CN102228413B - Lipstick and its preparation method - Google Patents
Lipstick and its preparation method Download PDFInfo
- Publication number
- CN102228413B CN102228413B CN201110178437A CN201110178437A CN102228413B CN 102228413 B CN102228413 B CN 102228413B CN 201110178437 A CN201110178437 A CN 201110178437A CN 201110178437 A CN201110178437 A CN 201110178437A CN 102228413 B CN102228413 B CN 102228413B
- Authority
- CN
- China
- Prior art keywords
- wax
- mastic
- silica gel
- temperature
- essence
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a lipstick and its preparation method, which comprises the steps of: (1) weighing the raw materials; (2) mixing a pigment with titanium dioxide and stirring them well, then adding octyl palmitate and mixing well; (3) mixing wax, body oil and vitamin E and heating the mixture; (4) stirring the mixture from step (2) and the mixture from step (3) well, adding hydrophobic silica, silicon-treated mica powder and pearl powder and mixing uniformly; (5) cooling the mixture of the last step and adding essence; (6) cooling the newly obtained mixture to a temperature of 40 DEG C, and discharging the materials, thus obtaining paste body; (7) preheating a silica gel mold to a temperature that is 4-5 DEG C higher than the dropping temperature of the paste body, filling the paste body heated to a temperature of 75-105 DEG C into the silica gel mold, cooling the silica gel mold rapidly, and when the temperature of the paste body falls below a dropping point and the paste body takes form, demolding in vacuum and packing the paste body. Being heat-resisting, the lipstick of the invention provides a solution to the problem that lipsticks are likely to "perspire" at a high temperature, thus the quality of finished products are ensured. Meanwhile, the lipstick provided in the invention is also suitable for consumers in high temperature areas.
Description
Technical field
The invention belongs to the daily cosmetics field, relate to a kind of lip pomade of not diaphoresis at high temperature particularly.
Background technology
The lip pomade industry standard is defined in 45 ± 1 ℃ and keeps 24h, return to room temperature after outward appearance do not have significant change, can normally use.But commercially available most of lip pomades are keeping the bright moisturizing effect that takes into account simultaneously; And high-load colorant and high-load humidizer can destroy the structure of lip pomade mastic; Cause in the constituent wax and greasy binding ability poor; When temperature was elevated to 45 ± 1 ℃, oils and fats was exuded to the lip pomade surface from lip pomade inside, " diaphoresis " phenomenon promptly occurred.The lip pomade in a single day quality of " diaphoresis " its product changes, and makes client be difficult to accept.
Lip pomade is perspired, and the science, the filling mould mode of lip pomade and cooling condition are not one of influence factors yet for wax and greasy proportioning in prescription.
Summary of the invention
The objective of the invention is to overcome deficiency of the prior art, a kind of lip pomade that also can " diaphoresis " in the time of 50 ± 1 ℃ is provided.
Second purpose of the present invention provides a kind of method for preparing of lip pomade.
Technical scheme of the present invention is summarized as follows:
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: wax 5-20%, octyl palmitate 6.5-10%, skin moistening oils and fats 13.5-25%, hydrophobic silica 2-12%, silicon are handled mica powder 9-10%, pearl essence 15-20%, vitamin E .1-5%, titanium dioxide 8-10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 4-5 ℃ of mastic titre,, said silica gel mould is placed 0-2 ℃ environment cooling rapidly down being heated in 75 ℃-105 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Said wax is that paraffin, Cera Flava, microwax, Brazil wax, candelilla wax, Tissuemat E, Japan wax and Ka Naba wax are at least a.
Said skin moistening oils and fats is at least four kinds of squalane, glycerol three monooctyl esters, glycerol ester in three last of the ten Heavenly stems, glycerol three iso stearyl esters, glycerol three adipate esters, isopropyl palmitate, three benzenetricarboxylic acids, 13 esters, isononyl isononanoate, isostearic acid isopropyl ester, Oleum Ricini, octyldodecanol and oleyl alcohol.
The lip pomade of above-mentioned method for preparing preparation.
Advantage of the present invention is;
Lip pomade of the present invention has heat-stable characteristics; When temperature is elevated to 45 ± 1 ℃, even can " not perspire " during to 50 ± 1 ℃, solve the difficult problem of high temperature lip pomade " perspiration "; Make the skin moistening composition be locked in the structure of forming by wax, ester etc. the better protection lips firmly.Guarantee the quality of finished product, also be fit to the use of high temperature area consumer simultaneously.
The specific embodiment
Following embodiment can make those skilled in the art understand the present invention better, but does not limit the present invention in any way.
Below in conjunction with specific embodiment the present invention is further described.
Embodiment 1
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: wax 10% (wherein: Brazil wax 2%, Cera Flava 6%, Japan wax 1%, Tissuemat E 1%), octyl palmitate 10%, skin moistening oils and fats 18% (wherein: glycerol three monooctyl esters 3%, squalane 5%, isopropyl palmitate 4%, octyldodecanol 6%), hydrophobic silica 12%, silicon are handled mica powder 10%, pearl essence 20%, vitamin E 5%, titanium dioxide 10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 5 ℃ of mastic titres,, said silica gel mould is placed 1 ℃ environment cooling rapidly down being heated in 85 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Embodiment 2
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: Brazil wax 5%, octyl palmitate 10%, skin moistening oils and fats 23% (wherein: three benzenetricarboxylic acids, 13 esters 9.5%, squalane 3%, isopropyl palmitate 4%, octyldodecanol 3.5%, Oleum Ricini 3%), hydrophobic silica 12%, silicon are handled mica powder 10%, pearl essence 20%, vitamin E 5%, titanium dioxide 10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 4 ℃ of mastic titres,, said silica gel mould is placed 2 ℃ environment cooling rapidly down being heated in 75 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Embodiment 3
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: wax 20% (wherein: Brazil wax 3%, Ka Naba wax 4%, microwax 4%, Cera Flava 9%), octyl palmitate 10%, skin moistening oils and fats 25% (wherein: glycerol ester in three last of the ten Heavenly stems 7%, glycerol three iso stearyl esters 6%, glycerol three adipate esters 7%, isononyl isononanoate 5%), hydrophobic silica 2%, silicon are handled mica powder 10%, pearl essence 15%, vitamin E 5%, titanium dioxide 8%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 5 ℃ of mastic titres,, said silica gel mould is placed 0 ℃ environment cooling rapidly down being heated in 105 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Embodiment 4
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: wax 15% (wherein: candelilla wax 4%, paraffin 3%, Tissuemat E 2%, Cera Flava 6%), octyl palmitate 6.5%, skin moistening oils and fats 23.5% (wherein: three benzenetricarboxylic acids, 13 esters 4%, isostearic acid isopropyl ester 6.5%, isopropyl palmitate 7%, oleyl alcohol 6%), hydrophobic silica 10%, silicon are handled mica powder 9%, pearl essence 20%, vitamin e1 %, titanium dioxide 10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 5 ℃ of mastic titres,, said silica gel mould is placed 2 ℃ environment cooling rapidly down being heated in 80 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Embodiment 5
A kind of method for preparing of lip pomade comprises the steps:
(1) take by weighing following raw material by mass percentage: wax 14.5% (wherein: candelilla wax 4%, paraffin 3%, Tissuemat E 2.5%, Cera Flava 5%), octyl palmitate 10%, skin moistening oils and fats 13.5% (wherein: three benzenetricarboxylic acids, 13 esters 1%, isostearic acid isopropyl ester 2.5%, isopropyl palmitate 5%, oleyl alcohol 5%), hydrophobic silica 12%, silicon are handled mica powder 10%, pearl essence 20%, vitamin E 5%, titanium dioxide 10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 4 ℃ of mastic titres,, said silica gel mould is placed 0 ℃ environment cooling rapidly down being heated in 90 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing.
Test:
Each 10 of the lip pomades of embodiment 1-embodiment 5 preparations are placed within 24 hours at 50 ℃ respectively, " diaphoresis " phenomenon do not occurred.And this heat resistant test extended to 3 months, " diaphoresis " phenomenon also appears.
Every kind each 10 of the lip pomades of two kinds of certain commercially available domestic brands, wherein a kind of 50 ℃ of placements 24 hours, wherein 100% " diaphoresis " phenomenon occurs.Another kind of placement 24 hours, 50 ℃ of 100% appearance " diaphoresis " phenomenon.
Claims (2)
1. the method for preparing of a lip pomade is characterized in that comprising the steps:
(1) take by weighing following raw material by mass percentage: wax 5-20%, octyl palmitate 6.5-10%, skin moistening oils and fats 13.5-25%, hydrophobic silica 2-12%, silicon are handled mica powder 9-10%, pearl essence 15-20%, vitamin E .1-5%, titanium dioxide 8-10%, pigment 3% and essence 2%;
(2) said pigment and titanium dioxide mixing are stirred, add octyl palmitate, mix homogeneously, subsequent use;
(3) said wax, skin moistening oils and fats, vitamin E are mixed, be heated to 85 ℃;
(4) material of step (2) acquisition and the material of step (3) acquisition are stirred, add said hydrophobic silica, silicon processing mica powder and pearl essence mix homogeneously;
(5) be cooled to 45 ℃ after, add essence;
(6) continue to be cooled to 40 ℃, discharging gets mastic;
(7) silica gel mould is preheated to is higher than 4-5 ℃ of mastic titre,, said silica gel mould is placed 0-2 ℃ environment cooling rapidly down being heated in 75 ℃-105 ℃ mastic fill to the said silica gel mould; Treating that the mastic temperature drops to is lower than dropping point; After the mastic molding, the vacuum demoulding, packing;
Said wax is that paraffin, Cera Flava, microwax, Brazil wax, candelilla wax, Tissuemat E, Japan wax and Ka Naba wax are at least a;
Said skin moistening oils and fats is at least four kinds of squalane, glycerol three monooctyl esters, glycerol ester in three last of the ten Heavenly stems, glycerol three iso stearyl esters, glycerol three adipate esters, isopropyl palmitate, three benzenetricarboxylic acids, 13 esters, isononyl isononanoate, isostearic acid isopropyl ester, Oleum Ricini, octyldodecanol and oleyl alcohol.
2. the lip pomade of the method for preparing of claim 1 preparation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110178437A CN102228413B (en) | 2011-06-29 | 2011-06-29 | Lipstick and its preparation method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110178437A CN102228413B (en) | 2011-06-29 | 2011-06-29 | Lipstick and its preparation method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102228413A CN102228413A (en) | 2011-11-02 |
| CN102228413B true CN102228413B (en) | 2012-10-24 |
Family
ID=44841048
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110178437A Expired - Fee Related CN102228413B (en) | 2011-06-29 | 2011-06-29 | Lipstick and its preparation method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102228413B (en) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102697700B (en) * | 2012-07-05 | 2013-05-22 | 吴慧萍 | Jasmine-fragrance-type lipstick and preparation method thereof |
| CN102697676B (en) * | 2012-07-05 | 2013-06-19 | 张燕梅 | Jasmine-fragrance-type lipstick and preparation method thereof |
| US10064810B2 (en) * | 2014-05-01 | 2018-09-04 | Avon Products, Inc. | Matte cosmetic compositions |
| CN104161697A (en) * | 2014-05-21 | 2014-11-26 | 厦门中妍生物科技有限公司 | Radix Pseudostellariae-based youthful look preserving and skin caring product and preparation method thereof |
| CN104606120A (en) * | 2015-02-13 | 2015-05-13 | 南通蛇类治疗研究所 | Nanometer negative ion natural plant lipstick |
| CN106137795B (en) * | 2016-08-15 | 2020-04-17 | 广州澳希亚实业有限公司 | Composition for inhibiting sweating of lip balm and repairing lip injury |
| CN106377441A (en) * | 2016-11-01 | 2017-02-08 | 山东大学 | Cup-staining-free lipstick and preparation method thereof |
| CN109199912A (en) * | 2017-06-29 | 2019-01-15 | 济南惠农玫瑰花精油有限公司 | A kind of rose lipstick and preparation method thereof |
| CN108498373B (en) * | 2018-05-04 | 2020-05-22 | 深圳市兰亭科技股份有限公司 | Lip cosmetic and preparation method thereof |
| CN108553321B (en) * | 2018-05-09 | 2021-08-10 | 重庆医药高等专科学校 | Pearlescent lipstick and preparation method thereof |
| CN110917082A (en) * | 2018-09-20 | 2020-03-27 | 中华全国供销合作总社南京野生植物综合利用研究所 | Lipstick containing lacquer wax and lacquer seed oil chilli red |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1135171A (en) * | 1993-10-18 | 1996-11-06 | 普罗克特和甘保尔公司 | Non-sweating lipsticks |
| CN1192133A (en) * | 1995-05-31 | 1998-09-02 | 普罗克特和甘保尔公司 | Transfer-resistant lip compositions |
| CN1344148A (en) * | 1999-02-12 | 2002-04-10 | 宝洁公司 | Cosmetic compsns. contg. vitamin B3 |
-
2011
- 2011-06-29 CN CN201110178437A patent/CN102228413B/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1135171A (en) * | 1993-10-18 | 1996-11-06 | 普罗克特和甘保尔公司 | Non-sweating lipsticks |
| CN1192133A (en) * | 1995-05-31 | 1998-09-02 | 普罗克特和甘保尔公司 | Transfer-resistant lip compositions |
| CN1344148A (en) * | 1999-02-12 | 2002-04-10 | 宝洁公司 | Cosmetic compsns. contg. vitamin B3 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102228413A (en) | 2011-11-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102228413B (en) | Lipstick and its preparation method | |
| EP2273972B1 (en) | Ternary and quaternary wax-resin composites for use in cosmetic and pharmaceutical preparations | |
| CN1332647C (en) | Lipid preparation, particularly cosmetic preparation | |
| CN109125138A (en) | A kind of lipstick and preparation method thereof of moist high glaze | |
| CN104902868A (en) | Solid powder cosmetic | |
| CN107375037A (en) | A kind of color-changing lipstick and preparation method thereof | |
| CN106309288A (en) | Cross color-preventive and easily produced discoloring lipstick | |
| CN104352361A (en) | Variable-colour transparent lipstick and preparation method thereof | |
| CN109864896A (en) | A kind of lipstick Combined raincoat object of Anti-fade and preparation method thereof | |
| CN105616208B (en) | A kind of aqueous full oil base color make-up composition and preparation method thereof | |
| CN110960449B (en) | Smooth lipstick and its production process | |
| CN111671676A (en) | Moisturizing aromatic lip balm and preparation method thereof | |
| CN103239367A (en) | Baking powder and preparation method thereof | |
| CN103200928B (en) | Resistance to de-cosmetics and preparation method thereof | |
| CN104546561A (en) | Three-dimensional molding wax oil powder and preparation method thereof | |
| CN110267642A (en) | Oily composition, its preparation method, oiliness base and skin preparations for extenal use | |
| CN109381379B (en) | Stick lipstick and preparation method thereof | |
| CN111110599A (en) | Transparent makeup removing cream, preparation method thereof and double-head product | |
| CN104739735A (en) | Lip protection oil and preparation method thereof | |
| KR20130122232A (en) | Powder composition with good coverage and moisturizing effects | |
| CN109172424A (en) | A kind of preparation method of shea butter cream | |
| CN107049891A (en) | A kind of lip gloss and preparation method thereof | |
| CN103536461B (en) | A kind of Oleum Vitis viniferae skin care cream and preparation method thereof | |
| CN104739702A (en) | Protection lip gloss and preparation method thereof | |
| CN110755276A (en) | Moisturizing and fixing honey powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Free format text: FORMER OWNER: TIANJIN TIANSHI BIOLOGICAL DEVELOPMENT CO., LTD. TIENS GROUP CO., LTD. Effective date: 20140328 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20140328 Address after: 301700, No. 18, Xinyuan Road, Wuqing Development Zone, Tianjin Patentee after: TIANJIN TIANSHI BIOLOGICAL DEVELOPMENT Co.,Ltd. Address before: 301700, No. 18, Xinyuan Road, Wuqing Development Zone, Tianjin Patentee before: TIANJIN TIANSHI BIOLOGICAL DEVELOPMENT Co.,Ltd. Patentee before: TIANJIN TIANSHI LIFE-RESOURCES Co.,Ltd. Patentee before: TIENS GROUP Co.,Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121024 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |