CN106377441A - Cup-staining-free lipstick and preparation method thereof - Google Patents

Cup-staining-free lipstick and preparation method thereof Download PDF

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Publication number
CN106377441A
CN106377441A CN201610941904.3A CN201610941904A CN106377441A CN 106377441 A CN106377441 A CN 106377441A CN 201610941904 A CN201610941904 A CN 201610941904A CN 106377441 A CN106377441 A CN 106377441A
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CN
China
Prior art keywords
parts
alginate
lip pomade
soluble
lipstick
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610941904.3A
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Chinese (zh)
Inventor
宋淑亮
张娥
吉爱国
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Shandong University
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Shandong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong University filed Critical Shandong University
Priority to CN201610941904.3A priority Critical patent/CN106377441A/en
Publication of CN106377441A publication Critical patent/CN106377441A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/733Alginic acid; Salts thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/58Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/02Preparations containing skin colorants, e.g. pigments
    • A61Q1/04Preparations containing skin colorants, e.g. pigments for lips
    • A61Q1/06Lipsticks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/42Colour properties
    • A61K2800/43Pigments; Dyes

Abstract

The invention discloses a cup-staining-free lipstick, which is prepared from the following raw materials in parts by weight: 12-24 parts of wax ingredients, 20-50 parts of oil ingredients, 4-32 parts of pigment ingredients, 0-20 parts of additive ingredients, 2-12 parts of soluble salt alginate and 4-20 parts of soluble metal salt, wherein the soluble salt alginate is selected from sodium alginate tech grade, potassium alginate or ammonium alginate; the soluble metal salt is the soluble metal of aluminum, barium, calcium, copper, ferrum, lead, zinc or nickel. According to the lipstick, the soluble salt alginate and the soluble metal salt are matched to form various ingredients, the weight proportion of each component is reasonably designed, the cup-staining-free lipstick is designed and obtained, and the defects and the deficiencies of traditional lipsticks are overcome. Through tests, the lipstick disclosed by the invention has a good cup-staining-free effect, and the use method is simple and easy to accept.

Description

A kind of non-sticky cup lip pomade and preparation method thereof
Technical field
The present invention relates to a kind of non-sticky cup lip pomade and preparation method thereof, belong to cosmetic technical field.
Background technology
Lip pomade, also known as lipstick, is one of important cosmetics in color make-up, and Main Ingredients and Appearance contains wax, oil and pigment.Lip pomade It is to make lip ruddy glossy, reaches moist, protection lip, increase facial aesthetic feeling and correction lip outline has the product of the effect of setting off Product, are the indispensable cosmetics of women.The method that lip makeup is commonly used is to apply lip pomade (lipstick).Correctly use lip pomade, both Beauty treatment purpose that is gorgeous, increasing glamour can be reached, and do not damage health.The Ms making up is liked all to pay much attention to lip adornment, but It is easiest to the position of de- adornment but also exactly lip.Have a meal, drink water or even speak and all can take off adornment, can be on water tumbler after especially drinking water Leave lip print, this is the behavior losing very much ceremony.
In order to solve the problems, such as that lip pomade is stained with cup, lip pomade manufacturer also production section product solving this problem.At present Mainly there are two methods, one kind is to increase oil components and volatile ingredient, form a film after so that lip pomade is coated on lip, separately A kind of outer method be exactly be painted with lip pomade after, repaste layer of transparent protecting film.Although former approach can avoid lip pomade to be stained with cup, It is using rear lip overdrying, life-time service easily causes the damage of lip;After later approach coats transparent protective film, lip mistake In thick and heavy, and the outside protection film that repeatedly drinks water also easily comes off, thus losing protective effect.And these method costs all than Higher.
Therefore, it is necessary to provide a kind of new lip pomade safe and effective, easy to use, with low cost, it is stained with solving lip pomade The problem of cup.
Content of the invention
For above-mentioned prior art, it is an object of the invention to provide a kind of non-sticky cup lip pomade and preparation method thereof.
For achieving the above object, the present invention adopts following technical proposals:
A kind of non-sticky cup lip pomade, is made up of the raw material of following weight portion:
Wax class component 12-24 part, oil component 20-50 part, colour component 4-32 part, additive component 0-20 part, solvable Property alginate 2-12 part, soluble metallic salt 4-20 part;
Described wax class group is selected from any one or more in cera alba, yellow beeswax or candelilla wax;
Described oil component selects any one or more in shea butter, Oleum Cocois, Flos Inulae oil or Oleum Vitis viniferae;
Described colour component is selected from one of mica powder or lipstick powder or two kinds;
Described additive component is selected from any one or more in lanoline, vaseline or Vitamin E;
Described soluble alginate is selected from sodium alginate, potassium alginate or ammonium alginate;It is preferably sodium alginate.
Described soluble metallic salt is aluminum, barium, calcium, copper, ferrum, the soluble-salt of lead, zinc or nickel;It is preferably gluconic acid Calcium, zinc gluconate, Citric acid calcium or zinc citrate.
Preferably, described non-sticky cup lip pomade by following 1), 2) or 3) shown in the raw material of weight portion make:
1) 12 parts of cera alba, 24 parts of shea butter, 20 parts of Oleum Cocois, 20 parts of mica powder, 12 parts of lipstick powder, sodium alginate 8 Part, 10 parts of calcium gluconate;
2) 20 parts of yellow beeswax, 20 parts of shea butter, 20 parts of Flos Inulae oil, 10 parts of lipstick powder, 3 parts of potassium alginate, lanoline 16 parts, 4 parts of Vitamin E, 6 parts of zinc gluconate;
3) 20 parts of candelilla wax, 20 parts of shea butter, 20 parts of Oleum Vitis viniferae, 4 parts of lipstick powder, 20 parts of vaseline, alginic acid 3.2 parts of sodium, 20 parts of Citric acid calcium.
The present invention also provides the preparation method of above-mentioned non-sticky cup lip pomade, and step is as follows:
(1) wax class component, oil component, colour component and additive component are mixed, be heated to compound and be completely dissolved;
(2) alginate is made alginate solution with water dissolution, add to the compound of step (1), keep temperature Degree, at 70~90 DEG C, stirs, and while keeping good fluidity, injects mould, after being cooled to room temperature, -15~-5 DEG C freezing conditions under freeze 30~60 minutes, the demoulding, prepare lip rod;
(3) by soluble metallic salt water dissolution, obtain soluble metal salt solution, soluble metal salt solution is infiltrated Cotton pads, or make spray.
Preferably, in step (2), the mass concentration of described alginate solution is 1-20%;Described alginate solution Viscosity<50mpa.s, better.
Preferably, in step (2), freeze 40 minutes under -10 DEG C of freezing conditions.
Preferably, in step (3), the mass concentration of described soluble metal salt solution is 0.1-10%;It is preferably 2.5%.
The using method of the non-sticky cup lip pomade of the present invention is:First lip is smeared using normal occupation mode lip rod, then Close lightly the cotton pads being impregnated with soluble metal salt solution with lips;Or soluble metal salt solution is sprayed onto lip, will Unnecessary solution is dried.
The present invention is creatively added with soluble alginate component in lip pomade formula, after preparing lip pomade, first Smear lip pomade by the normal occupation mode of lip pomade in lip, then can make the solvable of alginate precipitation in the use of lip pomade surface Property slaine, after soluble metallic salt is reacted with soluble alginate, can lip pomade surface formed a tunic, this tunic is almost Inviscid, thus while ensureing lip pomade profit lip effect, reaching the purpose of the non-sticky cup of lip pomade.
Beneficial effects of the present invention:
The invention soluble alginate and soluble metallic salt are arranged in pairs or groups uses, in conjunction with various ingredients, and Reasonably devise the weight proportion of each component, design has obtained the non-sticky cup lip pomade of the present invention, overcome lacking of existing lip pomade Fall into and not enough.After tested, the lip pomade of the present invention has good non-sticky cup effect, and using method is simply it is easy to accept.
Specific embodiment
Below by instantiation the present invention will be further elaborated it should explanation, the description below be only for The explanation present invention, is not defined to its content.
In the embodiment of the present invention, raw material used is conventional commercial product.
Embodiment 1:The preparation of non-sticky cup lip pomade
1. raw material composition:
Cera alba:12g
Shea butter:24g
Mica powder:20g
Oleum Cocois:20g
Sodium alginate:2g
Lipstick powder:12g
Calcium gluconate:10g
2. preparation method:
(1) weigh above-mentioned cera alba, shea butter, mica powder, Oleum Cocois, lipstick powder respectively, be put in a beaker, treat With.
(2) (sodium alginate viscosity is less than sodium alginate to be configured to the sodium alginate soln that mass percent is 10% 50mpa.s), it is put in beaker, stand-by.
(3) calcium gluconate is dissolved in distilled water, is made into the solution that mass fraction is 2.5%, and will be changed with this solution Adornment cotton infiltrates, and individually packs for every, and seal after cotton pads infiltrate.
(4) respectively by (1), (2) heating in water bath to 80 DEG C, treat that in (1), compound is completely dissolved and stirs.(2) Pour in (1), stir, maintain 80 DEG C of temperature simultaneously.
(5) to be mixed uniformly and while keep good fluidity, pour into de- after freezing 40min at lipstick grinding tool, -10 DEG C Mould, prepares lip rod.
3. using method:
During use, first lip rod is applied on lip, then closes lightly the cotton pads in (3) with lips.
Embodiment 2:The preparation of non-sticky cup lip pomade
1. raw material composition:
Yellow beeswax:20g
Shea butter:20g
Flos Inulae oil:20g
Lanoline:16g
Vitamin E:4g
Lipstick powder:10g
Potassium alginate:3g
Zinc gluconate:6g
2. preparation method:
(1) weigh above-mentioned yellow beeswax, shea butter, Flos Inulae oil, lanoline, Vitamin E, lipstick powder respectively, be put in one In individual beaker, stand-by.
(2) (potassium alginate viscosity is less than potassium alginate to be configured to the potassium alginate solution that mass percent is 5% 20mpa.s), it is put in beaker, stand-by.
(3) zinc gluconate is dissolved in distilled water, is made into the solution that mass fraction is 1.5%, and will be changed with this solution Adornment cotton infiltrates, and individually packs for every, and seal after cotton pads infiltrate.
(4) respectively by (1) (2) heating in water bath to 70 DEG C, treat that in (1), composition is completely dissolved and stirs.(2) are poured into (1) in, stir, maintain temperature 70 C simultaneously.
(5) to be mixed pour lipstick grinding tool into uniformly and while keep good fluidity, de- after freezing 60min at 4 DEG C Mould, prepares lip rod.
3. using method:
During use, first lip rod is applied on lip, then closes lightly the cotton pads in (3) with lips.
Embodiment 3:The preparation of non-sticky cup lip pomade
1. raw material composition:
Candelilla wax:20g
Shea butter:20g
Oleum Vitis viniferae:20g
Vaseline:20g
Lipstick powder:4g
Sodium alginate:3.2g
Citric acid calcium:20g
2. preparation method:
(1) weigh above-mentioned candelilla wax, shea butter, Oleum Vitis viniferae, vaseline, lipstick powder respectively, be put in a beaker In, stand-by.
(2) (sodium alginate viscosity is less than sodium alginate to be configured to the sodium alginate soln that mass percent is 8% 50mpa.s), it is put in beaker, stand-by.
(3) Citric acid calcium is dissolved in distilled water, is made into the solution that mass fraction is 4%, and will be made up with this solution Cotton infiltrates, and individually packs for every, and seal after cotton pads infiltrate.
(4) respectively by (1) (2) heating in water bath to 85 DEG C, treat that in (1), composition is completely dissolved and stirs.(2) are poured into (1) in, stir, maintain 85 DEG C of temperature simultaneously.
(5) to be mixed pour lipstick grinding tool into uniformly and while keep good fluidity, de- after room temperature cooling 100min Mould, makes lip rod.
3. using method:
During use, first lip rod is applied on lip, then closes lightly the cotton pads in (3) with lips.
Comparative example 1:Sodium alginate in embodiment 1 is removed, other are constant, be prepared into lip pomade as described in Example 1.
Experimental example 1:Cup experiment is stained with by lip pomade
Example 1, each 20 of the commercially available lip pomade of comparative example 1, comparative example and same color respectively, recruits healthy volunteer 20, tested using above-mentioned three kinds of lip pomades respectively.Embodiment 1 lip pomade using method is carried out by the explanation of embodiment 1, contrast Example 1 and commercially available lip pomade have been smeared the rear cotton pads with infiltrating distilled water and have been done same treatment, use dixie cup and transparent glass respectively using rear A glass situation is stained with by glass cup test lipstick, and statistical result is as follows:
A glass situation statistical table is stained with by 1 three kinds of lipsticks of table
By above-mentioned test, result shows that lipstick of the present invention has good non-sticky cup effect, and using method compares Simply it is easy to accept.
The physical and chemical index experiment of experimental example 2 lip pomade
The lip pomade of the preparation in embodiment 1, embodiment 2 and embodiment 3 is carried out according to GBT 26513-2011 lip gloss Heat-resisting, cold-resistant and determination of POV, testing result is shown in Table 2.
The red physical and chemical index testing result of the non-sticky rim of a cup of 2 three kinds of table
Heat-resisting Cold-resistant Peroxide value/%
Embodiment 1 lip pomade Qualified Qualified 0.05
Embodiment 2 lip pomade Qualified Qualified 0.01
Embodiment 3 lip pomade Qualified Qualified 0.03
Result above shows that the lip pomade of index of the present invention is combined lip gloss quality standard, can carry out large-scale mass production.

Claims (10)

1. a kind of non-sticky cup lip pomade is it is characterised in that be made up of the raw material of following weight portion:
Wax class component 12-24 part, oil component 20-50 part, colour component 4-32 part, additive component 0-20 part, solubility sea Alginate 2-12 part, soluble metallic salt 4-20 part;
Described soluble alginate is selected from sodium alginate, potassium alginate or ammonium alginate;It is preferably sodium alginate.
Described soluble metallic salt is aluminum, barium, calcium, copper, ferrum, the soluble-salt of lead, zinc or nickel;It is preferably calcium gluconate, Portugal Grape saccharic acid zinc, Citric acid calcium or zinc citrate.
2. as claimed in claim 1 non-sticky cup lip pomade it is characterised in that described wax class group be selected from cera alba, yellow beeswax or Any one or more in candelilla wax.
3. as claimed in claim 1 non-sticky cup lip pomade it is characterised in that described oil component select shea butter, Oleum Cocois, Any one or more in Flos Inulae oil or Oleum Vitis viniferae.
4. as claimed in claim 1 non-sticky cup lip pomade it is characterised in that described colour component is selected from mica powder or lipstick powder One or two.
5. as claimed in claim 1 non-sticky cup lip pomade it is characterised in that described additive component be selected from lanoline, vaseline Or any one or more in Vitamin E.
6. as claimed in claim 1 non-sticky cup lip pomade it is characterised in that described non-sticky cup lip pomade be by following 1), 2) or 3) The raw material of shown weight portion is made:
1) 12 parts of cera alba, 24 parts of shea butter, 20 parts of Oleum Cocois, 20 parts of mica powder, 12 parts of lipstick powder, 8 parts of sodium alginate, Portugal 10 parts of grape Calciofon;
2) 20 parts of yellow beeswax, 20 parts of shea butter, 20 parts of Flos Inulae oil, 10 parts of lipstick powder, 3 parts of potassium alginate, 16 parts of lanoline, 4 parts of Vitamin E, 6 parts of zinc gluconate;
3) 20 parts of candelilla wax, 20 parts of shea butter, 20 parts of Oleum Vitis viniferae, 4 parts of lipstick powder, 20 parts of vaseline, sodium alginate 3.2 Part, 20 parts of Citric acid calcium.
7. the preparation method of the non-sticky cup lip pomade described in any one of claim 1-5 is it is characterised in that step is as follows:
(1) wax class component, oil component, colour component and additive component are mixed, be heated to compound and be completely dissolved;
(2) alginate is made alginate solution with water dissolution, add to the compound of step (1), maintain the temperature at 70~90 DEG C, stir, while keeping good fluidity, inject mould, after being cooled to room temperature, at -15~-5 DEG C Freeze 30~60 minutes under freezing conditions, the demoulding, prepare lip rod;
(3) by soluble metallic salt water dissolution, obtain soluble metal salt solution, soluble metal salt solution is infiltrated and makes up Cotton, or make spray.
8. preparation method as claimed in claim 7 is it is characterised in that in step (2), the quality of described alginate solution is dense Spend for 1-20%.
9. preparation method as claimed in claim 7 is it is characterised in that in step (2), freeze under -10 DEG C of freezing conditions 40 minutes.
10. preparation method as claimed in claim 7 is it is characterised in that in step (3), described soluble metal salt solution Mass concentration is 0.1-10%;It is preferably 2.5%.
CN201610941904.3A 2016-11-01 2016-11-01 Cup-staining-free lipstick and preparation method thereof Pending CN106377441A (en)

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Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610941904.3A CN106377441A (en) 2016-11-01 2016-11-01 Cup-staining-free lipstick and preparation method thereof

Publications (1)

Publication Number Publication Date
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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519125A (en) * 2017-10-12 2017-12-29 广州番禺职业技术学院 One kind has moisturizing effect lipstick and preparation method thereof
CN107898668A (en) * 2017-12-08 2018-04-13 中山市美源化妆品有限公司 A kind of long-acting dumb light lip glaze formula of non-sticky cup
CN113827513A (en) * 2021-10-25 2021-12-24 瑞昌市瑞美化妆品有限公司 Permanent color lip gloss and preparation method thereof

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519125A (en) * 2017-10-12 2017-12-29 广州番禺职业技术学院 One kind has moisturizing effect lipstick and preparation method thereof
CN107898668A (en) * 2017-12-08 2018-04-13 中山市美源化妆品有限公司 A kind of long-acting dumb light lip glaze formula of non-sticky cup
CN107898668B (en) * 2017-12-08 2020-11-06 中山市美源化妆品有限公司 Long-acting matte lip glaze formula capable of being not stained with cup
CN113827513A (en) * 2021-10-25 2021-12-24 瑞昌市瑞美化妆品有限公司 Permanent color lip gloss and preparation method thereof

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Application publication date: 20170208