CN102232974A - Preparation method of Chinese medicinal granule for poultry - Google Patents
Preparation method of Chinese medicinal granule for poultry Download PDFInfo
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- CN102232974A CN102232974A CN2010101744294A CN201010174429A CN102232974A CN 102232974 A CN102232974 A CN 102232974A CN 2010101744294 A CN2010101744294 A CN 2010101744294A CN 201010174429 A CN201010174429 A CN 201010174429A CN 102232974 A CN102232974 A CN 102232974A
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Abstract
The invention discloses a preparation method of a Chinese medicinal granule for poultry, comprising the following steps of: preparing blank granule cores from an accessory by using a multifunctional medicinal granule granulation machine; transferring the blank granule cores into a boiling granulator; atomizing a Chinese medicine fluid extract in thermal current into fine liquid drops; coating the liquid drops on the blank granule cores layer by layer, boiling, mixing, spraying layer by layer and drying layer by layer to finally achieve the aim of micro emulsification of traditional Chinese medicine. Compared with the Chinese medicinal granule produced by the traditional Chinese medicine granulating method, the Chinese medicinal granule prepared by adopting the preparation method has the advantages of high production efficiency, higher uniformity in granularity of granules and better solubility. The traditional Chinese medicine is extracted by adopting a water decoction method; an extract solution is concentrated into the Chinese medicine fluid extract with the density of 1.08-1.11; the Chinese medicine fluid extract meets the requirement on spraying of the boiling granulator; the accessory of the granule is a water-soluble accessory; and a bonding agent for preparing the blank granule cores is a water-soluble bonding agent. The Chinese medicinal granule for poultry has favorable water solubility, can be used by drinking water and mixing materials and is convenient for farmers to use. The Chinese medicinal granule for poultry is a pure Chinese medicinal preparation and has no harm from residual medicine.
Description
Technical field
The present invention relates to the preparation method of fowl, relate to fields such as animal medicine, animal health with Chinese medicine granules.
Background technology
At present, China's animal husbandry development is rapid, fowl is already cultured to the trend of intensification, modernization development day by day ripe, in breeding process, no matter the multiple disease of fowl easy infection is prevention or treatment, and most of veterinarys are accustomed to using Western medicine on the market now, the still human clinical medicine commonly used of some Western medicine, the phenomenon that people fowl is raiseeed shared antibiotics is more serious.
Though the curative effect of Western medicine is rapid, after fowl was used Western medicine, medicine was eliminated slow in the fowl body, in Fowl meat, have residual easily, after Fowl meat entered the human foods chain, the drug residue in the Fowl meat directly influenced eater's health, and long-term edible meeting produces adverse influence to human beings'health; The drug residue problem of Fowl meat, fowl is already exported to be restricted, add the toxic and side effects of Western medicine, be difficult to satisfy the demand of foreign exchange earning and actual clinical, therefore, the drug residue problem of Fowl meat is subjected to people from all walks of life's common concern always, also is the problem that China's animal husbandry presses for solution at present.
China joins WTO now, and the outlet of poultry, fowl and milk product must be in line with international standards, and poultry, the used medicine of fowl also need strict control, the use of restriction Western medicine, and developing eutherapeutic modern Chinese medicine is the important directions of fowl medication research.
China region is wide, and natural resources of Chinese medicinal materials is abundant, and the exploitation tcm product has advantageous condition, and Chinese medicine preparation is subject to people's attention day by day.Fowl is used Chinese medicine, does not have the harm of drug residue, can prevent chemical sproof generation and chemical sproof indirect transfer; The Fowl meat export abroad of no drug residue can be earned foreign exchange, and production and marketing is pollution-free food at home, and therefore, exploitation fowl is used new product of Chinese medicine, and research fowl is a very important job with the new technology of Chinese medicine preparation.
Fowl mainly is dosage forms such as powder, oral liquid, granule with the dosage form of Chinese medicine.Studies show that in a large number Effective Components of Chinese Herb is present in the Chinese crude drug cell, directly oral Chinese medicine powder, owing to be difficult to digestion, cause effective ingredient not absorb fully and to utilize, curative effect is not obvious, Chinese powder medicine stable bad, caking easily in the storage is made troubles to the raiser; Though micronizing can make cell wall breaking, consumption is big, using method single (can only spice use), and manufacturing cost is too high, and because animal feed intake when sick descends, the Chinese medicine of micronizing also is difficult to guarantee all to enter in the fowl body.
Extract oral liquor ratio Chinese powder medicine with the obvious advantage, effective ingredient be easy to the gastral absorption of fowl, but the volume of oral liquid is big through extracting, weight is big, and transportation is difficult for, in storage process, easily mouldly lose rottenly, pH value changes easily, and effective ingredient produces degraded indirectly.In raiser's use, oral liquid can only be drunk water, and can only spice the same with Chinese powder medicine, occupation mode is restricted.
Chinese medicine granules is applicable to whole chicken group, and water-soluble back is the same with the effect of Chinese medicine oral liquid, and effective ingredient is easy to absorb, and meets the characteristics of poultry physiology digestion.Chinese medicine granules is a relevant technologies of using for reference the chemicals granule, in conjunction with a kind of preparation that the characteristics of solution dosages such as decoction, medicated wine, syrup form, has kept decoction to absorb fast, produce effects characteristics rapidly, can also cover the bitterness of Chinese medicine, the comfortable mouth of distinguish the flavor of.
Fowl is made the dosage form of granule with Chinese medicine, can guarantee effectively that Effective Components of Chinese Herb absorbs fully, good palatability, consumption is little, volume is little, be convenient to the transportation and the storage, the raiser is easy to use, drinking-water, spice all can, compare with the single usage of oral liquid, powder, the use of Chinese medicine granules is variation more; Chinese medicine is made granule, and the moisture Control strictness generally is no more than 6.0%, and moisture is low, and granule does not lump, do not go mouldy, and deliquescent probability is very little, and the stability of granule obviously is better than powder and oral liquid.
It is 1.32～1.35 thick paste that the production technology more complicated of Chinese medicine granule, Chinese medicine extraction liquid will be condensed into density earlier, and thick paste is an amount of with sucrose and dextrin again, granulates, and drying forms.The density measurement of Chinese medicine thick paste is a puzzlement problem, because of viscosity is too big, and the sampling difficulty, this moment, densimeter can't be measured the density of thick paste, can only use pycnometric determination density, measured the time-consuming length of density, and error is big.
During the actual production of Chinese medicine granule, the bad control of the viscosity of Chinese medicine thick paste, often determine by rule of thumb, cause granulating process loaded down with trivial details, poor repeatability, viscosity was big when material system wet grain, off line difficulty, the screen cloth loss phenomenon of granulation is serious, and the adhesion Chinese medical concrete is more on the granulation machine, loss is big, and it is time-consuming to clear out a gathering place; It is really up to the mark to become behind the wet grain drying, causes particulate dissolubility bad.Fowl not only requires particle integrity with Chinese medicine granules, and requires dissolubility to get well, and the amount that poultry once drinks water is fewer, and therefore middle drug solns flocculent deposit can not occur in put procedure, otherwise blocks up the water dispenser of chicken house easily.
The Chinese medicine granule uses starch to be adjuvant, though the processing ease that Chinese medicine is granulated is controlled, but the dissolubility of starch is bad, the dissolubility of making behind the granule is bad, directly influence drinking of poultry, traditional Chinese medicine method of granulating is suitable for doing the granules such as Radix Isatidis granules of human, the people can all drink slightly muddy medicinal liquid, and the poultry perfusion is relatively more difficult, particularly large-scale chicken house more can't gavage administration to each chicken, can only be mixed with medicinal liquid, allows chicken freely drink, therefore, fowl must be selected good adjuvant of dissolubility and binding agent with Chinese medicinal granule.
Chinese medicine granule method is that 100kg Chinese crude drug water decocting method extracts, and is condensed into density and is 1.32～1.35 thick paste (heavily about 30kg), adds the adjuvant granulation, gained granule gross weight 100kg, and every 100kg granule is equivalent to the 100kg crude drug; Invention preparation method is that 100kg Chinese crude drug water decocting method extracts, and is condensed into density and is 1.08～1.11 Chinese medicine fluid extract (heavily about 50kg), all sparge in the adjuvant, and gained granule gross weight 100kg, every 100kg granule is equivalent to the 100kg crude drug; Invention preparation method is consistent with the Chinese medicine content of traditional preparation process method, and every 1g Chinese medicine granules is equivalent to the 1g crude drug.
Given this, invented the preparation method of fowl with Chinese medicine granules, adopt the decocting cooking method that Chinese medicine is extracted, decoct with water each 1 hour 2 times, collecting decoction, filter, it is 1.08～1.11 Chinese medicine fluid extract that filtrate is condensed into density, and this moment, density was controlled easily, the common density meter just can be measured, and finding speed is fast; The Chinese medicine fluid extract wraps up blank particulate grain core with spray pattern, airpillow-dry, and drying time is short, and production technology is controlled easily, and is simple to operation, even particle size and complete, used boiling granulating machine is close with the price of traditional granulator.
Invention preparation method has reduced traditional granulation particulate operation of oven drying, Chinese medicine parcel and particle drying carry out simultaneously, once just can finish at an equipment, save the expense and the space of baking oven, clear out a gathering place conveniently, saved time and manpower, production capacity significantly improves, whole production period ratio traditional method shortens 30%, and production efficiency improves 20% than traditional handicraft.
Summary of the invention
The invention provides the preparation method of fowl with Chinese medicine granules.
Fowl provided by the invention with the preparation method of Chinese medicine granules is: adjuvant is made blank grain core with multi-functional electuary granulation machine earlier; change over to again in the boiling granulating machine; the Chinese medicine fluid extract is atomized into trickle drop in thermal current; be wrapped in layer by layer on the blank grain core; boiling mixes, spraying layer by layer, dry layer by layer; reach the dispersive purpose of ultra micro, the production efficiency height has solved the problem of fowl with Chinese medicine granulation difficulty.
Fowl of the present invention is used Chinese medicine granules, and every 100kg granule contains: water soluble adjuvant 70～80% (w/w), water-soluble binder 5～11% (w/w), Chinese medicine fluid extract 35～50% (w/w).
Fowl of the present invention is used the Chinese medicine fluid extract, can be the Chinese medicine of heat-clearing and toxic substances removing, removing dampness dysentery relieving, also can be the Chinese medicine of relieving the exterior syndrome with drugs of pungent in flavor and cool in nature, preventing phlegm from forming and stopping coughing, can also be the Chinese medicine or the Chinese medicine compound of tonify deficiency QI invigorating, invigorating the stomach and promoting digestion, promoting diuresis to eliminate damp pathogen, warming spleen and stomach for dispelling cold, relieving spasm to stop pain.
Fowl of the present invention is used Chinese medicine granules, adopts the decocting cooking method that Chinese medicine is extracted, and decocts with water 2 times, and each 1 hour, collecting decoction filtered, and it is 1.08～1.11 Chinese medicine fluid extract that filtrate is condensed into density, the requirement of suitable boiling granulating machine spraying.
Fowl of the present invention is used the water soluble adjuvant of Chinese medicine granules, can be in sucrose, glucose, water soluble starch, lactose, the shallow lake dimension powder one or more, preferably sucrose.
The water-soluble binder of blank grain core of the present invention can be in syrup, methylcellulose, sodium carboxymethyl cellulose, hypromellose, the polyvidone one or more, preferred syrup.
Fowl provided by the invention is used the preparation method of Chinese medicine granules, and favorable reproducibility helps industrialized mass production, the production efficiency height.Compare with the Chinese medicine method of granulating, particulate granularity is more even, dissolubility is better.
Fowl provided by the invention can strengthen the absorption and the utilization of Chinese medicine with the preparation method of Chinese medicine granules, guarantees the health of animal, has also just guaranteed human beings'health.
The specific embodiment
Example 1: fowl is used the preparation of Chinese medicine granules
Sucrose 75kg
60% syrup 9kg
Clearing away heat to cure dysentery Chinese medicine fluid extract 40kg
Granule is done back gross weight 100kg
Preparation method:
Clearing away heat to cure dysentery Chinese medicine fluid extract preparation: Rhizoma Coptidis 20kg, Cortex Phellodendri 20kg, Radix Et Rhizoma Rhei 10kg, Radix Scutellariae 20kg, Radix Isatidis 20kg, Radix Glycyrrhizae 10kg, decoct with water 2 times, each 1 hour, collecting decoction, filter, it is 1.08～1.11 Chinese medicine fluid extract (heavy 40kg) that filtrate is condensed into density
Mix: add sucrose in the trough type mixing machine, add syrup, mix homogeneously.
The blank grain of system core: multi-functional electuary granulation machine is made the blank grain of 12 purposes core.
Chinese medicine parcel and particle drying: wet granular is gone in the boiling granulating machine; carry out drying according to 60 ℃ of temperature setting; clearing away heat to cure dysentery Chinese medicine fluid extract is atomized into trickle drop in thermal current, be wrapped in layer by layer on the blank grain core, and Chinese medicine parcel and particle drying are finished simultaneously.
Granulate: dried granule carries out granulate through 10 order metallic sieves.
Example 2: fowl is used the preparation of Chinese medicine granules
Water soluble starch 15kg
Sucrose 59kg
2% methocel solution 11kg
Relieving the exterior syndrome with drugs of pungent in flavor and cool in nature Chinese medicine fluid extract 50kg
Granule is done back gross weight 100kg
Preparation method:
Relieving the exterior syndrome with drugs of pungent in flavor and cool in nature Chinese medicine fluid extract preparation: Radix Isatidis 40kg, Radix Glycyrrhizae 60kg, decoct with water 2 times, each 1 hour, collecting decoction filtered, and it is 1.08～1.11 Chinese medicine fluid extract (heavy 50kg) that filtrate is condensed into density
Mix: add water soluble starch and sucrose in the trough type mixing machine, add 2% methocel solution, mix homogeneously behind the mix homogeneously.
The blank grain of system core: multi-functional electuary granulation machine is made the blank grain of 12 purposes core.
Chinese medicine parcel and particle drying: wet granular is gone in the boiling granulating machine; carry out drying according to 60 ℃ of temperature setting; relieving the exterior syndrome with drugs of pungent in flavor and cool in nature Chinese medicine fluid extract is atomized into trickle drop in thermal current, be wrapped in layer by layer on the blank grain core, and Chinese medicine parcel and particle drying are finished simultaneously.
Granulate: dried granule carries out granulate through 10 order metallic sieves.
Example 3: fowl is used the preparation of Chinese medicine granules
Water soluble starch 35kg
Glucose 37kg
Gypsum Fibrosum (pulverizing) 10kg
5% povidone solution 10kg
Preventing phlegm from forming and stopping coughing Chinese medicine fluid extract 35kg
Granule is done back gross weight 100kg
Preparation method:
Preventing phlegm from forming and stopping coughing Chinese medicine fluid extract preparation: Herba Ephedrae 15kg, Semen Armeniacae Amarum 6kg, Radix Platycodonis 20kg, Folium Eriobotryae 15kg, Bulbus Fritillariae Uninbracteatae 6kg, Radix Peucedani 20kg, Radix Glycyrrhizae 8kg, decoct with water 2 times, each 1 hour, collecting decoction, filter, it is 1.08～1.11 Chinese medicine fluid extract (heavy 35kg) that filtrate is condensed into density
Mix: add Gypsum Fibrosum, water soluble starch and glucose in the trough type mixing machine, add 5% povidone solution, mix homogeneously behind the mix homogeneously.
The blank grain of system core: multi-functional electuary granulation machine is made the blank grain of 12 purposes core.
Chinese medicine parcel and particle drying: wet granular is gone in the boiling granulating machine; carry out drying according to 60 ℃ of temperature setting; preventing phlegm from forming and stopping coughing Chinese medicine fluid extract is atomized into trickle drop in thermal current, be wrapped in layer by layer on the blank grain core, and Chinese medicine parcel and particle drying are finished simultaneously.
Granulate: dried granule carries out granulate through 10 order metallic sieves.
The granule melting contrast of experimental example 1 invention preparation method and traditional method
This test is the melting of contrast invention preparation method and traditional preparation process method, according to " People's Republic of China's veterinary drug allusion quotation " 2005 editions two ones---the requirement of granule melting, the design experiment scheme, the clearing away heat to cure dysentery granule of traditional preparation process method is the I group, and the clearing away heat to cure dysentery granule of invention preparation method is the II group.
Melting test: get test sample 10g, add hot water 200ml, stirred 5 minutes, observe immediately, answer off-bottom or be the suspendible shape.Soluble particles is answered off-bottom, allows slight haze; Mix suspension grain is should be able to suspendible even; Effervescent granule should be able to produce gas rapidly and be the effervescent shape when meeting water.Granule all must not have foreign bodies such as breeze.Situation is dissolved in observation, the results are shown in Table 1.
The contrast of table 1 granule melting
As can be seen from Table 1, the granule dissolubility of invention preparation method is better than traditional preparation process method, places after 24 hours, and solution is still clarified, and helps drinking and absorbing of poultry.
The grain graininess contrast of experimental example 2 invention preparation methods and traditional method
This test is the grain graininess of contrast invention preparation method and traditional preparation process method, according to " People's Republic of China's veterinary drug allusion quotation " 2005 editions two ones---the requirement of granule granularity, the design experiment scheme, the clearing away heat to cure dysentery granule of traditional preparation process method is the I group, and the clearing away heat to cure dysentery granule of invention preparation method is the II group.
Granularity test: except as otherwise herein provided, measure, can not and can must not cross 15% by a sieve (10 order) by the summation of No. five sieves (80 order) according to granulometry (78 pages of appendix, second method, two sieve methods).The results are shown in Table 2.
The particulate granularity contrast of table 2
As can be seen from Table 2, the epigranular of the granule of invention preparation method greater than 10 purpose bulky grains with less than the summation of 80 purpose fine powders, is lacked than the traditional preparation process method, shows that the granule appearance character of invention preparation method is good, epigranular, and fine powder is few.
The stability contrast of experimental example 3 invention preparation methods and traditional method
This test is the stability of contrast invention preparation method and traditional preparation process method, according to " People's Republic of China's veterinary drug allusion quotation " 2005 editions an one---the requirement of veterinary drug stability test guideline, press the concrete regulation of pharmaceutical preparation under the veterinary drug stability test guideline item again, the design experiment scheme, the clearing away heat to cure dysentery granule of traditional preparation process method is the I group, and the clearing away heat to cure dysentery granule of invention preparation method is the II group.
Stability test: accelerated test and long term test
Stability high spot reviews project: character, have or not variable color, caking etc.
(1) accelerated test is by quickening the chemistry or the physical change of pharmaceutical preparation, inquiring into the stability of pharmaceutical preparation, for the data that provides necessary is improved, transports and stored to prescription design, process modification, quality research, packing.
Get each 3 batches of test I group and test II groups, commercially available back was placed 6 months under the condition of 40 ℃ ± 2 ℃ of temperature, relative humidity 75% ± 5%.Take a sample respectively once the 1st, 2,3,6 the end of month at duration of test, detect by stable high spot reviews project, with 1 batch be example the results are shown in Table 3:
The contrast of table 3 accelerated test
(2) long term test is to carry out under the actual storage requirement near medicine, its objective is that the effect duration for formulating medicine provides foundation.
Get each 3 batches of test I group and test II groups, commercially available back was placed 12 months under the condition of 25 ℃ ± 2 ℃ of temperature, relative humidity 60% ± 10%.Per 3 months the sampling once, respectively at 0,3,6,9,12 month the sampling, detect by stable high spot reviews project, with 1 batch be example the results are shown in Table 4:
The contrast of table 4 long term test
From table 3 and table 4 as can be seen, the result of accelerated test and long term test shows, the granule of invention preparation method is in the investigation condition of regulation with in the time, appearance character stable relatively good; Analyze the good reason of invention preparation granule stability, with the rare very big relation of the fine powder in the granule, just easy adhesion of Chinese medicine fine powder itself and caking, the fine powder of traditional preparation process method is many, directly influence particulate stability, invention preparation method can solve this difficult problem, and stability obviously is better than the traditional preparation process method.
Claims (7)
1. fowl is used the preparation method of Chinese medicine granules; it is characterized by: adjuvant is made blank grain core with multi-functional electuary granulation machine earlier; change over to again in the boiling granulating machine; the Chinese medicine fluid extract is atomized into trickle drop in thermal current; be wrapped in layer by layer on the blank grain core; boiling mixes, spraying layer by layer, dry layer by layer, and Chinese medicine reaches the dispersive purpose of ultra micro.Compare with the Chinese medicine method of granulating, the production efficiency height, particulate granularity is more even, dissolubility is better.
2. fowl according to claim 1 is used Chinese medicine granules, and every 100kg granule contains: water soluble adjuvant 70～80% (w/w), water-soluble binder 5～11% (w/w), Chinese medicine fluid extract 35～50% (w/w).
3. use Chinese medicine granules according to the arbitrary described fowl of claim 1-2, the Chinese medicine fluid extract can be the Chinese medicine of heat-clearing and toxic substances removing, removing dampness dysentery relieving, also can be the Chinese medicine of relieving the exterior syndrome with drugs of pungent in flavor and cool in nature, preventing phlegm from forming and stopping coughing, can also be the Chinese medicine or the Chinese medicine compound of tonify deficiency QI invigorating, invigorating the stomach and promoting digestion, promoting diuresis to eliminate damp pathogen, warming spleen and stomach for dispelling cold, relieving spasm to stop pain.
4. use Chinese medicine granules according to the arbitrary described fowl of claim 1-3, adopt the decocting cooking method that Chinese medicine is extracted, decoct with water 2 times; each 1 hour, collecting decoction filtered; it is 1.08～1.11 Chinese medicine fluid extract that filtrate is condensed into density, the requirement of suitable boiling granulating machine spraying.
5. use Chinese medicine granules according to the arbitrary described fowl of claim 1-4, the water soluble adjuvant of granule wherein can be in sucrose, glucose, water soluble starch, the lactose one or more, preferably sucrose.
6. using Chinese medicine granules according to the arbitrary described fowl of claim 1-5, wherein prepare the water-soluble binder of blank grain core, can be in syrup, methylcellulose, sodium carboxymethyl cellulose, hypromellose, the polyvidone one or more, preferred syrup.
7. the arbitrary described fowl of claim 1-6 is used the preparation method of Chinese medicine granules, its method is: water soluble adjuvant adds water-soluble binder, mix homogeneously, make blank grain core, the Chinese medicine fluid extract is atomized into drop and is wrapped on the blank grain core, Chinese medicine parcel and particle drying are finished simultaneously, obtain even-grained Chinese medicinal granule.
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| CN2010101744294A CN102232974A (en) | 2010-05-07 | 2010-05-07 | Preparation method of Chinese medicinal granule for poultry |
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| CN2010101744294A CN102232974A (en) | 2010-05-07 | 2010-05-07 | Preparation method of Chinese medicinal granule for poultry |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103405626A (en) * | 2013-07-09 | 2013-11-27 | 刘华武 | Lifei powder for livestock and poultry used in autumn |
| CN110812407A (en) * | 2019-11-22 | 2020-02-21 | 佛山市正典生物技术有限公司 | Sihuang dysentery stopping micro-capsule and preparation method thereof |
| CN111506976A (en) * | 2019-01-30 | 2020-08-07 | 北新集团建材股份有限公司 | Gypsum slurry caking analysis method and device |
-
2010
- 2010-05-07 CN CN2010101744294A patent/CN102232974A/en active Pending
Non-Patent Citations (2)
| Title |
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| 孙维广，何国熙，等: "中药颗粒剂的发展与制备工艺的改进", 《中药颗粒剂的发展与制备工艺的改进》 * |
| 张猛，范晓东，高志亮，等: "沸腾制粒技术及其应用", 《化工机械》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103405626A (en) * | 2013-07-09 | 2013-11-27 | 刘华武 | Lifei powder for livestock and poultry used in autumn |
| CN111506976A (en) * | 2019-01-30 | 2020-08-07 | 北新集团建材股份有限公司 | Gypsum slurry caking analysis method and device |
| CN111506976B (en) * | 2019-01-30 | 2022-07-26 | 北新集团建材股份有限公司 | Gypsum slurry caking analysis method and device |
| CN110812407A (en) * | 2019-11-22 | 2020-02-21 | 佛山市正典生物技术有限公司 | Sihuang dysentery stopping micro-capsule and preparation method thereof |
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Application publication date: 20111109 |