CN104195852B - A kind of environment-friendly type textile printing and dyeing liquid - Google Patents
A kind of environment-friendly type textile printing and dyeing liquid Download PDFInfo
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- CN104195852B CN104195852B CN201410518280.5A CN201410518280A CN104195852B CN 104195852 B CN104195852 B CN 104195852B CN 201410518280 A CN201410518280 A CN 201410518280A CN 104195852 B CN104195852 B CN 104195852B
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Abstract
The present invention relates to a kind of environment-friendly type textile printing and dyeing liquid, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 15��35 parts, aqueous polyurethane 10��25 parts, alkyl glycoside 5��10 parts, benzothiazole sulfonic acid 3��15 parts, isomeric alcohol polyethenoxy ether 10��50 parts, sorbitan fatty acid ester 5��20 parts, polyoxyethylene glycol 5��10 parts, sodium chlorate 2��10 parts, deionized water 100��200 parts. The useful effect of the present invention is: the dye liquor tinting strength of (1) the present invention is strong, and the rear cloth of colouring has good look firm. (2) dye liquor of the present invention can be stablized and deposits 1 month, there will not be precipitation. (3) dye liquor of the present invention is not containing heavy metal, Environmental Safety. (4) this product environmental protection, it may also be useful to convenient.
Description
Technical field
The present invention relates to a kind of environment-friendly type textile printing and dyeing liquid, belong to technical field of textile printing.
Background technology
Printing and dyeing liquid often uses, because natural fiber is as contained symbiosis impurity in cotton fibre, such as pectin, fat wax and nitrogenous substances etc., the existence of these symbiosis impurity reduces wetting ability and the adsorptivity of fiber, thus cause that dyeing is uneven or the imperfect problem of colour fastness, natural fiber carries out pre-treatment such as alkaline scouring, enzymatic scouring etc. by contained symbiosis Impurity removal, but still cannot to remove completely and remove also can with the unfavorable factor of cellulose degradation while symbiosis impurity. To this, it is necessary to use the printing and dyeing liquid of some environment-friendly types, the impact on environment can be reduced.
Summary of the invention
It is an object of the invention to provide the environment-friendly type printing and dyeing liquid that a kind of tinting strength is strong and stable.
It is as follows that the present invention realizes the technical scheme that above-mentioned purpose adopts:
A kind of environment-friendly type textile printing and dyeing liquid, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 15��35 parts, aqueous polyurethane 10��25 parts, alkyl glycoside 5��10 parts, benzothiazole sulfonic acid 3��15 parts, isomeric alcohol polyethenoxy ether 10��50 parts, sorbitan fatty acid ester 5��20 parts, polyoxyethylene glycol 5��10 parts, sodium chlorate 2��10 parts, deionized water 100��200 parts.
Further, above-mentioned environment-friendly type textile printing and dyeing liquid, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 20��30 parts, aqueous polyurethane 15��20 parts, alkyl glycoside 6��8 parts, benzothiazole sulfonic acid 5��10 parts, isomeric alcohol polyethenoxy ether 15��30 parts, sorbitan fatty acid ester 10��15 parts, polyoxyethylene glycol 6��8 parts, sodium chlorate 4��8 parts, deionized water 120��180 parts.
Further, above-mentioned environment-friendly type textile printing and dyeing liquid, its step of preparation process is as follows:
(1) get the disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate of above-mentioned mass fraction, aqueous polyurethane, benzothiazole sulfonic acid, polyoxyethylene glycol join in deionized water, be fully uniformly mixed, and it is for subsequent use to be warming up to 60��80 DEG C;
(2) in step (1) in obtained mixture, add alkyl glycoside and the isomeric alcohol polyethenoxy ether of above-mentioned mass fraction, warming while stirring, when temperature rises to 85 DEG C��90 DEG C, add a part sorbitan fatty acid ester, and maintain the temperature at 85 DEG C��90 DEG C 3��5 hours;
(3) it is cooled to 60 DEG C��70 DEG C, adds the sorbitan fatty acid ester of residual mass part number and the sodium chlorate of above-mentioned mass fraction, be incubated 15��45 minutes; Then it is cooled to 35 DEG C��50 DEG C, it is incubated 50��90 minutes, be then down to room temperature and then can obtain these printing and dyeing liquid product.
The useful effect of the present invention: the dye liquor tinting strength of (1) the present invention is strong, the rear cloth of colouring has good look firm. (2) dye liquor of the present invention can be stablized and deposits 1 month, there will not be precipitation. (3) dye liquor of the present invention is not containing heavy metal, Environmental Safety. (4) this product environmental protection, it may also be useful to convenient.
Embodiment
Below in conjunction with embodiment, the present invention is described in further details.
Embodiment 1
Environment-friendly type textile printing and dyeing liquid in the present embodiment, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 15 parts, aqueous polyurethane 10 parts, alkyl glycoside 5 parts, benzothiazole sulfonic acid 3 parts, isomeric alcohol polyethenoxy ether 10 parts, sorbitan fatty acid ester 5 parts, polyoxyethylene glycol 5 parts, sodium chlorate 2 parts, deionized water 100 parts.
Above-mentioned environment-friendly type textile printing and dyeing liquid, its step of preparation process is as follows:
(1) get the disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate of above-mentioned mass fraction, aqueous polyurethane, benzothiazole sulfonic acid, polyoxyethylene glycol join in deionized water, be fully uniformly mixed, and it is for subsequent use to be warming up to 60 DEG C;
(2) in step (1) in obtained mixture, add alkyl glycoside and the isomeric alcohol polyethenoxy ether of above-mentioned mass fraction, warming while stirring, when temperature rises to 85 DEG C, add a part sorbitan fatty acid ester, and maintain the temperature at 85 DEG C 5 hours;
(3) it is cooled to 60 DEG C, adds the sorbitan fatty acid ester of residual mass part number and the sodium chlorate of above-mentioned mass fraction, be incubated 45 minutes; Then it is cooled to 35 DEG C, it is incubated 90 minutes, be then down to room temperature and then can obtain these printing and dyeing liquid product.
Embodiment 2
Environment-friendly type textile printing and dyeing liquid in the present embodiment, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 35 parts, aqueous polyurethane 25 parts, alkyl glycoside 10 parts, benzothiazole sulfonic acid 15 parts, isomeric alcohol polyethenoxy ether 50 parts, sorbitan fatty acid ester 20 parts, polyoxyethylene glycol 10 parts, sodium chlorate 10 parts, deionized water 200 parts.
Above-mentioned environment-friendly type textile printing and dyeing liquid, its step of preparation process is as follows:
(1) get the disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate of above-mentioned mass fraction, aqueous polyurethane, benzothiazole sulfonic acid, polyoxyethylene glycol join in deionized water, be fully uniformly mixed, and it is for subsequent use to be warming up to 80 DEG C;
(2) in step (1) in obtained mixture, add alkyl glycoside and the isomeric alcohol polyethenoxy ether of above-mentioned mass fraction, warming while stirring, when temperature rises to 90 DEG C, add part sorbitan fatty acid ester, and maintain the temperature at 90 DEG C and add for 3 hours;
(3) it is cooled to 70 DEG C, adds the sorbitan fatty acid ester of residual mass part number and the sodium chlorate of above-mentioned mass fraction, be incubated 15 minutes; Then it is cooled to 50 DEG C of insulation 50 clocks, then it is down to room temperature and then can obtain these printing and dyeing liquid product.
Embodiment 3
Environment-friendly type textile printing and dyeing liquid in the present embodiment, it is made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 25 parts, aqueous polyurethane 18 parts, alkyl glycoside 8 parts, benzothiazole sulfonic acid 9 parts, isomeric alcohol polyethenoxy ether 30 parts, sorbitan fatty acid ester 13 parts, polyoxyethylene glycol 8 parts, sodium chlorate 6 parts, deionized water 150 parts.
Above-mentioned environment-friendly type textile printing and dyeing liquid, its step of preparation process is as follows:
(1) get the disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate of above-mentioned mass fraction, aqueous polyurethane, benzothiazole sulfonic acid, polyoxyethylene glycol join in deionized water, be fully uniformly mixed, and it is for subsequent use to be warming up to 70 DEG C;
(2) in step (1) in obtained mixture, add alkyl glycoside and the isomeric alcohol polyethenoxy ether of above-mentioned mass fraction, warming while stirring, when temperature rises to 88 DEG C, add a part sorbitan fatty acid ester, and maintain the temperature at 88 DEG C 4 hours;
(3) it is cooled to 65 DEG C, adds the sorbitan fatty acid ester of residual mass part number and the sodium chlorate of above-mentioned mass fraction, be incubated 30 minutes; Then it is cooled to 40 DEG C, it is incubated 70 minutes, be then down to room temperature and then can obtain these printing and dyeing liquid product.
Claims (1)
1. an environment-friendly type textile printing and dyeing liquid, it is characterized in that: be made up of following mass fraction component: disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate 15��35 parts, aqueous polyurethane 10��25 parts, alkyl glycoside 5��10 parts, benzothiazole sulfonic acid 3��15 parts, isomeric alcohol polyethenoxy ether 10��50 parts, sorbitan fatty acid ester 5��20 parts, polyoxyethylene glycol 5��10 parts, sodium chlorate 2��10 parts, deionized water 100��200 parts; Described environment-friendly type textile printing and dyeing liquid, its step of preparation process is as follows:
(1) get the disodium 4-dodecyl-2,4 '-oxydibenzenesulfonate of above-mentioned mass fraction, aqueous polyurethane, benzothiazole sulfonic acid, polyoxyethylene glycol join in deionized water, be fully uniformly mixed, and it is for subsequent use to be warming up to 60��80 DEG C;
(2) in step (1) in obtained mixture, add alkyl glycoside and the isomeric alcohol polyethenoxy ether of above-mentioned mass fraction, warming while stirring, when temperature rises to 85 DEG C��90 DEG C, add a part sorbitan fatty acid ester, and maintain the temperature at 85 DEG C��90 DEG C 3��5 hours;
(3) it is cooled to 60 DEG C��70 DEG C, adds the sorbitan fatty acid ester of residual mass part number and the sodium chlorate of above-mentioned mass fraction, be incubated 15��45 minutes; Then it is cooled to 35 DEG C��50 DEG C, it is incubated 50��90 minutes, be then down to room temperature and then can obtain these printing and dyeing liquid product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410518280.5A CN104195852B (en) | 2014-10-02 | 2014-10-02 | A kind of environment-friendly type textile printing and dyeing liquid |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410518280.5A CN104195852B (en) | 2014-10-02 | 2014-10-02 | A kind of environment-friendly type textile printing and dyeing liquid |
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| Publication Number | Publication Date |
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| CN104195852A CN104195852A (en) | 2014-12-10 |
| CN104195852B true CN104195852B (en) | 2016-06-01 |
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| CN201410518280.5A Expired - Fee Related CN104195852B (en) | 2014-10-02 | 2014-10-02 | A kind of environment-friendly type textile printing and dyeing liquid |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108360271A (en) * | 2018-03-26 | 2018-08-03 | 东莞市科迪实业有限公司 | A kind of aqueous, environmental protective dye liquor |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1644629A (en) * | 2004-05-12 | 2005-07-27 | 安徽大学 | Water polyurethane dye production of coating, textile, artificial leather and leather |
| CN101486852A (en) * | 2007-12-28 | 2009-07-22 | 天津兆阳纳米科技有限公司 | Pigment ink with excellent erasibility |
| CN101531836A (en) * | 2009-04-13 | 2009-09-16 | 杭州中富彩化工新材料有限公司 | Formula of environment-friendly type aqueous color paste for leather and coating as well as manufacturing method thereof |
| CN102146231A (en) * | 2011-04-07 | 2011-08-10 | 上海英威喷墨科技有限公司 | Waterbased pigment type ink-jet printing ink and preparation method and application thereof |
| CN102321984A (en) * | 2011-06-25 | 2012-01-18 | 百利合化工（中山）有限公司 | High-gloss washing resistant environmental-friendly print paste and preparation method thereof |
| CN102852010A (en) * | 2012-08-31 | 2013-01-02 | 无锡新德印染制品有限公司 | Dye liquor for printing and dyeing of cloth |
-
2014
- 2014-10-02 CN CN201410518280.5A patent/CN104195852B/en not_active Expired - Fee Related
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1644629A (en) * | 2004-05-12 | 2005-07-27 | 安徽大学 | Water polyurethane dye production of coating, textile, artificial leather and leather |
| CN101486852A (en) * | 2007-12-28 | 2009-07-22 | 天津兆阳纳米科技有限公司 | Pigment ink with excellent erasibility |
| CN101531836A (en) * | 2009-04-13 | 2009-09-16 | 杭州中富彩化工新材料有限公司 | Formula of environment-friendly type aqueous color paste for leather and coating as well as manufacturing method thereof |
| CN102146231A (en) * | 2011-04-07 | 2011-08-10 | 上海英威喷墨科技有限公司 | Waterbased pigment type ink-jet printing ink and preparation method and application thereof |
| CN102321984A (en) * | 2011-06-25 | 2012-01-18 | 百利合化工（中山）有限公司 | High-gloss washing resistant environmental-friendly print paste and preparation method thereof |
| CN102852010A (en) * | 2012-08-31 | 2013-01-02 | 无锡新德印染制品有限公司 | Dye liquor for printing and dyeing of cloth |
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| CN104195852A (en) | 2014-12-10 |
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