CN102228248A - Energy-saving and environmentally-protected production process of Songzhen capsules - Google Patents
Energy-saving and environmentally-protected production process of Songzhen capsules Download PDFInfo
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- CN102228248A CN102228248A CN2011101787523A CN201110178752A CN102228248A CN 102228248 A CN102228248 A CN 102228248A CN 2011101787523 A CN2011101787523 A CN 2011101787523A CN 201110178752 A CN201110178752 A CN 201110178752A CN 102228248 A CN102228248 A CN 102228248A
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Abstract
The invention relates to an improvement of processing technology of Songzhen capsules. The Songzhen capsules are healthcare products prepared by refining extracts of pine needles and pine park, which serve as main raw materials. Because the conventional production process of the Songzhen capsules is complex and high in energy consumption and low in efficiency, the production of the Songzhen capsules must be changed so as to fully utilize the diet therapy function of the pine needle; meanwhile, with the change in the production process procedures and the production process parameters, the content of active ingredients is raised, and the healthcare effect is improved. The Songzhen capsules produced by the production process can serve consumers at the sub-health state by better healthcare quality and make consumers regain health more quickly. The production process has the characteristics of low development cost, high technical content and big added value of products, and the product produced by the production process is the core product in current natural nutrient healthcare product markets as well as the front product in human health industry adapting to the changes in social development and economical development.
Description
Technical field
The invention belongs to Chinese medicine nutrient and healthcare products technical field, relate to the energy saving and environment friendly production technology of the precious capsule of a kind of pine.
Background technology
Along with society and expanding economy, the variation of human food's industrialization and living environment, make human diseases spectrum and healthy curve constantly change, sub-health population is more and more, various diseases becomes younger, and old DD etc., bring a series of medical treatment and social concern must for society and family.Meanwhile, human medical treatment is touched formula and is also changed the pattern that prevention, health care, rehabilitation combine into by simple disease treatment, and various health care kinds are substituting traditional medicine product, are just bringing into play increasing effect in serving the human health industry.Under this social environment, No. 157717 patent of invention that on June 2nd, 2004 authorized: " a kind of health products that delay senility, regulate blood fat " loose precious capsule is being brought into play bodyguard's function of its human health, the precious capsule of pine is to be main production raw material with Lignum Pini Nodi pine needle, loose skin, obtain pine needle pine bark extract through extracting, and then the refining health food that forms, contain large number of biological Flavonoid substances, PCA in the pine needle, also be rich in chlorophyll, multivitamin.Wherein pine needle flavonoids and proanth ocyanidins material become fragile and the effective good recovery effects of phenomenon such as blood vessel osmotic pressure is undesired to blood vessel, also can be used for the expansion artery blood vessel, increase the red blood cell oxygen carrying capacity, stimulate circulation, make the rejuvenation of organizing of health, play function in delaying senility.The production process complexity of the precious capsule of existing pine, high cost with low efficiency, cause environmental pollution easily, be unfavorable for increasing economic efficiency, realize that enterprise, society and consumer three win.
Summary of the invention
For the invention provides, the above-mentioned shortcoming that overcomes prior art a kind ofly can save capability resource, reduce bad environment pollution, improve the performance of enterprises, promote the local economy benefit, realize enterprise and social doulbe-sides' victory, simultaneously, for the consumer provides the health product of super quality and competitive price, be the processing technology of the loose precious capsule of global human health industry service.
The present invention solves the technical scheme that its technical problem takes: the energy saving and environment friendly production technology of the precious capsule of a kind of pine, the bright pine needle of gathering is cleaned, shredded, and collection pine bark, mix by part by weight in the prescription then, with concentration is 40-90%(V/V) alcoholic extraction 1 time, the weight of compound is 1:3～1:10 with the ratio of the volume of alcohol liquid during extraction, extracts temperature and be normal temperature to 90 ℃, 1.5 hours/time; To extract then material through concentrate and clarification after, the supernatant of getting after the clarification adds cycloheptaamylose by the weight proportion in the prescription; Make the finished product of 0.5g/ grain at last by capsule preparations technology.
In the extraction worker parameter of making loose precious capsule be: bright pine needle and 40-90% ethanol feed intake by 1:3-6, pine skin powder and 40-90% ethanol feed intake by 1:6-10, raw material and solvent are put in the extractor, about soak at room temperature 16h, intensification maintains 60-90 ℃, stressor layer is in the 0.02-0.05Mpa scope in jar, and the time is 1.5h, emits the extract metering.
Technological parameter at the enrichment process of making loose precious capsule is: steam pressure: 0.02-0.08Mpa, temperature: 70-94 ℃, flow: 400-500L/h, vacuum when vacuum concentrates :-0.01～-0.08Mpa, temperature: 50-65 ℃, the concentrate Baume degrees is about 6-20Be '.
Technological parameter in the spraying operation of making loose precious capsule is: parcel stirred 5 minutes; Spray liquid concentration 40-50%; 160 ± 10 ℃ of EATs, 90 ± 10 ℃ of leaving air temps.
The invention has the beneficial effects as follows: the research of this project improves the content of effective component when changing production process, processing parameter, improve health-care effect.Make loose precious capsule with the consumer of better quality services, the consumer is got well quickly in sub-health state.It is low that the present invention has development cost, with high content of technology, the characteristics that added value of product is big, and its product is the core product on the present natural nutrition health products market, also is the leading-edge products that adapts to the human health industry of social development and economic development variation.
[description of drawings]
Fig. 1 is the precious capsule manufacture craft of a pine of the present invention block diagram;
[
The specific embodiment]
The present invention is further described below in conjunction with drawings and Examples:
Referring to Fig. 1, the preparation method of loose precious capsule is among the present invention:
The first step is for extracting: bright pine needle and 40-90% edible ethanol feed intake by 1:3-6, pine skin powder and 40-90% edible ethanol feed intake by 1:6-10, raw material and solvent are put in the extractor, about soak at room temperature 16h, intensification maintains 60-90 ℃, stressor layer is in the 0.02-0.05Mpa scope in jar, and the time is 1.5h, emits the extract metering;
Second step is for concentrating: extract enters the thin film evaporator intensification and concentrates, and the control steam pressure is at 0.02-0.08Mpa, and temperature is at 70-94 ℃, and flow is in the scope of 400-500L/h, and its concentrate imports vacuum concentration pan through conveying pipeline; It is concentrated to reduce pressure, its vacuum degree control-0.01～-0.08Mpa, temperature is controlled in 50-65 ℃ the scope, liquid to be extracted is concentrated into 〉=6-20
oIn Be ' time, blowing is cooled to room temperature in clean stainless steel cask, behind the cooling clarification filtration, gets clear liquid and enters down operation, and accurately metering goes in the batch mixes jar and stirred 10 minutes, detects its Baume degrees, functional component, density and dry solids content;
The 3rd step was spray-drying: with dry substance in the concentrate is core, with the cycloheptaamylose is the wall material, adopt to stir the colloid mill about 5 minutes homogeneous that circulate, parcel, being effective composition enters in β-CD molecule, make the spray liquid about 30-50%, be heated to 40-60 ℃, the pine needle that spray liquid obtains being wrapped through the drying machine with centrifugal spray spray-drying, loose bark extract micro-capsule powder; With 160 ± 10 ℃ of EATs, 90 ± 10 ℃ of leaving air temps were collected pine needle pine skin spray powder at first separator when spray was done;
The 4th step was batch mixes: the accurate various supplementary materials of weighing, and mixing in multidirectional motion blender, incorporation time is 60 minutes;
The 5th step filled for capsule and polished: the precious mixed powder of uniform pine that will prepare, be filled to loose precious capsule by Autocapsulefillingmachine, and to guarantee in the filling process that the filling weight and the capsule method of double differences are different, prevent that microbial contamination, foreign matter from sneaking into; Material softgel shell is outer by the capsule polishing machine cleans down, and makes capsule bright and clean, is difficult for contaminated;
The 6th step was bottling or aluminum-plastic packaged: bottling, with populated loose precious capsule,, on bottled line, finish several cans, plug drier (1 bag), spiral cover, labeling, counting by 60/bottle; Aluminum-plastic packaged, become 12 of every plates with clean PVC, PTP plastic-aluminum, can not lack grain, breakage, require pressing tight, the bubble eye is neat, cuts regularly, and the date is clear;
The 7th one is external packing: dress box and vanning, and require date of manufacture and shelf-life clear to printing, Packing Sound must not be lacked the scarce box of bottle; Product is through the control laboratory sale of can dispatching from the factory after the assay was approved.
By the prepared loose precious capsule product quality standard that goes out of above-mentioned technology be:
Appearance index: proterties: Long Circle, the hard shell capsules that profile is complete does not have damaged, leakage phenomenon; Color and luster: content is faint yellow powder to pale brown look, does not have caking, phenomenon such as mouldy; Smell flavour: free from extraneous odour; Impurity: the visible impurity of no naked eyes;
Effective component index: PCA 〉=5g/100g; General flavone: 400-600mg/100g;
Physical and chemical index: moisture content≤9%; Disintegration time limited≤30 minute; Plumbous (in Pb)≤1.5mg/kg; Arsenic (in As)≤1.0mg/kg; Mercury (in Hg)≤0.3mg/kc; Ash content≤4%;
Microbiology index: total plate count≤1000cfu/g; Mould≤25cfu/g; Coliform≤40MPN/100g; Saccharomycete≤25cfu/g; Pathogenic bacteria (salmonella, Shigella, staphylococcus aureus, hemolytic streptococcus): must not detect.
Claims (4)
1. the present invention relates to the energy saving and environment friendly production technology of the precious capsule of a kind of pine, it is characterized in that: the bright pine needle that will gather is cleaned, chopping, and collection pine bark, mix by part by weight in the prescription then, with concentration is 40 ~ 90%(V/V) alcoholic extractions 1 time, the weight of compound is 1:3～1:10 with the ratio of the volume of alcohol liquid during extraction, and the extraction temperature is normal temperature～90 ℃, 1.5 hours/time; To extract then material through concentrate and clarification after, the supernatant of getting after the clarification adds cycloheptaamylose by the weight proportion in the prescription; Make the finished product of 0.5g/ grain at last by capsule preparations technology.
2. the energy saving and environment friendly production technology of the precious capsule of pine as claimed in claim 1, it is characterized in that: the extraction worker parameter of loose precious capsule in the present invention is: bright pine needle and 40-90% ethanol feed intake by 1:3-6, pine skin powder and 40-90% ethanol feed intake by 1:6-10, raw material and solvent are put in the extractor, about soak at room temperature 16h, heat up and maintain 60-90 ℃, stressor layer is in the 0.02-0.05Mpa scope in jar, time is 1.5h, emits the extract metering.
3. the energy saving and environment friendly production technology of the precious capsule of pine as claimed in claim 1, it is characterized in that: the technological parameter of the enrichment process of loose precious capsule in the present invention is: steam pressure: 0.02-0.08Mpa, temperature: 88-94 ℃, flow: 430-460L/h, vacuum when vacuum concentrates :-0.01～-0.08Mpa, temperature: 50-65 ℃, the concentrate Baume degrees is about 10Be '.
4. the energy saving and environment friendly production technology of the precious capsule of pine as claimed in claim 1 is characterized in that: the technological parameter of the spraying operation of loose precious capsule in the present invention is: parcel stirred 5 minutes; Spray liquid concentration 30-50%; 160 ± 10 ℃ of EATs, 90 ± 10 ℃ of leaving air temps.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011101787523A CN102228248A (en) | 2011-06-29 | 2011-06-29 | Energy-saving and environmentally-protected production process of Songzhen capsules |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2011101787523A CN102228248A (en) | 2011-06-29 | 2011-06-29 | Energy-saving and environmentally-protected production process of Songzhen capsules |
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| CN2011101787523A Pending CN102228248A (en) | 2011-06-29 | 2011-06-29 | Energy-saving and environmentally-protected production process of Songzhen capsules |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103271198A (en) * | 2013-06-03 | 2013-09-04 | 贵州大学 | Pinus massoniaha pine needle instant tea and production technology thereof |
| CN108065700A (en) * | 2016-11-14 | 2018-05-25 | 赵京洙 | Five-leaved pine pillow capable of prolonging life |
| CN112101772A (en) * | 2020-09-10 | 2020-12-18 | 重庆华森制药股份有限公司 | Intelligent manufacturing system and method for six-ingredient nerve-soothing capsules |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1362250A (en) * | 2001-12-28 | 2002-08-07 | 广东嵩珍营养源研究所 | Health tonic for delaying senility and regualting blood lipoid |
| CN1531949A (en) * | 2003-03-18 | 2004-09-29 | 王介庆 | Method for extracting pine needle active component and micro capsule preparation |
| CN101759727A (en) * | 2009-09-30 | 2010-06-30 | 钱娟 | Nano-scale pine bark extract and preparation method thereof |
| CN101810649A (en) * | 2010-05-13 | 2010-08-25 | 沈阳益丰源生物科技有限公司 | Method for preparing pine needle distilled and concentrated solution |
-
2011
- 2011-06-29 CN CN2011101787523A patent/CN102228248A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1362250A (en) * | 2001-12-28 | 2002-08-07 | 广东嵩珍营养源研究所 | Health tonic for delaying senility and regualting blood lipoid |
| CN1531949A (en) * | 2003-03-18 | 2004-09-29 | 王介庆 | Method for extracting pine needle active component and micro capsule preparation |
| CN101759727A (en) * | 2009-09-30 | 2010-06-30 | 钱娟 | Nano-scale pine bark extract and preparation method thereof |
| CN101810649A (en) * | 2010-05-13 | 2010-08-25 | 沈阳益丰源生物科技有限公司 | Method for preparing pine needle distilled and concentrated solution |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103271198A (en) * | 2013-06-03 | 2013-09-04 | 贵州大学 | Pinus massoniaha pine needle instant tea and production technology thereof |
| CN108065700A (en) * | 2016-11-14 | 2018-05-25 | 赵京洙 | Five-leaved pine pillow capable of prolonging life |
| CN112101772A (en) * | 2020-09-10 | 2020-12-18 | 重庆华森制药股份有限公司 | Intelligent manufacturing system and method for six-ingredient nerve-soothing capsules |
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Application publication date: 20111102 |