CN103087620A - Dual-component silvery primer - Google Patents
Dual-component silvery primer Download PDFInfo
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- CN103087620A CN103087620A CN201310038606XA CN201310038606A CN103087620A CN 103087620 A CN103087620 A CN 103087620A CN 201310038606X A CN201310038606X A CN 201310038606XA CN 201310038606 A CN201310038606 A CN 201310038606A CN 103087620 A CN103087620 A CN 103087620A
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- 239000000843 powder Substances 0.000 claims abstract description 18
- 239000010425 asbestos Substances 0.000 claims abstract description 17
- 229910052895 riebeckite Inorganic materials 0.000 claims abstract description 17
- DKPFZGUDAPQIHT-UHFFFAOYSA-N butyl acetate Chemical compound CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 13
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 7
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 7
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 7
- KTWOOEGAPBSYNW-UHFFFAOYSA-N ferrocene Chemical compound [Fe+2].C=1C=C[CH-]C=1.C=1C=C[CH-]C=1 KTWOOEGAPBSYNW-UHFFFAOYSA-N 0.000 claims abstract description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 claims abstract description 5
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 4
- -1 aluminum silver Chemical compound 0.000 claims abstract description 4
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 claims abstract description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims abstract description 4
- 229920002554 vinyl polymer Polymers 0.000 claims abstract description 4
- 239000011701 zinc Substances 0.000 claims abstract description 4
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 4
- 239000003973 paint Substances 0.000 claims description 18
- 230000037452 priming Effects 0.000 claims description 16
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 15
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 12
- 229910021641 deionized water Inorganic materials 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims description 9
- 229910052709 silver Inorganic materials 0.000 claims description 9
- 239000004332 silver Substances 0.000 claims description 9
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 5
- 150000003839 salts Chemical class 0.000 claims description 5
- NSOXQYCFHDMMGV-UHFFFAOYSA-N Tetrakis(2-hydroxypropyl)ethylenediamine Chemical compound CC(O)CN(CC(C)O)CCN(CC(C)O)CC(C)O NSOXQYCFHDMMGV-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- 230000007935 neutral effect Effects 0.000 claims description 4
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims description 4
- 229920000120 polyethyl acrylate Polymers 0.000 claims description 3
- 229910000077 silane Inorganic materials 0.000 claims description 3
- 239000002002 slurry Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- CIHOLLKRGTVIJN-UHFFFAOYSA-N tert‐butyl hydroperoxide Chemical compound CC(C)(C)OO CIHOLLKRGTVIJN-UHFFFAOYSA-N 0.000 claims description 3
- SJECZPVISLOESU-UHFFFAOYSA-N 3-trimethoxysilylpropan-1-amine Chemical compound CO[Si](OC)(OC)CCCN SJECZPVISLOESU-UHFFFAOYSA-N 0.000 claims 1
- OMPJBNCRMGITSC-UHFFFAOYSA-N Benzoylperoxide Chemical compound C=1C=CC=CC=1C(=O)OOC(=O)C1=CC=CC=C1 OMPJBNCRMGITSC-UHFFFAOYSA-N 0.000 claims 1
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims 1
- 235000019400 benzoyl peroxide Nutrition 0.000 claims 1
- 238000001035 drying Methods 0.000 abstract description 4
- 206010027627 Miliaria Diseases 0.000 abstract description 3
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 abstract description 3
- 239000007787 solid Substances 0.000 abstract description 3
- 239000002904 solvent Substances 0.000 abstract description 2
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 abstract 2
- 150000004985 diamines Chemical class 0.000 abstract 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 201000004169 miliaria rubra Diseases 0.000 abstract 1
- 229920000058 polyacrylate Polymers 0.000 abstract 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 abstract 1
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- 238000000576 coating method Methods 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 235000019832 sodium triphosphate Nutrition 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 3
- 239000004593 Epoxy Substances 0.000 description 2
- 101710194948 Protein phosphatase PhpP Proteins 0.000 description 2
- VBICKXHEKHSIBG-UHFFFAOYSA-N beta-monoglyceryl stearate Natural products CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 2
- 235000019439 ethyl acetate Nutrition 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- HWGNBUXHKFFFIH-UHFFFAOYSA-I pentasodium;[oxido(phosphonatooxy)phosphoryl] phosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O HWGNBUXHKFFFIH-UHFFFAOYSA-I 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- UNXRWKVEANCORM-UHFFFAOYSA-I triphosphate(5-) Chemical compound [O-]P([O-])(=O)OP([O-])(=O)OP([O-])([O-])=O UNXRWKVEANCORM-UHFFFAOYSA-I 0.000 description 2
- 239000002023 wood Substances 0.000 description 2
- 101100002917 Caenorhabditis elegans ash-2 gene Proteins 0.000 description 1
- 229920001875 Ebonite Polymers 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000013638 trimer Substances 0.000 description 1
Landscapes
- Paints Or Removers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a dual-component silvery primer which consists of components A and B, wherein the component A is composed of the following raw materials in parts by weight: 70-78 parts of hydroxy acrylic resin, 4-6 parts of ferrocene, 10-15 parts of talcum powder, 6-10 parts of aluminum silver paste, 4-7 parts of glycol ether acetate, 5-6 parts of n-butyl acetate, 2-4 parts of zinc stearate, 1-3 parts of modified asbestos powder, 0.8-1 part of vinyl tri (beta-methoxy ethyoxy) silicane, 0.8-1 part of hydroquinone, 0.6-0.8 part of zinc dialkyl dithiophosphate, 0.4-0.6 part of ethyl polyacrylate and 0.4-0.6 part of diethylamine. The primer disclosed by the invention has an excellent solvent release performance, and is capable of effectively preventing generation of prickly heat bubbles; through participation of toluene diisocynate tripolymer and ethidene diamine, the primer is excellent in low-temperature drying performance; and through a reasonable formula, the primer has a comparatively rapid drying speed and good storage stability, and hardness, solid content and viscosity of the primer are kept at comparatively high quality levels as well.
Description
Technical field
The present invention relates generally to a kind of priming paint, relates in particular to a kind of pair of component silver color priming paint.
Background technology
coating is finishing material indispensable in the modern life, Application of coatings gives aesthetic feeling, sense of touch, give coated article with beauty, decorate and protection, paint is a kind of of coating, be capped on the rear paint film that forms in surface of object, make object attractive in appearance and be protected, in recent years, be used for solid wood board, the wood grain panel, on the equipment such as hard rubber sheet priming paint obtained widely development, under cold condition, rate of drying waits shortcoming more slowly but the priming paint that is used at present woodwork coating exists, could polish for a long time thereby need to place, and, the workability of filming that this priming paint forms is relatively poor, has high temperature easily heat rash appears the shortcoming such as bubble.
Summary of the invention
The object of the invention is exactly in order to make up the defective of prior art, a kind of pair of component silver color priming paint to be provided.
The present invention is achieved by the following technical solutions:
A kind of pair of component silver color priming paint, it is comprised of first and second liang of components, and wherein the first component is comprised of the raw material of following weight parts:
Hydroxylated acrylic resin 70-78, ferrocene 4-6, talcum powder 10-15, aluminium-silver slurry 6-10, ethylene glycol ether acetate 4-7, n-butyl acetate 5-6, Zinic stearas 2-4, modified asbestos powder 1-3, vinyl three ('beta '-methoxy oxyethyl group) silane 0.8-1, Resorcinol 0.8-1, zinc dialkyl dithiophosphate 0.6-0.8, polyethyl acrylate 0.4-0.6, diethylamine 0.4-0.6;
The preparation method of described modified asbestos powder is:
Asbestos powder is used 10-15% salt acid soak 3-4 hour, deionized water wash, then soaked 3-4 hour with the 10-12% sodium hydroxide solution, more extremely neutral with deionized water wash, oven dry;
The tripoly phosphate sodium STPP that will be equivalent to asbestos powder weight 2-3% is dissolved in deionized water, the stearic acid monoglyceride, the paregal O of 1-2%, the epoxy tetrahydro-2-ethylhexyl phthalate of 2-3%, the 3-5% aluminum oxide that add again asbestos powder weight 2-3%, high speed 1200-1500 rev/min of stirring, obtain dispersion liquid, dispersion liquid oven dry, pulverizing namely get described modified asbestos powder;
The preparation method of described first component is:
(1) Hydroxylated acrylic resin, glycol ether acetic ester, n-butyl acetate, the ferrocene of above-mentioned weight part are put in reactor, the speed take rotating speed as 600-800 rev/min mixes 10-20 minute;
(2) add Zinic stearas, the talcum powder of above-mentioned weight part, disperseed 25-30 minute with the speed of rotating speed 900-1100 rev/min;
(3) add each raw material of residue of above-mentioned weight part, the speed take rotating speed as 600-800 rev/min mixes 20-30 minute, namely gets described first component;
Described component B is comprised of the raw material of following weight parts:
2,4 toluene diisocyanate tripolymer 65-70, quadrol 10-15, dimethylbenzene 20-30, trees ash 1-2, t-butyl hydroperoxide 0.8-1;
The trees ash of above-mentioned weight part is used 10-15% salt acid soak 3-4 hour, deionized water wash, then soaked 3-4 hour with the 10-12% sodium hydroxide solution, extremely neutral with deionized water wash again, then oven dry mixes with each raw material of above-mentioned weight part, remembers described component B;
First and second liang of components are pressed the weight ratio of 1-1.5:1 and mix, namely get described pair of component silver color priming paint.
Advantage of the present invention is:
Priming paint of the present invention has good solvent release energy, the bubble that can prevent effectively that heat rash appears, owing to having added toluene diisocyanate trimer and quadrol, make this priming paint have good cryodrying, by rational formula, make this priming paint have rate of drying and storage stability faster, its hardness, solid content and viscosity have also kept higher quality level.
Embodiment
Embodiment 1
A kind of pair of component silver color priming paint, it is comprised of first and second liang of components, and wherein the first component is comprised of the raw material of following weight parts (kilogram):
Hydroxylated acrylic resin 78, ferrocene 6, talcum powder 15, aluminium-silver slurry 10, ethylene glycol ether acetate 7, n-butyl acetate 6, Zinic stearas 4, modified asbestos powder 1, vinyl three ('beta '-methoxy oxyethyl group) silane 0.8, Resorcinol 0.8, zinc dialkyl dithiophosphate 0.8, polyethyl acrylate 0.6, diethylamine 0.6;
The preparation method of described modified asbestos powder is:
Asbestos powder is with 15% salt acid soak 3 hours, deionized water wash, then soaked 3 hours with 12% sodium hydroxide solution, then with deionized water wash to neutral, oven dry;
The tripoly phosphate sodium STPP that will be equivalent to asbestos powder weight 3% is dissolved in deionized water, add again the stearic acid monoglyceride of asbestos powder weight 3%, 2% paregal O, 3% epoxy tetrahydro-2-ethylhexyl phthalate, 3-5% aluminum oxide, 1500 rev/mins of stirrings at a high speed, obtain dispersion liquid, dispersion liquid oven dry, pulverizing namely get described modified asbestos powder;
The preparation method of described first component is:
(1) Hydroxylated acrylic resin, glycol ether acetic ester, n-butyl acetate, the ferrocene of above-mentioned weight part are put in reactor, mixed 20 minutes take rotating speed as the speed of 800 rev/mins;
(2) add Zinic stearas, the talcum powder of above-mentioned weight part, disperseed 30 minutes with the speed of 1100 rev/mins of rotating speeds;
(3) add each raw material of residue of above-mentioned weight part, mix 30 minutes take rotating speed as the speed of 800 rev/mins, namely get described first component;
Described component B is comprised of the raw material of following weight parts:
2,4 toluene diisocyanate tripolymer 70, quadrol 15, dimethylbenzene 30, trees ash 2, t-butyl hydroperoxide 0.8;
With the trees of above-mentioned weight part ash with 15% salt acid soak 4 hours, deionized water wash, then soaked 4 hours with 12% sodium hydroxide solution, then with deionized water wash to neutrality, dry, then mix with each raw material of above-mentioned weight part, remember described component B;
First and second liang of components are pressed the weight ratio of 1:1 and mix, namely get described pair of component silver color priming paint.
Performance test:
Claims (1)
1. two component silver color priming paint, is characterized in that it is comprised of first and second liang of components, and wherein the first component is comprised of the raw material of following weight parts:
Hydroxylated acrylic resin 70-78, ferrocene 4-6, talcum powder 10-15, aluminium-silver slurry 6-10, ethylene glycol ether acetate 4-7, n-butyl acetate 5-6, Zinic stearas 2-4, modified asbestos powder 1-3, vinyl three ('beta '-methoxy oxyethyl group) silane 0.8-1, Resorcinol 0.8-1, zinc dialkyl dithiophosphate 0.6-0.8, polyethyl acrylate 0.4-0.6, diethylamine 0.4-0.6;
The preparation method of described modified asbestos powder is:
With asbestos powder and the dibenzoyl peroxide of its quality 4-5%, the vinylbenzene of its quality 5-6%, the N-2-(aminoethyl of its quality 1-2%)-the 3-aminopropyl trimethoxysilane mixes, high speed 1200-1500 rev/min of stirring, ovendry power is broken into ultrafine powder, namely gets described modified asbestos powder;
The preparation method of described first component is:
(1) Hydroxylated acrylic resin, ethylene glycol ether acetate, n-butyl acetate, the ferrocene of above-mentioned weight part are put in reactor, the speed take rotating speed as 600-800 rev/min mixes 10-20 minute;
(2) add Zinic stearas, the talcum powder of above-mentioned weight part, disperseed 25-30 minute with the speed of rotating speed 900-1100 rev/min;
(3) add each raw material of above-mentioned residue, the speed take rotating speed as 600-800 rev/min mixes 20-30 minute, namely gets described first component;
Described component B is comprised of the raw material of following weight parts:
2,4 toluene diisocyanate tripolymer 65-70, quadrol 10-15, dimethylbenzene 20-30, trees ash 1-2, t-butyl hydroperoxide 0.8-1;
The trees ash of above-mentioned weight part is used 10-15% salt acid soak 3-4 hour, deionized water wash, then soaked 3-4 hour with the 10-12% sodium hydroxide solution, extremely neutral with deionized water wash again, then oven dry mixes with each raw material of above-mentioned weight part, namely gets described component B;
First and second liang of components are pressed the weight ratio of 1-1.5:1 and mix, namely get described pair of component silver color priming paint.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310038606.XA CN103087620B (en) | 2013-01-31 | 2013-01-31 | A kind of two component silver color priming paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310038606.XA CN103087620B (en) | 2013-01-31 | 2013-01-31 | A kind of two component silver color priming paint |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103087620A true CN103087620A (en) | 2013-05-08 |
| CN103087620B CN103087620B (en) | 2016-05-11 |
Family
ID=48200768
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310038606.XA Expired - Fee Related CN103087620B (en) | 2013-01-31 | 2013-01-31 | A kind of two component silver color priming paint |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103087620B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482586A (en) * | 2015-12-25 | 2016-04-13 | 北京展辰新材料有限公司 | Water-based bi-component white primer and preparation method thereof |
| CN107748163A (en) * | 2017-09-07 | 2018-03-02 | 西北农林科技大学 | Application of N (2 aminoethyl) 3 aminopropyl trimethoxysilanes in hydroquinones is detected |
| CN116535958A (en) * | 2023-05-29 | 2023-08-04 | 龙牌涂料(北京)有限公司 | Quick-drying type double-component polyurethane water-based paint and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557895A (en) * | 2004-01-17 | 2004-12-29 | 江西省横峰县旋塑防腐设备总厂 | Lasting metal corrosion-resistant paint |
| CN1986708A (en) * | 2005-12-21 | 2007-06-27 | 比亚迪股份有限公司 | Primer composition and its preparing process and use |
| CN101029197A (en) * | 2006-02-28 | 2007-09-05 | 上海捷邦精细化工有限公司 | Metal water flashing base coat of automobile |
-
2013
- 2013-01-31 CN CN201310038606.XA patent/CN103087620B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1557895A (en) * | 2004-01-17 | 2004-12-29 | 江西省横峰县旋塑防腐设备总厂 | Lasting metal corrosion-resistant paint |
| CN1986708A (en) * | 2005-12-21 | 2007-06-27 | 比亚迪股份有限公司 | Primer composition and its preparing process and use |
| CN101029197A (en) * | 2006-02-28 | 2007-09-05 | 上海捷邦精细化工有限公司 | Metal water flashing base coat of automobile |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105482586A (en) * | 2015-12-25 | 2016-04-13 | 北京展辰新材料有限公司 | Water-based bi-component white primer and preparation method thereof |
| CN107748163A (en) * | 2017-09-07 | 2018-03-02 | 西北农林科技大学 | Application of N (2 aminoethyl) 3 aminopropyl trimethoxysilanes in hydroquinones is detected |
| CN107748163B (en) * | 2017-09-07 | 2020-07-03 | 西北农林科技大学 | Application of N- (2-aminoethyl) -3-aminopropyltrimethoxysilane in detection of hydroquinone |
| CN116535958A (en) * | 2023-05-29 | 2023-08-04 | 龙牌涂料(北京)有限公司 | Quick-drying type double-component polyurethane water-based paint and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103087620B (en) | 2016-05-11 |
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