CN112293634B - Seaweed powder solid beverage and preparation method thereof - Google Patents
Seaweed powder solid beverage and preparation method thereof Download PDFInfo
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- CN112293634B CN112293634B CN201910708718.9A CN201910708718A CN112293634B CN 112293634 B CN112293634 B CN 112293634B CN 201910708718 A CN201910708718 A CN 201910708718A CN 112293634 B CN112293634 B CN 112293634B
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- 239000000843 powder Substances 0.000 title claims abstract description 96
- 241001474374 Blennius Species 0.000 title claims abstract description 66
- 239000007787 solid Substances 0.000 title claims abstract description 52
- 235000013361 beverage Nutrition 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 40
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 40
- 241001330002 Bambuseae Species 0.000 claims abstract description 40
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 40
- 239000011425 bamboo Substances 0.000 claims abstract description 40
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 25
- 239000002245 particle Substances 0.000 claims abstract description 21
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229920001100 Polydextrose Polymers 0.000 claims abstract description 8
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 claims abstract description 8
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000001259 polydextrose Substances 0.000 claims abstract description 8
- 229940035035 polydextrose Drugs 0.000 claims abstract description 8
- 235000013856 polydextrose Nutrition 0.000 claims abstract description 8
- QYSXJUFSXHHAJI-YRZJJWOYSA-N vitamin D3 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-YRZJJWOYSA-N 0.000 claims abstract description 8
- 239000000811 xylitol Substances 0.000 claims abstract description 8
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 claims abstract description 8
- 229960002675 xylitol Drugs 0.000 claims abstract description 8
- 235000010447 xylitol Nutrition 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- 235000012054 meals Nutrition 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 10
- 229910021641 deionized water Inorganic materials 0.000 claims description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 7
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- 239000007788 liquid Substances 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 239000001509 sodium citrate Substances 0.000 claims description 3
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 3
- 238000002137 ultrasound extraction Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 239000011575 calcium Substances 0.000 abstract description 49
- 229910052791 calcium Inorganic materials 0.000 abstract description 49
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 48
- 238000010521 absorption reaction Methods 0.000 abstract description 17
- 230000000694 effects Effects 0.000 abstract description 14
- 210000000988 bone and bone Anatomy 0.000 abstract description 9
- 230000009286 beneficial effect Effects 0.000 abstract description 6
- 229940069978 calcium supplement Drugs 0.000 abstract description 6
- 229910052500 inorganic mineral Inorganic materials 0.000 abstract description 6
- 239000011707 mineral Substances 0.000 abstract description 6
- 235000013305 food Nutrition 0.000 abstract description 5
- 235000016709 nutrition Nutrition 0.000 abstract description 5
- 230000035764 nutrition Effects 0.000 abstract description 5
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 229960005069 calcium Drugs 0.000 description 47
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 26
- 241000700159 Rattus Species 0.000 description 20
- 238000012360 testing method Methods 0.000 description 20
- 239000000047 product Substances 0.000 description 16
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 14
- 229910000019 calcium carbonate Inorganic materials 0.000 description 13
- 210000000689 upper leg Anatomy 0.000 description 9
- 230000037396 body weight Effects 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 239000000377 silicon dioxide Substances 0.000 description 7
- 230000037182 bone density Effects 0.000 description 6
- 235000012239 silicon dioxide Nutrition 0.000 description 6
- 230000036541 health Effects 0.000 description 5
- 235000010755 mineral Nutrition 0.000 description 5
- 241001465754 Metazoa Species 0.000 description 4
- 235000013325 dietary fiber Nutrition 0.000 description 4
- 210000003608 fece Anatomy 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000001692 EU approved anti-caking agent Substances 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
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- 244000269722 Thea sinensis Species 0.000 description 2
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- 239000003651 drinking water Substances 0.000 description 2
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- 238000011156 evaluation Methods 0.000 description 2
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- 238000009472 formulation Methods 0.000 description 2
- 150000007524 organic acids Chemical class 0.000 description 2
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- 238000010998 test method Methods 0.000 description 2
- 239000012085 test solution Substances 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- 241000251511 Holothuroidea Species 0.000 description 1
- 229920000168 Microcrystalline cellulose Polymers 0.000 description 1
- 241000227425 Pieris rapae crucivora Species 0.000 description 1
- 230000006978 adaptation Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000003321 atomic absorption spectrophotometry Methods 0.000 description 1
- 230000003139 buffering effect Effects 0.000 description 1
- FNAQSUUGMSOBHW-UHFFFAOYSA-H calcium citrate Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O.[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O FNAQSUUGMSOBHW-UHFFFAOYSA-H 0.000 description 1
- 239000001354 calcium citrate Substances 0.000 description 1
- 229960004256 calcium citrate Drugs 0.000 description 1
- 239000004227 calcium gluconate Substances 0.000 description 1
- 229960004494 calcium gluconate Drugs 0.000 description 1
- 235000013927 calcium gluconate Nutrition 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 1
- 239000001527 calcium lactate Substances 0.000 description 1
- 229960002401 calcium lactate Drugs 0.000 description 1
- 235000011086 calcium lactate Nutrition 0.000 description 1
- 230000003913 calcium metabolism Effects 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 description 1
- 230000008859 change Effects 0.000 description 1
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- 235000019634 flavors Nutrition 0.000 description 1
- 230000037406 food intake Effects 0.000 description 1
- 235000012631 food intake Nutrition 0.000 description 1
- 238000011990 functional testing Methods 0.000 description 1
- 210000004211 gastric acid Anatomy 0.000 description 1
- 238000003304 gavage Methods 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 210000000936 intestine Anatomy 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000008108 microcrystalline cellulose Substances 0.000 description 1
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- 239000011573 trace mineral Substances 0.000 description 1
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- 235000013337 tricalcium citrate Nutrition 0.000 description 1
- 230000004584 weight gain Effects 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention belongs to the technical field of foods, and particularly relates to a seaweed powder solid beverage and a preparation method thereof. The seaweed powder solid beverage comprises the following components in parts by weight: 18 to 30 portions of seaweed powder, 30 to 40 portions of polydextrose, 30 to 40 portions of xylitol, 8 to 12 portions of orange powder and microencapsulated vitamin D 3 0.0002 to 0.0007 portion of; the bamboo shoot powder anti-caking agent also comprises 5-12 parts of anti-caking agent, wherein the anti-caking agent consists of bamboo shoot powder with the particle size of 10-30 mu m and bamboo shoot powder with the particle size of 160-200 mu m. The seaweed powder solid beverage provided by the invention takes seaweed powder as a main calcium source, is scientific in compatibility, comprehensive in nutrition, capable of further improving the absorption and utilization of calcium by organisms, effectively increasing bone mineral density, remarkable in calcium supplement effect, good in anti-caking property and fluidity, easy to obtain raw materials, simple and easy to prepare, low in cost and beneficial to large-scale production.
Description
Technical Field
The invention belongs to the technical field of food, and particularly relates to a seaweed powder solid beverage and a preparation method thereof.
Background
With the improvement of living standard and the popularization of health knowledge, more and more people have come to recognize the importance of calcium supplement on body health. Calcium preparations can be divided into three categories according to the chemical composition of the calcium source: inorganic calcium, organic calcium and organic calcium. Inorganic calcium takes calcium carbonate, calcium oxide and the like as main components, and has the common characteristics of poor water solubility, difficult absorption, constipation, inappetence and the like caused by long-term taking, and a plurality of products in the current market still belong to the category. The organic acid calcium is compounded by organic acid and inorganic calcium ions, mainly comprises calcium gluconate, calcium lactate, calcium citrate and the like, and has the common characteristics of capability of dissolving in water, low calcium content and low bioavailability. The organic calcium is mainly represented by amino acid chelated calcium, has good solubility and high bioavailability, but is expensive and difficult to be enjoyed by the public.
The natural seaweed powder is rich in calcium, the calcium content is up to 35 percent, the seaweed calcium has a honeycomb type porous structure (a structure close to human skeleton), the buffering effect is excellent, the seaweed calcium is easy to rapidly dissolve and ionize in intestines and stomach, the calcium is mainly absorbed in small intestine after dissolving and ionizing in stomach, the digestion and absorption capacity of human body is improved, and the effect of neutralizing gastric acid is remarkable; the seaweed powder also contains various mineral substances and trace elements necessary for human bodies, and can further improve the absorption rate of calcium in the human bodies. Compared with mineral calcium, the seaweed calcium has higher safety, so the seaweed powder serving as a novel calcium food source can be processed into a calcium supplement product with good water solubility, high bioavailability and substantial price.
At present, calcium supplement products containing seaweed meal in the market mainly focus on swallow tablets and soft capsule formulations, the nutrition is single, the taste is monotonous, and the solid beverage has the advantages of convenience in eating, unique flavor, various varieties, convenience in carrying and the like, and is popular with consumers. However, the seaweed powder is easy to absorb moisture and wet, so that the caking phenomenon is easy to occur in the processing and storage processes of the existing seaweed powder solid beverage, the quality of the product is seriously influenced, the feedback experience of consumers can not find that the caking is a serious disaster area of the solid beverage complained in the shelf life, although the caking of the product can be prevented by adding the anticaking agents such as silicon dioxide, microcrystalline cellulose and the like, the health of a human body is influenced by excessive intake of the anticaking agents.
Therefore, the seaweed powder solid beverage which is not easy to absorb moisture and block and does not contain anticaking agents such as silicon dioxide and the like, and has high bioavailability and low price is urgently needed.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide a seaweed powder solid beverage and a preparation method thereof. The seaweed powder solid beverage provided by the invention takes the seaweed powder as a main calcium source, has scientific compatibility and comprehensive nutrition, further improves the absorption and utilization of calcium by organisms, effectively increases the bone mineral density, has obvious calcium supplement effect, has good anti-caking property and fluidity, is easy to obtain raw materials, is simple and easy to prepare, has lower cost and is beneficial to realizing large-scale production.
The invention provides a seaweed powder solid beverage which comprises the following components in parts by weight: 18 to 30 portions of seaweed powder, 30 to 40 portions of polydextrose, 30 to 40 portions of xylitol, 8 to 12 portions of orange powder and microencapsulated vitamin D 3 0.0002 to 0.0007 portion.
Further, the seaweed powder solid beverage comprises the following components in parts by weight: 21 parts of seaweed powder, 34 parts of polydextrose, 35 parts of xylitol, 10 parts of orange powder and microencapsulated vitamin D 3 0.0006 part.
Further, the seaweed powder solid beverage also comprises 5-12 parts of an anticaking agent.
Further, the anticaking agent consists of bamboo shoot powder with the grain diameter of 10-30 mu m and bamboo shoot powder with the grain diameter of 160-200 mu m.
Further, the mass ratio of the bamboo shoot powder with the particle size of 10-30 microns to the bamboo shoot powder with the particle size of 160-200 microns is 1.
Further, the preparation method of the bamboo shoot powder comprises the following steps:
drying and crushing bamboo shoots, adding deionized water according to the mass ratio of feed liquid of 1-50, adding 0.8-1.2 mol/L sodium citrate solution to adjust the pH value to 4-5, carrying out ultrasonic extraction for 15-25 min at the temperature of 60-80 ℃ and the power of 300-500W, centrifuging, and taking supernatant; adjusting the pH value of the supernatant to 8-9 by using 0.05-0.15 mol/L NaOH solution, centrifuging, and taking the precipitate; washing the precipitate with deionized water to neutrality, oven drying, and pulverizing.
Meanwhile, the invention also provides a preparation method of the seaweed powder solid beverage, which comprises the following steps:
s1, microencapsulating vitamin D 3 Mixing with polydextrose to obtain premix;
s2, adding the premix, the seaweed meal, the xylitol, the orange meal and the anticaking agent into a mixer to be uniformly mixed, sieving, and packaging.
The existing seaweed powder solid beverage is easy to absorb moisture and damp, and particularly, the seaweed calcium serving as an effective component in the seaweed powder solid beverage is of a fluffy honeycomb type porous structure, so that the seaweed powder solid beverage is easier to absorb moisture and damp, the existing seaweed powder solid beverage is easy to agglomerate, and the quality of the product is influenced. The inventor tries to add the anticaking agent silicon dioxide, which can effectively prevent the product from caking, but the powder has overlarge flowability and is not beneficial to the flow rate control of the product production package, and the health of a human body is influenced by excessive intake of the anticaking agent.
The invention surprisingly discovers that the bamboo shoot powder which is usually used as dietary fiber food is added as an anticaking agent, so that the hygroscopicity and the fluidity of the product can be improved simultaneously, the problem that the product absorbs moisture and is agglomerated is avoided, and the fluidity of the product just meets the requirements of the production and packaging conditions of the solid beverage. A large number of creative tests show that the effect is related to the configuration and the particle size of the bamboo shoot powder, and the anticaking agent consisting of the bamboo shoot powder with the particle size of 10-30 mu m and the bamboo shoot powder with the particle size of 160-200 mu m according to the mass ratio of 1-1.5 has remarkable effects of improving the anticaking property and the fluidity of the seaweed powder solid beverage.
The above effects are presumably caused by the fact that the bamboo shoot powder contains a large amount of dietary fibers after the acid-base extraction, and the fiber surface has irregular surface morphology such as many cracks and pores, which increases the specific surface area of the bamboo shoot powder particles. The normal bamboo shoot powder dietary fiber is a compact long-chain structure, and the bamboo shoot powder with the particle size of 10-30 mu m destroys the long-chain structure of the fiber, so that the whole structure of the bamboo shoot powder becomes bulky and porous, the specific surface area is increased, the moisture absorption of the bamboo shoot powder is further improved, but the water holding capacity is poor due to the excessively small particle size; the dietary fiber in the bamboo shoot powder with the grain diameter of 160-200 mu m can keep a relatively intact long chain structure, and the moisture absorption effect is not better than that of the bamboo shoot powder with the grain diameter of 10-30 mu m, but the water holding capacity is better. The combination of the two bamboo shoot powders with different particle sizes can ensure that the anti-caking agent bamboo shoot powder has extremely strong moisture absorption capacity and water holding capacity, on one hand, the anti-caking agent bamboo shoot powder can effectively prevent the solid beverage matrix from absorbing moisture, and on the other hand, the anti-caking agent bamboo shoot powder can be effectively prevented from being desorbed, so that the anti-caking property of the product is remarkably improved. In addition, the bamboo shoot powder with the particle size of 10-30 μm has extremely strong adsorbability, and the characteristic can lead the bamboo shoot powder to be adsorbed on the surface of solid beverage powder particles, especially the surface of seaweed calcium with a honeycomb type porous structure, reduce the specific surface area of the powder particles and improve the flowability of products.
The invention has the beneficial effects that:
1. the natural seaweed meal is used as a main calcium source, the compatibility is scientific, the nutrition is comprehensive, the components interact with each other, the absorption and the utilization of the organism to calcium are further improved, the bone mineral density is effectively increased, the calcium supplement effect is obvious, and safe and well-absorbed dietary nutrition supplement food is provided for consumers.
2. The anti-caking agent prepared by the bamboo shoot powder with two different particle sizes is added, so that the anti-caking property and the fluidity of the seaweed powder solid beverage can be effectively improved, the seaweed powder solid beverage is good in taste and is more easily accepted by consumers.
3. The seaweed powder solid beverage provided by the invention is simple in preparation method, easy in raw material obtaining, low in cost and beneficial to large-scale production.
Detailed Description
The present invention will be described in further detail with reference to the following examples. It should not be understood that the scope of the above-described subject matter of the present invention is limited to the following examples.
Example 1 preparation method of bamboo shoot powder
Drying and crushing bamboo shoots, adding deionized water according to the mass ratio of the feed liquid of 1 to 40, adding 1.0mol/L sodium citrate solution to adjust the pH value to 4, carrying out ultrasonic extraction for 20min at the temperature of 70 ℃ and the power of 400W, centrifuging, and taking supernatant; adjusting the pH value of the supernatant to 9 by using 0.1mol/L NaOH solution, centrifuging, and taking a precipitate; washing the precipitate with deionized water to neutrality, oven drying, and pulverizing into bamboo shoot powder with particle sizes of 10, 30, 160, 180 and 200 μm.
Example 2 to 4A seaweed powder solid beverage
TABLE 1 seaweed powder solid beverage formulation and amount (parts) thereof of inventive examples 2-4
The preparation method of the seaweed powder solid beverage comprises the following steps:
s1, microencapsulating vitamin D 3 Mixing with polydextrose to obtain premix;
s2, adding the premix, the seaweed powder, the xylitol, the orange powder and the anticaking agent into a mixer, uniformly mixing, sieving by a 60-mesh sieve, and packaging to obtain the sea cucumber feed.
Comparative example 1 seaweed meal solid drink
The difference from example 4 is that no anticaking agent was added, and the remaining components and preparation method refer to example 4.
Comparative example 2 seaweed powder solid beverage
The difference from example 4 is that the anti-caking agent was bamboo shoot powder having a particle size of 180 μm, and the remaining components and the preparation method thereof were referred to example 4.
Comparative example 3 seaweed powder solid beverage
The difference from the example 4 is that the anti-caking agent is bamboo shoot powder with the grain diameter of 10 μm, and the rest components and the preparation method refer to the example 4.
Comparative example 4 seaweed meal solid drink
The difference from the embodiment 4 is that silicon dioxide is used for replacing bamboo shoot powder, the using amount of the silicon dioxide is 0.5 part, and the rest components and the preparation method refer to the embodiment 4.
Test example 1 evaluation of Effect of increasing bone Density
Animal experiments were conducted according to the functional test method for increasing bone mineral density and calcium absorption experiments in the "health food test and evaluation technical Specification" (2003 edition of Ministry of health).
1. Test materials:
1.1 test samples and materials:
the seaweed powder solid beverages prepared in examples 2 to 4 were used as samples; in the test, 50 SPF healthy weaning rats (4 weeks old) are selected, the weight of the rats is 70-80 g, the temperature of a feeding room is 20-25 ℃, and the relative humidity is 40-70%.
1.2 dose design: the recommended dose of the seaweed powder solid beverage for adults (the weight is 60 kg) to take per day is 8g/60kg.BW, the pharmacological experiment methodology compiled by professor of xu tert-yun is referred to, the equivalent dose ratio between human and animals according to the conversion of the body surface area is 6.17, and the dose of the groups of examples 2-4 is 0.82g/kg.BW. A basal feed group was set, and a calcium carbonate control group (calcium level was the same as that of example 4 group).
1.3 sample preparation: adding deionized water to 10mL of the seaweed powder solid beverage prepared in the embodiment 2-4, and uniformly preparing a test solution; dissolving calcium carbonate in 10ml of ionized water, and uniformly mixing to prepare a calcium carbonate control group test solution. Each group of drinking water was deionized water.
2. The test method comprises the following steps:
after one week of adaptation period, weaning rats born for 4 weeks were fasted for 12 hours and weighed, and immediately grouped according to body weight, 10 rats in each group were raised in cages. Deionized water was drunk to avoid calcium pick-up from drinking water. Gavage and sample feeding are carried out once a day, deionized water is fed to the basal feed group, and the other groups are fed with samples according to dosage design for 3 months. Body weight and body length were recorded once a week for each group of animals. During this period, all the test rats were fed 6g of normal feed per day, 3 times per day.
3. Calcium absorption test
Performing calcium metabolism test for 3 days after feeding for 3 weeks, recording food intake for 3 days, collecting feces for 72 hours, oven drying the rat feces sample in a 105 deg.C oven, cooling in a drier, and grinding; feed samples were mixed evenly and sieved through a 20 mesh sieve. The calcium content in the feed and the excrement is measured by an atomic absorption spectrophotometry.
Calculated according to the following formula:
calcium intake (mg/d) = calcium content in feed (mg/g) × feed consumption (g/d),
fecal calcium (mg/d) = calcium content in feces (mg/g) × feces excretion (g/d),
apparent absorption rate of calcium = (calcium intake-calcium faecal)/calcium intake × 100%.
4. Measuring the bone density of the femur:
after feeding for 3 months, sacrificed, rats were dissected, the left femur was dissected, the femur was baked to constant weight, and the dry weight of the femur was measured. The Discovery-wi type bone densitometer is used for measuring the bone density of the midpoint of the femur and the distal end of the femur of a rat, and the bone calcium content is measured by an atomic absorption method.
5. The data statistical method comprises the following steps:
performing mean comparison by adopting single-factor variance analysis in SPSS10.0 statistical software, and performing pairwise comparison by using an LSD (least squares) method when variances are uniform; when the variance is uneven, the Tamhane method is adopted for pairwise comparison among the groups.
6. And (3) test results:
6.1 Effect of seaweed powder solid drink of the invention on rat body weight
As can be seen from table 2, the weight average of the test precursors of the rats in the groups of examples 2 to 4 was not significantly different from that of the basal feed group and the calcium carbonate control group, and the weight average of the body of the rats in the groups of examples 2 to 4 was significantly increased after the test (p < 0.05).
Table 2 Effect of seaweed powder solid drink of the present invention on rat body weight
Group of | Animal number (only) | Body weight (g) before test | Test for terminal body weight (g) | Weight gain (g) |
Basal feed group | 10 | 72.3±5.8 | 437.2±24.7 | 364.9±33.6 |
Calcium carbonate control group | 10 | 70.4±3.2 | 472.1±31.3 | 401.7±36.2 |
EXAMPLE 2 group | 10 | 70.3±2.4 | 504.3±23.4 #* | 434.0±27.4 #* |
EXAMPLE 3 group | 10 | 71.2±5.6 | 507.6±29.8 #* | 436.4±29.5 #* |
EXAMPLE 4 group | 10 | 73.6±3.1 | 519.4±33.8 #* | 445.8±31.1 #* |
Note: comparison with basal feed group: # p is less than 0.05; comparison with calcium carbonate control: * p<0.05。
6.2 Effect of seaweed powder solid beverage of the invention on calcium absorption of rats
As can be seen from table 3, there was no significant difference in the body weight and body length before the test in the rats of examples 2 to 4, and there was a significant increase in the body weight and body length after the test in the rats of examples 2 to 4 (p < 0.05); meanwhile, the expressed absorption rates of the calcium of the rats in the groups 2 to 4 are higher than those of the basal feed group and the calcium carbonate control group, and the difference is significant (p is less than 0.05), which shows that the seaweed meal solid beverage has higher calcium absorption rate and is better than that of the calcium carbonate control group.
Table 3 influence of seaweed powder solid drink of the present invention on calcium absorption of rats
Note: comparison with basal feed group: # p is less than 0.05; comparison with calcium carbonate control: * p<0.05。
6.3 Effect of seaweed powder solid beverage of the invention on rat femur Dry weight, bone Density and bone calcium content
As can be seen from Table 4, after the test, the dry weight of femur, bone density and bone calcium content of the rats in the groups of examples 2-4 are significantly increased (p is less than 0.05) compared with the basal feed group and the calcium carbonate control group, which indicates that the seaweed meal solid beverage of the invention has a significant calcium supplementing effect and is superior to the calcium carbonate control group.
Table 4 influence of seaweed powder solid drink of the present invention on rat femur dry weight, bone density and bone calcium content
Note: comparison with basal feed group: # p is less than 0.05; comparison with calcium carbonate control: * p<0.05。
test example 2, general Performance test
1. Test materials: seaweed meal solid beverages prepared in examples 2 to 4 and comparative examples 1 to 4.
2. The test method comprises the following steps:
(1) Anti-caking property: each group is sampled for 500g, and the samples are respectively sealed and packaged by common white plastic bags, each bag is 25g, and each group has 20 bags. Placing the bagged tea for 3 months under the conditions that the temperature is 40 ℃ and the humidity is 75%, randomly taking out 5 bags of samples from each group when the bagged tea is placed for 0, 10, 30 and 90 days, sieving the samples by a 60-mesh sieve, and calculating the caking rate.
Caking = product mass left on screen/product mass x 100%.
(2) Fluidity: angle of repose injection, 50g of each group of samples are respectively dropped onto a horizontally placed flat plate along a funnel, after the samples completely drop, the included angle between the inclined plane of the sample pile on the flat plate and the flat plate is tested and recorded as the angle of repose, the operation is repeated three times, and the average value is taken.
3. And (3) test results: the results of the conventional performance tests are shown in Table 5.
TABLE 5 results of conventional Performance test
As can be seen from Table 3, on day 90, the samples of examples 2 to 4 and comparative examples 1 to 3 all showed caking, but the samples of examples 2 to 4 had a very low caking rate and a comparable anti-caking ability to that of conventional anti-caking agent silica.
The flowability of the samples in the groups 2 to 4 is obviously superior to that of the samples in the groups 1 to 3 in the comparative examples, which shows that the anti-caking agent prepared by the invention can obviously improve the flowability of the seaweed powder solid beverage; however, the flowability of the samples in the groups 2 to 4 is lower than that of the sample in the comparative example 4, which shows that the flow-aiding effect of the anticaking agent prepared by the invention is not as good as that of silicon dioxide, however, in the preparation process of the solid beverage, the flowability of the powder is too large, which is not beneficial to the flow rate control of the production package of the product, and the anticaking agent prepared by the invention just meets the requirements of the production package conditions of the solid beverage.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Those skilled in the art can modify or change the above-described embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.
Claims (3)
1. The seaweed meal solid beverage is characterized by comprising the following components in parts by weight: 18 to 30 portions of seaweed powder, 30 to 40 portions of polydextrose, 30 to 40 portions of xylitol, 8 to 12 portions of orange powder and microencapsulated vitamin D 3 0.0002 to 0.0007 part and 5 to 12 parts of an anticaking agent, wherein the anticaking agent is composed of bamboo shoot powder with the particle size of 10 to 30 microns and bamboo shoot powder with the particle size of 160 to 200 microns, the mass ratio of the bamboo shoot powder with the particle size of 10 to 30 microns to the bamboo shoot powder with the particle size of 160 to 200 microns is 1 to 1.5, and the preparation method of the bamboo shoot powder comprises the following steps:
drying and crushing the bamboo shoots, adding deionized water according to the mass ratio of the feed liquid of 1 to 50, then adding 0.8 to 1.2mol/L sodium citrate solution to adjust the pH value to 4 to 5, carrying out ultrasonic extraction for 15 to 25min under the conditions that the temperature is between 60 and 80 ℃ and the power is between 300 and 500W, centrifuging, and taking supernatant; adjusting the pH value of the supernatant to 8-9 by using 0.05-0.15 mol/L NaOH solution, centrifuging, and taking the precipitate; washing the precipitate with deionized water to neutrality, oven drying, and pulverizing.
2. The seaweed meal solid beverage according to claim 1, characterized by comprising the following components in parts by weight: 21 parts of seaweed powder, 34 parts of polydextrose, 35 parts of xylitol, 10 parts of orange powder and microencapsulated vitamin D 3 0.0006 part.
3. A method for preparing a seaweed meal solid beverage according to claim 1 or 2, characterized in that it comprises the following steps:
s1, microencapsulating vitamin D 3 Mixing with polydextrose uniformly to obtain premix;
s2, adding the premix, the seaweed meal, the xylitol, the orange meal and the anticaking agent into a mixer to be uniformly mixed, sieving, and packaging.
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