CN102943380B - Formula and synthetic process of multifunctional fluffy additive - Google Patents
Formula and synthetic process of multifunctional fluffy additive Download PDFInfo
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Abstract
The invention discloses a formula and a synthetic process and particularly relates to a formula and a synthetic process of a multifunctional fluffy additive. The formula and the synthetic process effectively improve filling power of wool fabric. The multifunctional fluffy additive comprises 130-170 parts of sulfonate succinic acid dioctyl-phthalate sodium salt, 250-300 parts of fatty alcohol-polyoxyethylene ether, 240-260 parts of N-dimethyl formamide, 45-55 parts of sodium chloride, 45-55 parts of urea and 200-250 parts of water. The formula and the synthetic process are low in production cost and simple in processing technology, and the processed products are good in effect.
Description
Technical field
The present invention relates to a kind of formula and synthesis technique, especially a kind of formula of multi-functional fluffy additive and synthesis technique.
Background technology
Leavening agent is a kind of on the make one of indispensable additive of woollen sweater, and the quality of leavening agent directly has influence on the quality of Color in woollen sweater subsequent production process.At present, leavening agent washing force and penetrability effect that each enterprise is used are all poor, and fabric color after treatment, mellowness are undesirable, often occur that the look after woollen sweater garment dyeing, stamp is colored, and the local problem such as inhomogeneous of look shallow.
In addition, in existing leavening agent, contain the chemical compositions such as formaldehyde, heavy metal, APEO, environment is had to great pollution, therefore also do not meet the environmental protection concept of modern production.
Summary of the invention
The object of the invention is the deficiency in order to solve above-mentioned technology and a kind of formula and synthesis technique of a kind of multi-functional fluffy additive of effective raising wool fabric bulking intensity are provided.
In order to achieve the above object, the formula of the designed a kind of multi-functional fluffy additive of the present invention, it comprises 130-170 part sulfosuccinate dibutyl ester sodium salt, 250-300 part fatty alcohol-polyoxyethylene ether, 240-260 part dinethylformamide, 45-55 part sodium chloride, 45-55 part urea, 200-250 part water; Above umber calculates by weight.
As preferably, described formula also comprises glacial acetic acid, is used for regulating pH value.
Production technology: the first step, in reactor, add 200-250 part water, be heated to 50 DEG C, stir; Second step, adds 130-170 part sulfosuccinate dibutyl ester sodium salt, 250-300 part fatty alcohol-polyoxyethylene ether to render to together in reactor, and insulation reaction 45 minutes also stirs, and is heated to 80 DEG C, is incubated 2 hours; The 3rd step, adds 45-55 part sodium chloride, 45-55 part urea, and insulation reaction 45 minutes also stirs; The 4th step, adds glacial acetic acid to regulate pH value to 5～6, stirs, and cooling, discharging.
The formula of a kind of multi-functional fluffy additive that the present invention obtains and synthesis technique, add when cleaning before wool stripping squama, can effectively improve the bulking intensity of wool fabric, and be conducive to the uniformity of fabric face chlorination after wool stripping squama, can effectively prevent that the look after woollen sweater garment dyeing, stamp is colored, look shallow and the local problem such as inhomogeneous.This formula and method, production cost is low, and processing technology is simple, and the product effect processing is remarkable.
Brief description of the drawings
Nothing.
Detailed description of the invention
Be further described below by embodiment the present invention.
Embodiment 1:
Formula and the synthesis technique of a kind of multi-functional fluffy additive that the present embodiment is described, the first step adds 200 parts of water in reactor, is heated to 50 DEG C, stirs; Second step, adds 130 parts of sulfosuccinate dibutyl ester sodium salts, 250 parts of fatty alcohol-polyoxyethylene ether to render to together in reactor, and insulation reaction 45 minutes also stirs, and is heated to 80 DEG C, is incubated 2 hours; The 3rd step, adds 45 parts of sodium chloride, 45 parts of urea, and insulation reaction 45 minutes also stirs; The 4th step, adds glacial acetic acid to regulate pH value to 5～6, stirs, and cooling, discharging.
Embodiment 2:
Formula and the synthesis technique of a kind of multi-functional fluffy additive that the present embodiment is described, the first step adds 250 parts of water in reactor, is heated to 50 DEG C, stirs; Second step, adds 170 parts of sulfosuccinate dibutyl ester sodium salts, 300 parts of fatty alcohol-polyoxyethylene ether to render to together in reactor, and insulation reaction 45 minutes also stirs, and is heated to 80 DEG C, is incubated 2 hours; The 3rd step, adds 55 parts of sodium chloride, 55 parts of urea, and insulation reaction 45 minutes also stirs; The 4th step, adds glacial acetic acid to regulate pH value to 5～6, stirs, and cooling, discharging.
Embodiment 3:
Formula and the synthesis technique of a kind of multi-functional fluffy additive that the present embodiment is described, the first step adds 230 parts of water in reactor, is heated to 50 DEG C, stirs; Second step, adds 150 parts of sulfosuccinate dibutyl ester sodium salts, 250 parts of fatty alcohol-polyoxyethylene ether to render to together in reactor, and insulation reaction 45 minutes also stirs, and is heated to 80 DEG C, is incubated 2 hours; The 3rd step, adds 50 parts of sodium chloride, 50 parts of urea, and insulation reaction 45 minutes also stirs; The 4th step, adds glacial acetic acid to regulate pH value to 5～6, stirs, and cooling, discharging.
Claims (1)
1. a synthesis technique for multi-functional fluffy additive, is characterized in that: the first step, in reactor, add 200-250 part water, and be heated to 50 DEG C, stir; Second step, adds 130-170 part sulfosuccinate dibutyl ester sodium salt, 250-300 part fatty alcohol-polyoxyethylene ether to render to together in reactor, and insulation reaction 45 minutes also stirs, and is heated to 80 DEG C, is incubated 2 hours; The 3rd step, adds 45-55 part sodium chloride, 45-55 part urea, and insulation reaction 45 minutes also stirs; The 4th step, adds glacial acetic acid to regulate pH value to 5～6, stirs, and cooling, discharging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201210476401.5A CN102943380B (en) | 2012-11-21 | 2012-11-21 | Formula and synthetic process of multifunctional fluffy additive |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210476401.5A CN102943380B (en) | 2012-11-21 | 2012-11-21 | Formula and synthetic process of multifunctional fluffy additive |
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| Publication Number | Publication Date |
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| CN102943380A CN102943380A (en) | 2013-02-27 |
| CN102943380B true CN102943380B (en) | 2014-08-20 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201210476401.5A Active CN102943380B (en) | 2012-11-21 | 2012-11-21 | Formula and synthetic process of multifunctional fluffy additive |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103726328A (en) * | 2013-12-02 | 2014-04-16 | 常熟市新蕾针织有限公司 | Preparation method for swelling agent for woolen sweater |
| CN103741479A (en) * | 2013-12-04 | 2014-04-23 | 江苏双圆袋鼠服饰有限公司 | Preparation process of leavening agent for woollen sweater |
| CN107956105A (en) * | 2017-11-30 | 2018-04-24 | 苏州绣艳天下刺绣工艺有限公司 | A kind of preparation method embroidered with fluffy finishing agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1061632A (en) * | 1991-09-20 | 1992-06-03 | 朝阳毛纺织厂 | Production process of rough spinning wool fabric for moth-proof |
| WO2001064171A2 (en) * | 2000-03-01 | 2001-09-07 | L'oreal S.A. | Hair relaxer compositions utilizing complexing agent activators |
| CN101812806A (en) * | 2010-03-18 | 2010-08-25 | 品德实业(太原)有限公司 | Processing technology for smooth and non-shrinkable wool yarns |
| CN102251392A (en) * | 2011-06-16 | 2011-11-23 | 宁波康赛妮毛绒制品有限公司 | Fluffy softening treatment method for wool |
-
2012
- 2012-11-21 CN CN201210476401.5A patent/CN102943380B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1061632A (en) * | 1991-09-20 | 1992-06-03 | 朝阳毛纺织厂 | Production process of rough spinning wool fabric for moth-proof |
| WO2001064171A2 (en) * | 2000-03-01 | 2001-09-07 | L'oreal S.A. | Hair relaxer compositions utilizing complexing agent activators |
| CN101812806A (en) * | 2010-03-18 | 2010-08-25 | 品德实业(太原)有限公司 | Processing technology for smooth and non-shrinkable wool yarns |
| CN102251392A (en) * | 2011-06-16 | 2011-11-23 | 宁波康赛妮毛绒制品有限公司 | Fluffy softening treatment method for wool |
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| CN102943380A (en) | 2013-02-27 |
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Effective date of registration: 20180606 Address after: 314502 Yongan Road, Pu Yuan Town, Tongxiang, Zhejiang Province, No. 323 Patentee after: Tongxiang Hengyue textile finishing Co., Ltd. Address before: 314500 Zhejiang Jiaxing Tongxiang city Pu Yuan town Wen Yuan Road Industrial Park Tongxiang Pu Yuan Mao knitting technical service center Patentee before: Tongxiang Puyuan Woolen Knitting Technology Service Center |
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| CP03 | Change of name, title or address | ||
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Address after: No. 323, Yong'an Road, Puyuan Town, Tongxiang City, Jiaxing City, Zhejiang Province Patentee after: Tongxiang Hengyue textile finishing Co., Ltd. Address before: 314502 Yongan Road, Pu Yuan Town, Tongxiang, Zhejiang Province, No. 323 Patentee before: Tongxiang Hengyue textile finishing Co., Ltd. |