CN102181083A - Oil-resistant anti-slip rubber for soles and preparation method thereof - Google Patents
Oil-resistant anti-slip rubber for soles and preparation method thereof Download PDFInfo
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- CN102181083A CN102181083A CN2011101153903A CN201110115390A CN102181083A CN 102181083 A CN102181083 A CN 102181083A CN 2011101153903 A CN2011101153903 A CN 2011101153903A CN 201110115390 A CN201110115390 A CN 201110115390A CN 102181083 A CN102181083 A CN 102181083A
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Abstract
The invention relates to the field of shoe making, in particular to a rubber for manufacturing soles and a preparation method thereof. The oil-resistant anti-slip rubber for the soles is prepared from the following raw materials in part by weight: 8 to 12 parts of 3L standard rubber, 3 to 12 parts of styrene butadiene rubber (SBR), 70 to 85 parts of nitrile-butadiene rubber, 25 to 45 parts of white carbon black, 3 to 6 parts of active agent, 4 to 7 parts of zinc oxide, 0.8 to 1.5 parts of stearic acid, 2 to 3 parts of accelerant, 0.4 to 0.6 part of antifogging agent, 5 to 10 parts of resin and 2 to 3 parts of sulfur. Compared with the prior art, the oil-resistant anti-slip rubber has remarkable advantages of oil resistance and slip prevention compared with the traditional rubber for the soles.
Description
Technical field
The present invention relates to shoe-making field, be specifically related to a kind of rubber of making on sole and preparation method thereof that is used to.
Background technology
Shoes are requisite daily necessities in people's daily life.The comfort level of shoes, work-ing life are relevant with the material and the performance of sole to a great extent.The material of sole is in the majority with rubber-sole at present.At the bottom of General Purpose Rubber, the hot compression molding moulding divides natural rubber and regenerated rubber.Though wear resistance is good, anti-skidding, flexible, easy fracture not, pliability is better, expandability good, contraction is stable, good, the good bandability of hardness, waterproof.But that shortcoming is a quality is heavier, easily tell frost, not perishable; Not hard, pricked saturating easily; Ventilation property, water absorbability are bad, are afraid of the oil immersion bubble, should not wear in the oily place of contacts such as filling station.Some are also arranged at present is high-pressure polyethylene rubber-sole, is the sole of major ingredient with high-pressure polyethylene and rubber, and rubber and plastics are also used.At the bottom of but it is rubber, so matter is heavy, and more expensive, oil resistant is not thermo-labile, and non-skid property can not satisfy high requirement.
Summary of the invention
The technical problem to be solved in the present invention is the not oil resistant that overcomes prior art, and non-skid property can not satisfy the problem of high requirement, and a kind of novel oil resistant on-slip sole glue is provided.
The present invention addresses the above problem the technical scheme that is adopted:
A kind of oil resistant on-slip sole glue is by comprising that following raw materials in weight portion makes: 8～12 parts in glue of 3L mark, 3～12 parts in SBR styrene-butadiene rubber(SBR), 70～85 parts of nitrile rubbers, 25～45 parts of white carbon blacks, 3～6 parts of promoting agents, 4～7 parts in zinc oxide, 0.8～1.5 part of stearic acid, 2～3 parts of promotor, 0.4～0.6 part of antifogging agent, 5～10 parts of resins, 2～3 parts in sulphur.
Preferably, by comprising that following raw materials in weight portion makes: 9～10 parts in glue of 3L mark, 5～10 parts in SBR styrene-butadiene rubber(SBR), 75～80 parts of nitrile rubbers, 30～40 parts of white carbon blacks, 4～5 parts of promoting agents, 5～6 parts in zinc oxide, 1～1.2 part of stearic acid, 2.2～2.8 parts of promotor, 0.4～0.6 part of antifogging agent, 7～8 parts of resins, 2.2～2.8 parts in sulphur.
More preferably, by comprising that following raw materials in weight portion makes: 10 parts in glue of 3L mark, 5～10 parts in SBR styrene-butadiene rubber(SBR), 75～80 parts of nitrile rubbers, 30～40 parts of white carbon blacks, 4～5 parts of promoting agents, 5～6 parts in zinc oxide, 1.1 parts of stearic acid, 2.5 parts of promotor, 0.5 part of antifogging agent, 7～8 parts of resins, 2.5 parts in sulphur.
The present invention also provides the preparation method of described oil resistant on-slip sole with glue, and this preparation method may further comprise the steps:
(1) earlier nitrile rubber is plasticated;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 0.5～1.5 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 3～5 minutes, slice;
(3) place after 12 hours, mixing again 2～4 minutes, and then the slice of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.
The oil resistant on-slip sole of the present invention preparation method of glue, another program is, may further comprise the steps:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, mixing again 3 minutes, and then the slice of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.
Preferably, described step (3) is: place after 24 hours, mixing in mill, plate is put into 6～5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating.
Preferably, curing temperature is 130～170 ℃ in the described step (4), and curing time is 3～4 minutes.
More preferably, curing temperature is 150 ℃ in the described step (4), and curing time is 3.5 minutes.
Compared with prior art, oil resistant on-slip glue of the present invention has the advantage of significant lightweight, oil resistant and on-slip with rubber than traditional sole.And the preparation method is simple, and cost is lower, the production efficiency height.
Embodiment
Some embodiments of the present invention below are provided, understand the present invention to help further, but protection scope of the present invention are not limited in this.Raw material in following examples does not specify, all adopts commercially available industry common raw material.
Embodiment 1
A kind of oil resistant on-slip sole glue, raw material and each parts by weight of raw materials proportioning are as follows: 10 parts in glue of 3L mark, 5～10 parts in SBR styrene-butadiene rubber(SBR), 75～80 parts of nitrile rubbers, 30～40 parts of white carbon blacks, 4～5 parts of promoting agents, 5～6 parts in zinc oxide, 1.1 parts of stearic acid, 2.5 parts of promotor, 0.5 part of antifogging agent, 7～8 parts of resins, 2.5 parts in sulphur.Wherein, every part is 5 kilograms.
Preparation as follows:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, every material claims 40 kilograms, and is mixing in mill, and plate is put into 6～5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating.
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.Curing temperature is 150 ℃, and curing time is 3.5 minutes.
After testing, prepared oil resistant on-slip sole is as follows with the performance index of glue: DIN:130-250, and folding 10-12 ten thousand times, proportion: 1.126, dry on-slip 1.82, the water on-slip 1.21 of wetting.As seen the sole of gained of the present invention has the advantage of good lightweight, oil resistant, folding, on-slip with glue.This preparation method is simple, and cost is lower, the production efficiency height.
Embodiment 2
Get 8 parts in glue of following raw materials in weight portion: 3L mark, 3 parts in SBR styrene-butadiene rubber(SBR), 70 parts of nitrile rubbers, 25 parts of white carbon blacks, 3 parts of promoting agents, 4 parts in zinc oxide, 0.8 part of stearic acid, 2 parts of promotor, 0.4 part of antifogging agent, 5 parts of resins, 2 parts in sulphur.2 kilograms every part.
The preparation method:
(1) earlier nitrile rubber is plasticated;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 0.5 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 3 minutes, slice;
(3) place after 12 hours, mixing again 2 minutes, and then the slice of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.Curing temperature is 130 ℃, and curing time is 4 minutes.
Embodiment 3
A kind of oil resistant on-slip sole glue, raw material and proportioning:
10 parts in glue of 3L mark, 8 parts in SBR styrene-butadiene rubber(SBR), 75 parts of nitrile rubbers, 30 parts of white carbon blacks, 4 parts of promoting agents, 5 parts in zinc oxide, 1 part of stearic acid, 2.2 parts of promotor, 0.4 part of antifogging agent, 8 parts of resins, 2.8 parts in sulphur.8 kilograms every part.
Preparation:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, mixing again 3 minutes, place after 24 hours, mixing in mill, plate is put into 6～5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.170 ℃ of curing temperatures, curing time are 3 minutes.
Embodiment 4
A kind of oil resistant on-slip sole glue is made by following raw materials in weight portion: 9 parts in glue of 3L mark, 5 parts in SBR styrene-butadiene rubber(SBR), 80 parts of nitrile rubbers, 40 parts of white carbon blacks, 5 parts of promoting agents, 6 parts in zinc oxide, 1.2 parts of stearic acid, 2.8 parts of promotor, 0.6 part of antifogging agent, 8 parts of resins, 2.2 parts in sulphur.10 kilograms every part.
Preparation:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, mixing in mill, plate is put into 6～5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.Curing temperature is 150 ℃, and curing time is 3.5 minutes.
Embodiment 5
A kind of oil resistant on-slip sole glue is made by following raw materials in weight portion: 12 parts in glue of 3L mark, 12 parts in SBR styrene-butadiene rubber(SBR), 85 parts of nitrile rubbers, 45 parts of white carbon blacks, 6 parts of promoting agents, 7 parts in zinc oxide, 1.5 parts of stearic acid, 3 parts of promotor, 0.6 part of antifogging agent, 10 parts of resins, 3 parts in sulphur.Every part is 50 kilograms.
Preparation:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, mixing in mill, plate is put into 5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.Curing temperature is 160 ℃, and curing time is 4 minutes.
Claims (8)
1. oil resistant on-slip sole glue, it is characterized in that, by comprising that following raw materials in weight portion makes: 8～12 parts in glue of 3L mark, 3～12 parts in SBR styrene-butadiene rubber(SBR), 70～85 parts of nitrile rubbers, 25～45 parts of white carbon blacks, 3～6 parts of promoting agents, 4～7 parts in zinc oxide, 0.8～1.5 part of stearic acid, 2～3 parts of promotor, 0.4～0.6 part of antifogging agent, 5～10 parts of resins, 2～3 parts in sulphur.
2. oil resistant on-slip sole glue according to claim 1, it is characterized in that, by comprising that following raw materials in weight portion makes: 9～10 parts in glue of 3L mark, 5～10 parts in SBR styrene-butadiene rubber(SBR), 75～80 parts of nitrile rubbers, 30～40 parts of white carbon blacks, 4～5 parts of promoting agents, 5～6 parts in zinc oxide, 1～1.2 part of stearic acid, 2.2～2.8 parts of promotor, 0.4～0.6 part of antifogging agent, 7～8 parts of resins, 2.2～2.8 parts in sulphur.
3. oil resistant on-slip sole glue according to claim 2, it is characterized in that, by comprising that following raw materials in weight portion makes: 10 parts in glue of 3L mark, 5～10 parts in SBR styrene-butadiene rubber(SBR), 75～80 parts of nitrile rubbers, 30～40 parts of white carbon blacks, 4～5 parts of promoting agents, 5～6 parts in zinc oxide, 1.1 parts of stearic acid, 2.5 parts of promotor, 0.5 part of antifogging agent, 7～8 parts of resins, 2.5 parts in sulphur.
4. the described oil resistant on-slip of the arbitrary claim of claim 1 to 3 sole is characterized in that with the preparation method of glue, may further comprise the steps:
(1) earlier nitrile rubber is plasticated;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 0.5～1.5 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 3～5 minutes, slice;
(3) place after 12 hours, mixing again 2～4 minutes, and then the slice of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.
5. the described oil resistant on-slip of the arbitrary claim of claim 1 to 3 sole is characterized in that with the preparation method of glue, may further comprise the steps:
(1) earlier nitrile rubber is plasticated the 3 thin bags of in mill, plasticating;
(2) put into nitrile rubber, 3L mark glue, SBR styrene-butadiene rubber(SBR) after plasticating then during banburying earlier, put into white carbon black, promoting agent again, mixing 1 minute, put into zinc oxide, stearic acid, promotor, antifogging agent, resin again, mixing 4 minutes, slice;
(3) place after 24 hours, mixing again 3 minutes, and then the slice of plasticating;
(4) add sulphur, sulfidization molding promptly gets described oil resistant on-slip sole glue.
6. according to the preparation method of the described oil resistant on-slip of claim 5 sole with glue, it is characterized in that described step (3) is: place after 24 hours, mixing in mill, plate is put into 6～5 millimeters, mixing 3 minutes; And then plate got to 3 millimeters, the 3 thin sheets that contract out of plasticating.
7. according to the preparation method of the described oil resistant on-slip of claim 6 sole with glue, it is characterized in that curing temperature is 130～170 ℃ in the described step (4), curing time is 3～4 minutes.
8. according to the preparation method of the described oil resistant on-slip of claim 7 sole with glue, it is characterized in that curing temperature is 150 ℃ in the described step (4), curing time is 3.5 minutes.
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| CN2011101153903A CN102181083A (en) | 2011-05-05 | 2011-05-05 | Oil-resistant anti-slip rubber for soles and preparation method thereof |
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| CN2011101153903A CN102181083A (en) | 2011-05-05 | 2011-05-05 | Oil-resistant anti-slip rubber for soles and preparation method thereof |
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Cited By (13)
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|---|---|---|---|---|
| CN102898690A (en) * | 2012-09-29 | 2013-01-30 | 广东智达行新材料有限公司 | Anti-static rubber for sole and preparation method thereof |
| CN103159993A (en) * | 2013-04-03 | 2013-06-19 | 叶建华 | Oil-resistant non-skid sole material and preparation method thereof |
| CN103156330A (en) * | 2011-12-09 | 2013-06-19 | 际华三五一七橡胶制品有限公司 | Jie Fang rubber shoes with grease proofing function |
| CN103772763A (en) * | 2013-12-25 | 2014-05-07 | 泉州鑫泰鞋材有限公司 | Rubber composite and preparation process thereof |
| CN103910916A (en) * | 2014-04-01 | 2014-07-09 | 安徽金科橡塑制品有限公司 | Lightweight wear-resistant antiskid rubber |
| CN104356496A (en) * | 2014-11-13 | 2015-02-18 | 茂泰(福建)鞋材有限公司 | Antistatic anti-slip rubber-plastic foamed shoe sole and preparation method thereof |
| CN104893027A (en) * | 2015-06-24 | 2015-09-09 | 厦门迈图新材料有限公司 | Cold-resistant non-slip rubber sports shoe material and manufacturing method thereof |
| CN105295138A (en) * | 2015-12-01 | 2016-02-03 | 吴江市风尚鞋厂 | Antiskid shoe material and preparation method thereof |
| CN105820383A (en) * | 2016-05-24 | 2016-08-03 | 宁波市中迪鞋业有限公司 | Composite wear-resisting shoe sole |
| CN106317506A (en) * | 2016-08-24 | 2017-01-11 | 际华三五三实业有限公司 | Anti-skid and oil-resistant rubber soles with dual density |
| RU2609396C2 (en) * | 2011-12-23 | 2017-02-01 | Компани Женераль Дез Этаблиссман Мишлен | Shoe sole containing composition based on nitrile rubber, oil and resin |
| CN106589499A (en) * | 2016-11-22 | 2017-04-26 | 茂泰(福建)鞋材有限公司 | Slippery resistant safe shoe rubber sole and preparation method thereof |
| CN107325341A (en) * | 2017-08-18 | 2017-11-07 | 晋江市池店镇娇鹏贸易有限公司 | A kind of formula for making anti-slip rubber sole |
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103156330A (en) * | 2011-12-09 | 2013-06-19 | 际华三五一七橡胶制品有限公司 | Jie Fang rubber shoes with grease proofing function |
| RU2609396C2 (en) * | 2011-12-23 | 2017-02-01 | Компани Женераль Дез Этаблиссман Мишлен | Shoe sole containing composition based on nitrile rubber, oil and resin |
| CN102898690A (en) * | 2012-09-29 | 2013-01-30 | 广东智达行新材料有限公司 | Anti-static rubber for sole and preparation method thereof |
| CN103159993A (en) * | 2013-04-03 | 2013-06-19 | 叶建华 | Oil-resistant non-skid sole material and preparation method thereof |
| CN103772763A (en) * | 2013-12-25 | 2014-05-07 | 泉州鑫泰鞋材有限公司 | Rubber composite and preparation process thereof |
| CN103910916A (en) * | 2014-04-01 | 2014-07-09 | 安徽金科橡塑制品有限公司 | Lightweight wear-resistant antiskid rubber |
| CN104356496B (en) * | 2014-11-13 | 2017-01-25 | 茂泰(福建)鞋材有限公司 | Antistatic anti-slip rubber-plastic foamed shoe sole and preparation method thereof |
| CN104356496A (en) * | 2014-11-13 | 2015-02-18 | 茂泰(福建)鞋材有限公司 | Antistatic anti-slip rubber-plastic foamed shoe sole and preparation method thereof |
| CN104893027A (en) * | 2015-06-24 | 2015-09-09 | 厦门迈图新材料有限公司 | Cold-resistant non-slip rubber sports shoe material and manufacturing method thereof |
| CN105295138A (en) * | 2015-12-01 | 2016-02-03 | 吴江市风尚鞋厂 | Antiskid shoe material and preparation method thereof |
| CN105820383A (en) * | 2016-05-24 | 2016-08-03 | 宁波市中迪鞋业有限公司 | Composite wear-resisting shoe sole |
| CN105820383B (en) * | 2016-05-24 | 2018-01-02 | 宁波市中迪鞋业有限公司 | A kind of composite-material abrasive sole |
| CN106317506A (en) * | 2016-08-24 | 2017-01-11 | 际华三五三实业有限公司 | Anti-skid and oil-resistant rubber soles with dual density |
| CN106317506B (en) * | 2016-08-24 | 2018-07-27 | 际华三五一三实业有限公司 | A kind of anti-skidding and oil resistant dual-density rubber sole |
| CN106589499A (en) * | 2016-11-22 | 2017-04-26 | 茂泰(福建)鞋材有限公司 | Slippery resistant safe shoe rubber sole and preparation method thereof |
| CN106589499B (en) * | 2016-11-22 | 2018-07-03 | 茂泰(福建)鞋材有限公司 | A kind of oil resistant slides safety shoe rubber soles and preparation method thereof |
| CN107325341A (en) * | 2017-08-18 | 2017-11-07 | 晋江市池店镇娇鹏贸易有限公司 | A kind of formula for making anti-slip rubber sole |
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Application publication date: 20110914 |