CN104546561A - Three-dimensional molding wax oil powder and preparation method thereof - Google Patents
Three-dimensional molding wax oil powder and preparation method thereof Download PDFInfo
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- CN104546561A CN104546561A CN201510037740.7A CN201510037740A CN104546561A CN 104546561 A CN104546561 A CN 104546561A CN 201510037740 A CN201510037740 A CN 201510037740A CN 104546561 A CN104546561 A CN 104546561A
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- powder
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Abstract
The invention discloses three-dimensional molding wax oil powder. The wax oil powder comprises the following components in percentage by mass: 3-20 percent of a curing agent, 10-25 percent of a skin moistening agent, 0.1-5 percent of a film forming agent, 10-20 percent of a powder filling agent and the balance of a pigment. The invention also provides a preparation method of the wax oil powder. A wet powder preparation process is combined with a thermal-filling preparation process, so that powder type cosmetic products are endowed with new characteristics, are soft and smooth in touch feeling when being coated and are not thick or oily.
Description
technical field:
The invention belongs to chemical field, particularly relate to a kind of cosmetics, specifically a kind of three-dimensional plastotype wax oil powder and preparation method thereof.
background technology:
Muffin, eye shadow, the processing technology of the powder classes such as rouge can be divided into 2 large classes, dry powder molding and wet-milling molding, and dry powder molding is traditional press-powder, and wet-milling molding refers to baking powder etc.,
Conventional pastes oils product is as strip lipstick, and eye shadow cream, plane lip wet goods processing technology is that heat is filled with, and it is that heating is dissolved solid content, disperseed, fill, cooled and solidified molding that heat fills with technique.
When powder series products is by wet-milling or traditional press-powder processing technology, the smoothness of product is inadequate, and docile is bad floating powder, and powder face stereoeffect is bad.
When product is heat filling, too thickness and too greasy problem can be there is, because of formula thickness, stereo shaping is difficult, though Silicon moulds can be used for stereo shaping, can there is cost high, the problems such as service life is short, formulation selection high (if material body hardness is inadequate, the demoulding is difficult).
summary of the invention:
The object of the present invention is to provide a kind of three-dimensional plastotype wax oil powder and preparation method thereof, it is inadequate that described this three-dimensional plastotype wax oil powder and preparation method thereof will solve smoothness in powder series products preparation process of the prior art, there is floating powder, colouring property is bad, or too thickness, too greasy technical problem.
A kind of three-dimensional plastotype wax oil powder of the present invention, comprise firming agent, emollient, film former, powder filler and pigment, in described wax oil powder, the mass percent of described firming agent is 3 ~ 20%, the mass percent of described emollient is 10 ~ 25%, the mass percent of described film former is 0.1 ~ 5%, and the mass percent of described powder filler is 10 ~ 20%, and surplus is described pigment.
Further, also include antiseptic in described wax oil powder, in described wax oil powder, the mass percent of described antiseptic is 0.2 ~ 1.0%.
Further, described pigment includes but not limited to pigment, color lake or pearlescent pigment.
Further, the mass percent of described firming agent is 6% ~ 14%.
Further, described firming agent is wax, and described wax is selected from any one or two or more combinations in candelilla wax, Cera Flava, Brazil wax, paraffin, ceresine, synthetic wax or microwax.
Further, the mass percent of described emollient is 15%-20%.
Further, described emollient is selected from any one or two or more combinations in fats, oils, fatty acid, fatty acid ether or fatty acid ester.
Further, described emollient is selected from sad triglyceride, capric acid triglyceride, hydrogenated coco-glyceride class, hydrogenated vegetable oils, octyldodecanol, vaseline, isostearic acid triglycerin esters, isopropyl palmitate, isopropyl myristate, branched paraffin, alcohols, esters, Semen Maydis oil, olive oil, Jojoba oil, American Avocado Tree oil, mineral oil, Butyrospermum parkii fruit fat, ethylhexyl palmitate, volatile silicone oils, non-volatile silicone oil, any one or two or more combinations in Silicone DC 556.
Concrete, volatile silicone oils can be dimethicone.
Further, described emollient is selected from any one or two or more combinations in sad triglyceride, capric acid triglyceride, polydimethylsiloxane, hydrogenated coco-glyceride class, isononyl isononanoate, spermol ricinoleate ester, isopropyl palmitate.
Further, described powder filler is selected from any one or two or more combinations in Pulvis Talci, Muscovitum, sericite, Kaolin, synthetic mica, calcium carbonate, Silicon stone, boron nitride, chinlon, polyethylene, polyurethane, polymethyl methacrylate, cellulose, silicones, the copolymer of silicones, ball-type resin-oatmeal, chinlon.
Further, when these powder are hydrophilic, use again after treatment surface may be needed to become hydrophobicity.The method of process is not limited especially, and such as, silicon, fluoridizes, coupling agent, metallic soap, fatty acid, and aminoacid etc. processes.
Further, described pigment is all inorganic or organic pigments, and can use after surface treatment, e.g., silicon, fluoridizes, coupling agent, metallic soap, fatty acid, and aminoacid etc. processes.Consumption changes according to the difference of color.
Further, described film former is oily melt into membrane or MQ resin, include but not limited to isobutyl methacrylate/bis--hydroxypropyl polydimethylsiloxane acrylate copolymer, hydrogenation (styrene/methyl styrene/indenes) copolymer, VP/ hexadecene copolymer, VP/ eicosene copolymer, trimethyl silicane alcoxyl base esters of silicon acis, hydrogenated polycyclopentadiene, phenylpropyl dimethyl-silicon alcoxyl base esters of silicon acis.
Further, described oil-soluble film former includes but not limited to adipic acid/diethylene glycol/glycerin crosspolymers, acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer, trimethyl silicane alcoxyl base esters of silicon acis, VP/ hexadecene copolymer.
Further, the mass percent of described oil-soluble film former in described wax oil powder is 0.1% ~ 5%.
The function of emollient helps to use and adhere to, and is most significantly to provide closed moisture-keeping function.The composition of film former provides adhesiveness and lasting nature.
Present invention also offers the preparation method of above-mentioned a kind of wax oil powder, first in first container by powder filler, antiseptic and pigment mixing, then second container is adopted, by firming agent, film former, emollient adds, and be heated to the thawing of solid material, then the powder filler will mixed in first container, antiseptic and pigment join in second container, mix homogeneously, add volatile solvent again, be heated to 70 ~ 90 DEG C, it is made to become flow regime, pour into mould, after cooling curing, the demoulding, remove solvent flashing, obtain above-mentioned three-dimensional plastotype wax oil powder.
Wet processing is mixing base material of cosmetics and some solvent, loads container, then removes solvent, and it is stir to dissolve wax and emollient at the temperature of about 70 degree to 90 degree that heat fills with technique, and mixture pours into mould at a proper temperature.
Wet-milling processing technology and heat are filled with processing technology and are combined, and make the powder series products of color make-up have new feature.Silk soft and smooth suitable sense of touch is had when smearing, simultaneously also can not thickness or greasy.The wax oil powder made by method of the present invention, is brought to user and more lubricates, docile, super good colouring, moistens, ductile smear experience while, do not have again tradition heat and fill with the not docile of the too thickness of formula and greasy feeling and wet-milling.
Production technology of the present invention combines wet method and heat fills with technique, and select suitable solvent, as hexane, volatile silicone oils, lightweight isoparaffin etc., consumption is not particularly limited.
The present invention compares with prior art, and its effect is actively with obvious.The present invention, by wet-milling moulding process and heat being filled with the combination of technique, adds special formula composition and just can bring up the product more lubricating the super good colouring of docile easy extension.
The present invention brings to user and more lubricates, docile, moistens, ductile scribble effect.The present invention can make the pattern in powder face be plane, also can be 3D solid.The present invention can accomplish traditional wet-milling, press-powder, and the 3D stereoeffect that heat filling technique is not accomplished.
detailed description of the invention:
Embodiment 1
A
(Muscovitum) 10%
(chinlon-12) 5%
(antiseptic) 0.2%
(pigment+pearlescent pigment) 51.8%
B
(microwax) 13%
(trimethyl silicane alcoxyl base esters of silicon acis) 4%
(hydrogenated coco-glyceride class) 6%
(Jojoba oil) 10%
Preparation method:
Batch mixing A phase
Heating B phase is to admittedly expecting to melt
Add A phase to B phase, stir aftershaping.
Forming method: add solvent flashing in the A+ B of mix homogeneously, be heated to 80C, make it become flow regime, pour into mould.After cooling curing, the demoulding, removes solvent flashing.
Wet processing is mixing base material of cosmetics and some solvent, loads container, then removes solvent, and it is stir to dissolve wax and emollient at the temperature of about 70 degree to 90 degree that heat fills with technique, and mixture pours into mould at a proper temperature.
Embodiment 2
A
(Muscovitum) 9%
(Silicon stone) 6%
(antiseptic) 0.2
(pigment+pearlescent pigment) 57.8%
B
(synthetic wax) 7%
(VP/ hexadecene copolymer) 3%
(Butyrospermum parkii fruit fat) 11%
(dimethicone) 6%
Technique is with embodiment 1.
Embodiment 3
A
Pulvis Talci 7%
Synthesis fluorophologopite 5%
Polymethyl methacrylate 5%
(antiseptic) 0.2
(pigment+pearlescent pigment) 51.8%
B
(candelilla wax) 6%
(hydrogenated polycyclopentadiene) 2%
(Cera Flava) 5%
(caprylic/capric triglyceride) 18%
Technique is with embodiment 1.
Claims (13)
1. a three-dimensional plastotype wax oil powder, it is characterized in that: comprise firming agent, emollient, film former, powder filler and pigment, in described wax oil powder, the mass percent of described firming agent is 3 ~ 20%, the mass percent of described emollient is 10 ~ 25%, the mass percent of described film former is 0.1 ~ 5%, and the mass percent of described powder filler is 10 ~ 20%, and surplus is described pigment.
2. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: also include antiseptic in described wax oil powder, and in described wax oil powder, the mass percent of described antiseptic is 0.2 ~ 1.0%.
3. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: described pigment includes but not limited to pigment, color lake or pearlescent pigment.
4. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: the mass percent of described firming agent is 6% ~ 14%.
5. one according to claim 1 three-dimensional plastotype wax oil powder, it is characterized in that: described firming agent is wax, described wax is selected from any one or two or more combinations in candelilla wax, Cera Flava, Brazil wax, paraffin, ceresine, synthetic wax or microwax.
6. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: the mass percent of described emollient is 15% ~ 20%.
7. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: described emollient is selected from any one or two or more combinations in fats, oils, fatty acid, fatty acid ether or fatty acid ester.
8. one according to claim 1 three-dimensional plastotype wax oil powder, it is characterized in that: described emollient is selected from caprylic/capric triglyceride, hydrogenated coco-glyceride class, hydrogenated vegetable oils, octyldodecanol, vaseline, isostearic acid triglycerin esters, isopropyl palmitate, isopropyl myristate, branched paraffin, alcohols, esters, Semen Maydis oil, olive oil, Jojoba oil, American Avocado Tree oil, mineral oil, Butyrospermum parkii fruit fat, ethylhexyl palmitate, volatile silicone oils, non-volatile silicone oil, any one or two or more combinations in Silicone DC 556.
9. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: described emollient is selected from any one or two or more combinations in caprylic/capric triglyceride, polydimethylsiloxane, hydrogenated coco-glyceride class, isononyl isononanoate, spermol ricinoleate ester, isopropyl palmitate.
10. one according to claim 1 three-dimensional plastotype wax oil powder, is characterized in that: described powder filler is selected from any one or two or more combinations in Pulvis Talci, Muscovitum, sericite, Kaolin, synthetic mica, calcium carbonate, Silicon stone, boron nitride, chinlon, polyethylene, polyurethane, polymethyl methacrylate, cellulose, silicones, the copolymer of silicones, ball-type resin-oatmeal.
11. one according to claim 1 three-dimensional plastotype wax oil powder, it is characterized in that: described film former is oily melt into membrane or MQ resin, include but not limited to isobutyl methacrylate/bis--hydroxypropyl polydimethylsiloxane acrylate copolymer, hydrogenation (styrene/methyl styrene/indenes) copolymer, VP/ hexadecene copolymer, VP/ eicosene copolymer, trimethyl silicane alcoxyl base esters of silicon acis, hydrogenated polycyclopentadiene, phenylpropyl dimethyl-silicon alcoxyl base esters of silicon acis.
12. one according to claim 11 three-dimensional plastotype wax oil powder, is characterized in that: described oil-soluble film former includes but not limited to adipic acid/diethylene glycol/glycerin crosspolymers, acrylic acid (ester) class/polydimethylsiloxanecopolymer copolymer, trimethyl silicane alcoxyl base esters of silicon acis, VP/ hexadecene copolymer.
13. 1 kinds of methods preparing wax oil powder according to claim 1, it is characterized in that: first in first container by powder filler, antiseptic and pigment mixing, then second container is adopted, by firming agent, film former, emollient adds, and be heated to the thawing of solid material, then the powder filler will mixed in first container, antiseptic and pigment join in second container, mix homogeneously, add volatile solvent again, be heated to 70 ~ 90 DEG C, it is made to become flow regime, pour into mould, after cooling curing, the demoulding, remove solvent flashing, obtain above-mentioned three-dimensional plastotype wax oil powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201510037740.7A CN104546561A (en) | 2015-01-26 | 2015-01-26 | Three-dimensional molding wax oil powder and preparation method thereof |
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| CN201510037740.7A CN104546561A (en) | 2015-01-26 | 2015-01-26 | Three-dimensional molding wax oil powder and preparation method thereof |
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| CN104546561A true CN104546561A (en) | 2015-04-29 |
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| CN201510037740.7A Pending CN104546561A (en) | 2015-01-26 | 2015-01-26 | Three-dimensional molding wax oil powder and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014030A (en) * | 2017-12-22 | 2018-05-11 | 丽鑫生技化妆品（上海）有限公司 | Three-dimensional plastotype wax oil powder and preparation method thereof |
| CN110652458A (en) * | 2019-10-12 | 2020-01-07 | 苏州蓓希颜化妆品股份有限公司 | Super-three-dimensional pouring powder and preparation method thereof |
| CN111514065A (en) * | 2020-05-13 | 2020-08-11 | 丽鑫生技化妆品（上海）有限公司 | Liquid baking powder blush and preparation method thereof |
| CN115154336A (en) * | 2022-08-10 | 2022-10-11 | 义乌市菲米化妆品有限公司 | Three-dimensional shaping ointment type highlight powder and preparation method thereof |
Citations (2)
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| CN101951874A (en) * | 2007-12-20 | 2011-01-19 | 莱雅公司 | Cosmetic product, its purposes and the cosmetic test kit that contains described product |
| EP2420221A1 (en) * | 2009-04-16 | 2012-02-22 | Shiseido Company, Ltd. | Powdered solid cosmetic and manufacturing method therefor |
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2015
- 2015-01-26 CN CN201510037740.7A patent/CN104546561A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101951874A (en) * | 2007-12-20 | 2011-01-19 | 莱雅公司 | Cosmetic product, its purposes and the cosmetic test kit that contains described product |
| EP2420221A1 (en) * | 2009-04-16 | 2012-02-22 | Shiseido Company, Ltd. | Powdered solid cosmetic and manufacturing method therefor |
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| 罗怡情: "《化妆品成分辞典》", 31 May 2005 * |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108014030A (en) * | 2017-12-22 | 2018-05-11 | 丽鑫生技化妆品（上海）有限公司 | Three-dimensional plastotype wax oil powder and preparation method thereof |
| CN110652458A (en) * | 2019-10-12 | 2020-01-07 | 苏州蓓希颜化妆品股份有限公司 | Super-three-dimensional pouring powder and preparation method thereof |
| CN111514065A (en) * | 2020-05-13 | 2020-08-11 | 丽鑫生技化妆品（上海）有限公司 | Liquid baking powder blush and preparation method thereof |
| CN115154336A (en) * | 2022-08-10 | 2022-10-11 | 义乌市菲米化妆品有限公司 | Three-dimensional shaping ointment type highlight powder and preparation method thereof |
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Application publication date: 20150429 |