | Method of multistep chemical treatment of sheep's wool to imitate Alpack fibre |
| CN101418515A (en) * | 2008-11-27 | 2009-04-29 | 浙江雀屏纺织化工股份有限公司 | Mercerization and shrinkproof finishing method for woven fabric |
-
2011
- 2011-06-16 CN CN2011101616360A patent/CN102251392B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH01124677A (en) * | 1987-11-09 | 1989-05-17 | Seiji Kubo | Shrinkproof processing of knitted/woven fabric by spun wool yarn |
| CN1117099A (en) * | 1994-07-16 | 1996-02-21 | 张海燕 | Surface modification treatment of sheep wool |
| CN1414170A (en) * | 2002-10-25 | 2003-04-30 | 泰安康平纳毛纺织有限公司 | Method of multistep chemical treatment of sheep's wool to imitate Alpack fibre |
| CN101418515A (en) * | 2008-11-27 | 2009-04-29 | 浙江雀屏纺织化工股份有限公司 | Mercerization and shrinkproof finishing method for woven fabric |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102943380A (en) * | 2012-11-21 | 2013-02-27 | 桐乡市濮院毛针织技术服务中心 | Formula and synthetic process of multifunctional fluffy additive |
| CN102943380B (en) * | 2012-11-21 | 2014-08-20 | 桐乡市濮院毛针织技术服务中心 | Formula and synthetic process of multifunctional fluffy additive |
| CN103243547A (en) * | 2013-04-24 | 2013-08-14 | 上海嘉麟杰纺织品股份有限公司 | Preparation method of humidity controlled wool blended knitted fabric |
| CN103243547B (en) * | 2013-04-24 | 2015-03-04 | 上海嘉麟杰纺织品股份有限公司 | Preparation method of humidity controlled wool blended knitted fabric |
| CN103850121A (en) * | 2014-02-21 | 2014-06-11 | 朱文潮 | Wool spinning softening agent |
| CN105113220A (en) * | 2015-09-29 | 2015-12-02 | 武汉纺织大学 | Method for removing scales on surface of wool |
| CN105795699A (en) * | 2016-05-13 | 2016-07-27 | 无为县荣华鬃刷制品有限公司 | Solution capable of improving weathering resistance of bristles |
| CN109023911A (en) * | 2018-09-13 | 2018-12-18 | 许昌市建安区东和畜牧养殖专业合作社 | The low damage wool of one kind tentatively cleans bleaching process |
| CN112981934A (en) * | 2019-12-17 | 2021-06-18 | 米歇尔（苏州）羊毛工业有限公司 | Wool heat preservation quilt |
| CN113005777A (en) * | 2019-12-20 | 2021-06-22 | 米歇尔（苏州）羊毛工业有限公司 | Washable shrinkage-proof wool quilt |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102251392B (en) | 2013-04-24 |
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Address after: 315032 Zhejiang Province, Ningbo Jiangbei District Haichuan Road No. 65 Patentee after: CONSINEE GROUP CO.,LTD. Address before: 315032 Zhejiang Province, Ningbo Jiangbei District Haichuan Road No. 65 Patentee before: NINGBO CONSINEE PLUSH PRODUCTS CO.,LTD. |
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Granted publication date: 20130424 |