CN103156330A - Jie Fang rubber shoes with grease proofing function - Google Patents
Jie Fang rubber shoes with grease proofing function Download PDFInfo
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- CN103156330A CN103156330A CN2011104070565A CN201110407056A CN103156330A CN 103156330 A CN103156330 A CN 103156330A CN 2011104070565 A CN2011104070565 A CN 2011104070565A CN 201110407056 A CN201110407056 A CN 201110407056A CN 103156330 A CN103156330 A CN 103156330A
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Abstract
The invention relates to a Jie Fang rubber shoes with a grease proofing function. Each raw material proportion by weight of a grease proofing undersole thereof comprises 85-90 portions of chloroprene rubber adhesive, 10-15 portions of standard rubber, 0.5-0.7 portions of accelerant DM, 0.3-0.5 portions of sodium (NA)-22, 3-5 portions of zinc oxide, 3-5 portions of magnesium oxide, 2-4 portions of stearic acid, 0.4-0.8 portions of paraffin wax, 8-10 portions of machine oil, 5-8 portions of phthalic acid dibutyl ester, 10-12 portions of argil, 2-4 portions of spindle oil, 45-55 portions of high wear-resisting carbon black N330, 10-15 portions of white carbon black and 0.5-1.5 portions of antiager. Each raw material proportion by weight of a gease proofing foxing strip and a toecap comprises 85-90 portions of the chloroprene rubber adhesive, 10-15 portions of the standard rubber, 0.3-0.5 portions of the accelerant DM, 0.3-0.5 portions of the NA-22, 3-5 portions of the zinc oxide, 3-5 portions of the magnesium oxide, 2-4 portions of the stearic acid, 0.3-0.5 portions of paraffin wax, 3-5 portions of pine tar, 4-6 portions of the phthalic acid dibutyl ester, 3-5 portions of the spindle oil, 55-65 portions of the argil, 20-30 portions of the high wear-resisting carbon black N330 and 0.5-1.5 portions of the antiager. Each raw material proportion by weight of grease proofing adhesive cements comprises 100 portions of the chloroprene rubber adhesive, 0.4-0.8 portions of the accelerant DM, 0.4-0.8 portions of the accelerant NA-22, 3-5 portions of the zinc oxide, 3-5 portions of the magnesium oxide, 4-8 portions of phenolic resin, 15-25 portions of calcium carbonate, 0.5-1.5 portions of the antiager. The Jie Fang rubber shoes with the grease proofing function are good in grease proofing effects, low in cost and high in qualification rate.
Description
Technical field
The present invention relates to rubber overshoes, refer in particular to a kind of liberation rubber overshoes with oil-resistant function.
Background technology
Liberate rubber overshoes as a kind of shoes for working, liked by consumers in general such as peasant, builder, workers in enterprise, sanitationman, its main feature is cheap, comfortable, endurable, and is economical and economical.But in consumer's use procedure, its some shortcomings show especially out gradually, and particularly the consumer contacts with oils when wearing, and the phenomenons such as it swelling occurs, comes unglued, the disconnected end cause and wear service life and significantly reduce, and the characteristics that cost performance is not high are especially obvious.
Summary of the invention
The objective of the invention is provides a kind of liberation rubber overshoes with oil-resistant function for the shortcoming that exists in background technology and problem improvement and bring new ideas in addition.
Technical solution of the present invention is a kind of rubber overshoes that are comprised of vamp and sole of structure, wherein sole comprises the large end, foxing and packet header, rubber sole, foxing and packet header are made by grease proofing formula material, and bonding by grease proofing rubber cement, and wherein the grease proofing large end is made by the raw material of following weight portion:
Neoprene 85-90 part, standard rubber 10-15 part, altax 0.5-0.7 part, accelerant N A-22 0.3-0.5 part, zinc oxide 3-5 part, magnesia 3-5 part, stearic acid 2-4 part, paraffin 0.4-0.8 part, machine oil 8-10 part, dibutyl phthalate 5-8 part, potter's clay 10-12 part, bobbin oil 2-4 part, high abrasion furnace carbon black N330 45-55 part, white carbon 10-15 part, age resistor 0.5-1.5 part.
Grease proofing foxing and packet header are made by the raw material of following weight portion:
Neoprene 85-90 part, standard rubber 10-15 part, altax 0.3-0.5 part, accelerant N A-22 0.3-0.5 part, zinc oxide 3-5 part, magnesia 3-5 part, stearic acid 2-4 part, paraffin 0.3-0.5 part, pine tar 3-5 part, dibutyl phthalate 4-6 part, bobbin oil 3-5 part, potter's clay 55-65 part, high abrasion furnace carbon black N330 20-30 part, age resistor 0.5-1.5 part;
Grease proofing rubber cement is made by the raw material of following weight portion:
100 parts of neoprenes, altax 0.4-0.8 part, accelerant N A-22 0.4-0.8 part, zinc oxide 3-5 part, magnesia 3-5 part, phenolic resins 4-8 part, calcium carbonate 15-25 part, age resistor 0.5-1.5 part.
The optimum amount weight portion of each raw material of the grease proofing large end of the present invention is:
88 parts of neoprenes, 12 parts of standard rubbers, 0.6 part of altax, 0.4 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 3 parts of stearic acid, 0.6 part, paraffin, 9 parts, machine oil, 6.5 parts of dibutyl phthalates, 11 parts, potter's clay, 3 parts, bobbin oil, 50 parts of high abrasion furnace carbon black N330s, 12 parts of white carbons, 1 part, age resistor.
The optimum amount weight portion of the grease proofing foxing of the present invention and each raw material of packet header is:
88 parts of neoprenes, 12 parts of standard rubbers, 0.4 part of altax, 0.4 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 3 parts of stearic acid, 0.4 part, paraffin, 4 parts of pine tars, 5 parts of dibutyl phthalates, 4 parts, bobbin oil, 60 parts, potter's clay, 25 parts of high abrasion furnace carbon black N330s, 1 part, age resistor;
The optimum amount weight portion of grease proofing each raw material of rubber cement of the present invention is:
100 parts of neoprenes, 0.6 part of altax, 0.6 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 6 parts, phenolic resins, 20 parts, calcium carbonate, 1 part, age resistor.
Advantage of the present invention and beneficial effect:
1, the present invention adopts neoprene as liberation rubber overshoes rubber components rubber, utilizes its grease proofing effective characteristics, the rubber components formulas such as the redesign liberation rubber overshoes large ends, foxing, packet header, thus increase oil-resistant function on liberation rubber overshoes original function basis.
2, rubber mixing technique of the present invention is simplified former technique, has shortened technological process, has improved production efficiency, and meets the instructions for use of each rubber shoes product enterprise fully.
3, the present invention has improved liberation rubber shoe molding technique, has reduced production cost, has improved product percent of pass, and other performances of rubber components meet the relevant national standard requirement fully.
The specific embodiment
Embodiment 1:
1, make at the grease proofing large end:
1) batching:
Rubber: neoprene 85kg, standard rubber 15kg, middle material: altax 0.5kg, magnesia 3kg, stearic acid 2kg, paraffin 0.4kg, age resistor 0.5kg, oil plant: machine oil 8kg, dibutyl phthalate 5kg, bobbin oil 2kg, powder: potter's clay 10kg, high abrasion furnace carbon black N330 45kg, white carbon 10kg, vulcanizing agent: accelerant N A-22 0.3kg, zinc oxide 3kg.
2) refining glue:
A, plasticate: standard rubber is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
2, make grease proofing foxing, packet header:
1) batching:
Rubber: neoprene 85kg, standard rubber 15kg; Middle material: altax 0.3kg, magnesia 3kg, age resistor 0.5kg, stearic acid 2kg, paraffin 0.3kg; Oil plant: pine tar 3kg, dibutyl phthalate 4kg, bobbin oil 3kg; Powder: potter's clay 55kg, high abrasion furnace carbon black N330 20kg; Vulcanizing agent: accelerant N A-22 0.3kg, zinc oxide 3kg.
2) refining glue:
A, plasticate: standard rubber is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
3, make grease proofing rubber cement:
1) batching:
Neoprene 100 kg, altax 0.4kg, accelerant N A-22 0.4kg, zinc oxide 3kg, magnesia 3kg, phenolic resins 4kg, calcium carbonate 15kg, age resistor 0.5kg.
2) refining glue:
Neoprene adds various compounding ingredients after 450 mill thin-pass 4 times (35-45 ℃ of roller temperature, roll spacing is below 2 millimeters), thick roll spacing is put on material feeding limit, limit, roll spacing is adjusted to 2 millimeters after powder is suffered all and is beaten triangle bag 6-8, and thick roller slice, section are stand-by.
3) making beating:
The oil of going to the bottom: 30 kilograms of acetate butyls, 10 kilograms, gasoline, drop into 71.4 kilograms of the blob of viscoses that cut, open cooling water, drive to stir the oiling (21 kilograms, fourth fat, 24 kilograms, gasoline) of stopping after 8 hours, stirred again 2 hours, and added appropriate solvent (2 kilograms, gasoline, 1 kilogram, fourth fat) and adjust concentration.Glue is 1:1.2 than oil; Fourth fat is 60:40 than gasoline.
4, molding process of the present invention:
The sizing material that mixes is cut into large egative film through mill heat refining and calender calendering (according to client's needs decorative pattern pattern) respectively, sponge sheet, the foxing sheet, Bumper is for moulding.
Upper of a shoe and middle base fabric are sewed up, the cover shoe last or hat block, brush packet header rubber cement, brush foxing rubber cement is filled out sponge after oven dry, sticking packet header, the upper large end, surround bar, pressing is reprocessed, and checks, quits, and advances the digester (-tor) sulfuration, and is cooling, and delasting is joined twoly, checks packing, finished product warehouse-in.
Embodiment 2:
1, make at the grease proofing large end:
1) batching:
Rubber: neoprene 88kg, standard rubber 12kg, middle material: altax 0.6kg, magnesia 4kg, stearic acid 3kg, paraffin 0.4kg, age resistor 1.0kg, oil plant: machine oil 9kg, dibutyl phthalate 6.5kg, bobbin oil 3kg, powder: potter's clay 11kg, high abrasion furnace carbon black N330 50kg, white carbon 12.5kg, vulcanizing agent: accelerant N A-22 0.4kg, zinc oxide 4kg.
2) refining glue:
A, plasticate: natural gum is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
2, make grease proofing foxing, packet header:
1) batching:
Rubber: neoprene 90kg, standard rubber 10kg; Middle material: altax 0.4kg, magnesia 4kg, age resistor 1.0kg, stearic acid 3kg, paraffin 0.4kg; Oil plant: pine tar 4kg, dibutyl phthalate 5kg, bobbin oil 4kg; Powder: potter's clay 60kg, high abrasion furnace carbon black N330 25kg; Vulcanizing agent: accelerant N A-22 0.4kg, zinc oxide 4kg.
2) refining glue:
A, plasticate: natural gum is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
3, make grease proofing rubber cement:
1) batching:
Neoprene 100kg, altax 0.6kg, accelerant N A-22 0.6kg, zinc oxide 4kg, magnesia 4kg, phenolic resins 6kg, calcium carbonate 20kg, age resistor 1kg.
2) refining glue:
Neoprene adds various compounding ingredients after 450 mill thin-pass 4 times (35-45 ℃ of roller temperature, roll spacing is below 2 millimeters), thick roll spacing is put on material feeding limit, limit, roll spacing is adjusted to 2 millimeters after powder is suffered all and is beaten triangle bag 6-8, and thick roller slice is stand-by.
3) making beating:
The oil of going to the bottom: 30 kilograms of acetate butyls, 10 kilograms, gasoline, drop into 71.4 kilograms of the blob of viscoses that cut, open cooling water, drive to stir the oiling (21 kilograms, fourth fat, 24 kilograms, gasoline) of stopping after 8 hours, stirred again 2 hours, and added appropriate solvent (2 kilograms, gasoline, 1 kilogram, fourth fat) and adjust concentration.Glue is 1:1.2 than oil; Fourth fat is 60:40 than gasoline.
4, molding process of the present invention:
The sizing material that mixes is cut into large egative film through mill heat refining and calender calendering (according to client's needs decorative pattern pattern) respectively, sponge sheet, the foxing sheet, Bumper is for moulding.
Upper of a shoe and middle base fabric are sewed up, the cover shoe last or hat block, brush packet header rubber cement, brush foxing rubber cement is filled out sponge after oven dry, sticking packet header, the upper large end, surround bar, pressing is reprocessed, and checks, quits, and advances the digester (-tor) sulfuration, and is cooling, and delasting is joined twoly, checks packing, finished product warehouse-in.
Embodiment 3:
1, make at the grease proofing large end:
1) batching:
Rubber: neoprene 90kg, standard rubber 10kg, middle material: altax 0.7kg, magnesia 5kg, stearic acid 4kg, paraffin 0.8kg, age resistor 1.5kg, oil plant: machine oil 10kg, dibutyl phthalate 8kg, bobbin oil 4kg, powder: potter's clay 12kg, high abrasion furnace carbon black N330 55kg, white carbon 15kg, vulcanizing agent: accelerant N A-22 0.5kg, zinc oxide 5kg.
2) refining glue:
A, plasticate: standard rubber is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
2, make grease proofing foxing, packet header:
1) batching:
Rubber: neoprene 90kg, standard rubber 10kg; Middle material: altax 0.5, magnesia 5kg, age resistor 1.5kg, stearic acid 4kg, paraffin 0.5kg; Oil plant: pine tar 5kg, dibutyl phthalate 6kg, bobbin oil 5kg; Powder: potter's clay 65kg, high abrasion furnace carbon black N330 30kg; Vulcanizing agent: accelerant N A-22 0.5kg, zinc oxide 5kg.
2) refining glue:
A, plasticate: standard rubber is incorporated thick refining of neoprene into and is reached 0.4 rear Ting Fang ﹑ Leng Que ﹑ to plasticity and check after 450 mill thin-pass 6 times (30-40 ℃ of roller temperature, roll spacing is below 1 millimeter), stand-by.
B, mixing: the rubber that will plasticate drops into banbury moulding 1-2 minute, add vulcanizing agent when adding middle material, powder, oil plant to steady load, moulding 30-50 is binder removal (gelatin temperature control is below 120 ℃) after second, after drawing logical three roads, flat-bed machine breaks into thin slice, through the cooling water below 40 ℃, hang cool horse heat radiation and dry up, park after 12 hours stand-by.
3, make grease proofing rubber cement:
1) batching:
Neoprene 100kg, altax 0.8kg, accelerant N A-22 0.8kg, zinc oxide 5kg, magnesia 5kg, phenolic resins 8kg, calcium carbonate 25kg, age resistor 1.5kg.
2) refining glue:
Neoprene adds various compounding ingredients after 450 mill thin-pass 4 times (35-45 ℃ of roller temperature, roll spacing is below 2 millimeters), thick roll spacing is put on material feeding limit, limit, roll spacing is adjusted to 2 millimeters after powder is suffered all and is beaten triangle bag 6-8, and thick roller slice is stand-by.
3) making beating:
The oil of going to the bottom: 30 kilograms of acetate butyls, 10 kilograms, gasoline, drop into 71.4 kilograms of the blob of viscoses that cut, open cooling water, drive to stir the oiling (21 kilograms, fourth fat, 24 kilograms, gasoline) of stopping after 8 hours, stirred again 2 hours, and added appropriate solvent (2 kilograms, gasoline, 1 kilogram, fourth fat) and adjust concentration.Glue is 1:1.2 than oil; Fourth fat is 60:40 than gasoline.
4, molding process of the present invention:
The sizing material that mixes is cut into large egative film through mill heat refining and calender calendering (according to client's needs decorative pattern pattern) respectively, sponge sheet, the foxing sheet, Bumper is for moulding.
Upper of a shoe and middle base fabric are sewed up, the cover shoe last or hat block, brush packet header rubber cement, brush foxing rubber cement is filled out sponge after oven dry, sticking packet header, the upper large end, surround bar, pressing is reprocessed, and checks, quits, and advances the digester (-tor) sulfuration, and is cooling, and delasting is joined twoly, checks packing, finished product warehouse-in.
Embodiment of the present invention is only the description that the preferred embodiment of the present invention is carried out; be not that design of the present invention and scope are limited; under the prerequisite that does not break away from design philosophy of the present invention; various modification and improvement that in this area, engineers and technicians make technical scheme of the present invention; all should fall into protection scope of the present invention; the technology contents that the present invention asks for protection all is documented in claims.
Claims (2)
1. liberation rubber overshoes with oil-resistant function, be comprised of vamp and sole, wherein sole comprises the large end, foxing and packet header, it is characterized in that rubber sole, foxing and packet header made by grease proofing formula material, and bonding by grease proofing rubber cement, wherein the grease proofing large end, made by the raw material of following weight portion:
Neoprene 85-90 part, standard rubber 10-15 part, altax 0.5-0.7 part, accelerant N A-22 0.3-0.5 part, zinc oxide 3-5 part, magnesia 3-5 part, stearic acid 2-4 part, paraffin 0.4-0.8 part, machine oil 8-10 part, dibutyl phthalate 5-8 part, potter's clay 10-12 part, bobbin oil 2-4 part, high abrasion furnace carbon black N330 45-55 part, white carbon 10-15 part, age resistor 0.5-1.5 part.
Grease proofing foxing and packet header are made by the raw material of following weight portion:
Neoprene 85-90 part, standard rubber 10-15 part, altax 0.3-0.5 part, accelerant N A-22 0.3-0.5 part, zinc oxide 3-5 part, magnesia 3-5 part, stearic acid 2-4 part, paraffin 0.3-0.5 part, pine tar 3-5 part, dibutyl phthalate 4-6 part, bobbin oil 3-5 part, potter's clay 55-65 part, high abrasion furnace carbon black N330 20-30 part, age resistor 0.5-1.5 part;
Grease proofing rubber cement is made by the raw material of following weight portion:
100 parts of neoprenes, altax 0.4-0.8 part, accelerant N A-22 0.4-0.8 part, zinc oxide 3-5 part, magnesia 3-5 part, phenolic resins 4-8 part, calcium carbonate 15-25 part, age resistor 0.5-1.5 part.
2. liberation rubber overshoes with oil-resistant function according to claim 1 is characterized in that the described grease proofing large end made by the raw material of following weight portion:
88 parts of neoprenes, 12 parts of standard rubbers, 0.6 part of altax, 0.4 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 3 parts of stearic acid, 0.6 part, paraffin, 9 parts, machine oil, 6.5 parts of dibutyl phthalates, 11 parts, potter's clay, 3 parts, bobbin oil, 50 parts of high abrasion furnace carbon black N330s, 12 parts of white carbons, 1 part, age resistor.
Grease proofing foxing and packet header are made by the raw material of following weight portion:
88 parts of neoprenes, 12 parts of standard rubbers, 0.4 part of altax, 0.4 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 3 parts of stearic acid, 0.4 part, paraffin, 4 parts of pine tars, 5 parts of dibutyl phthalates, 4 parts, bobbin oil, 60 parts, potter's clay, 25 parts of high abrasion furnace carbon black N330s, 1 part, age resistor;
Grease proofing rubber cement is made by the raw material of following weight portion:
100 parts of neoprenes, 0.6 part of altax, 0.6 part of accelerant N A-22,4 parts, zinc oxide, 4 parts, magnesia, 6 parts, phenolic resins, 20 parts, calcium carbonate, 1 part, age resistor.
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CN103342412A (en) * | 2013-08-02 | 2013-10-09 | 武汉钢铁(集团)公司 | Coke particle biomembrane carrier and preparation method thereof |
CN104311901A (en) * | 2014-10-30 | 2015-01-28 | 际华三五三七制鞋有限责任公司 | Plastifying process for calendering type grass green rubber foxing rubber for liberation shoes |
CN105440371A (en) * | 2015-12-14 | 2016-03-30 | 桐乡市亿源鞋业有限公司 | Anti-oil sole material |
CN105713267A (en) * | 2016-05-06 | 2016-06-29 | 际华三五三九制鞋有限公司 | Outsole sizing material for protective boots |
CN110615926A (en) * | 2019-09-27 | 2019-12-27 | 际华三五三七有限责任公司 | Black rubber sole for oil-proof shoes, preparation method and vulcanization process thereof |
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CN104311901A (en) * | 2014-10-30 | 2015-01-28 | 际华三五三七制鞋有限责任公司 | Plastifying process for calendering type grass green rubber foxing rubber for liberation shoes |
CN105440371A (en) * | 2015-12-14 | 2016-03-30 | 桐乡市亿源鞋业有限公司 | Anti-oil sole material |
CN105713267A (en) * | 2016-05-06 | 2016-06-29 | 际华三五三九制鞋有限公司 | Outsole sizing material for protective boots |
CN105713267B (en) * | 2016-05-06 | 2017-12-05 | 际华三五三九制鞋有限公司 | The big bottom sizing of Protective Boots |
CN110615926A (en) * | 2019-09-27 | 2019-12-27 | 际华三五三七有限责任公司 | Black rubber sole for oil-proof shoes, preparation method and vulcanization process thereof |
CN110628103A (en) * | 2019-09-27 | 2019-12-31 | 际华三五三七有限责任公司 | Rubber sole for kitchen use, preparation method and secondary vulcanization process thereof |
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