CN102174742A - Antibacterial simulation hair preparation method and simulation hair product - Google Patents
Antibacterial simulation hair preparation method and simulation hair product Download PDFInfo
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- CN102174742A CN102174742A CN201110029338.6A CN201110029338A CN102174742A CN 102174742 A CN102174742 A CN 102174742A CN 201110029338 A CN201110029338 A CN 201110029338A CN 102174742 A CN102174742 A CN 102174742A
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- keratin
- chemical fiber
- preparation
- hairs
- fiber hairs
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Abstract
The invention provides an antibacterial simulation hair preparation method. The method comprises the following steps of: preparing a keratin surfactant; adsorbing and fixing the keratin and chemical fiber hairs; and performing aftertreatment on a chemical fiber hair product. The invention also provides a simulation hair product which is produced by the preparation method. The simulation hair product comprises the chemical fiber hairs and the keratin adsorbed on the surfaces of the chemical fiber hairs. By the technical scheme, a layer of keratin with the same chemical compositions as human hairs is attached to the surfaces of the chemical fiber hairs, so that the perspiration absorption property, the air permeability and the heat preservation property of the chemical fiber hairs are improved, and the chemical fiber hairs are changed into simulation hairs which have the same soft and smooth properties as the human hairs and high affinity and health-care performance on a human body.
Description
Technical field
The present invention relates to emulation and send out the manufacturing field, more specifically, relate to the emulation that a kind of keratin combines with chemical fiber hairs and send out and preparation method thereof.
Background technology
Along with the continuous development and the growth of hair product industry, people's hair plait raw material is fewer and feweri, and domestic stranger sends out resource and peters out, and presses for to seek the substitute that a kind of people sends out resource.
Some enterprises substitute with animal ceratin fibers such as long ox hair, oxtail, long wool, horse hair, horse-hairs, but because the growth cycle of these animal ceratin fibers is grown, yielded poorly, far can not satisfy the wilderness demand in market.
In recent years, occurred the chemical fibre silk that makes with chemical fibre on the market, substituted natural hair and make hair products, because the chemical fibre silk is cheap and easy to get, so it has obtained fast development.Though chemical fiber hairs can substitute natural hair at aspects such as shape, dyeability and Nai La intensity, but its chemical composition and natural hair are completely different, when producing hair products, alternative people has some problems, relatively poor as its hygroscopicity, gas permeability, warmth retention property, and can not show a candle to natural human with the compatibility of human body sends out, people's long periods of wear can be felt sulks, not bulk, not submissive, even skin disease can occur, influences the application and the development of chemical fiber hairs.
Also useful at home and abroad in the recent period animal/vegetable protein and chemical fibre macromolecular compound mix, make spinning solution and carry out wire drawing, make the chemical fibre azelon and produce hair products, but because the chemical fibre macromolecular compound in this product mostly concentrates on the surface of product, so it still exists absorption of perspiration, gas permeability poor, do not possess the shortcoming of the affine health care of human body.
Summary of the invention
Send out in order to solve above-mentioned existing people that the substitute absorption of perspiration is poor, gas permeability, warmth retention property are poor, sulks, not bulk, not submissive, with problem such as human body compatibility difference or one of at least, the invention provides a kind of method, improve the moisture absorption of chemical fiber hairs, ventilative, thermal property, and with the affinity of human body, improve chemical fiber hairs and keratic binding ability simultaneously.
In view of this, the invention provides the preparation method that a kind of antibiotic emulation is sent out, comprising:
In technique scheme, preferably, in the step 106, the preparation flow of keratin surfactant comprises:
Wherein, organic slat solution is by anion and cation composition, and anion is chlorion or acetate ion, and CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole;
In technique scheme, preferably, in the step 108, the keratin surfactant concentrations is 15%～16%, and oscillator is a ultrasonic oscillator, and the vibration temperature is 50 ℃ ± 2 ℃.
In technique scheme, preferably, in the step 110, solidify program and be: the chemical fiber hairs goods are immersed 30% (NH
4)
2SO
4In the solidification liquid, make angle liquid albumen become solid.
In technique scheme, preferably, in the step 110, cure and comprise: 80～105 ℃ down 20～30 minutes prebakes and 115～120 ℃ of 1～3 minute bake down.
In technique scheme, preferably, in the step 110, post processing comprises:
Step 200 is cleaned chemical fibre product with soft water;
Preferably, post-treatment agent is a silicone softening agent, and main component is a dimethyl silicone polymer.
The present invention also provides a kind of emulation hair products of implementing technique scheme, comprises that chemical fiber hairs 1 reaches attached to its surperficial keratin 2.
In technique scheme, preferably, make keratin 2 absorption, be fixed on the surface of chemical fiber hairs 1 by ultrasonic oscillator.
According to the present invention, make chemical fiber hairs surface attachment one deck and people send out the identical keratin protein of chemical composition, the chemical fibre hair is become with the people send out to have softness the same, smooth and easy and human body has the emulation of good affinity and health properties to send out.
Description of drawings
Fig. 1 is the preparation flow figure that emulation according to an embodiment of the invention is sent out;
Fig. 2 is the concrete implementing procedure figure of step 106 among Fig. 1;
Fig. 3 is the post processing flow chart of step 110 among Fig. 1;
Fig. 4 is the cross sectional representation of emulation hair products.
The specific embodiment
In order more to be expressly understood above-mentioned purpose of the present invention, feature and advantage, the present invention is further described in detail below in conjunction with the drawings and specific embodiments.
Set forth a lot of details in the following description so that fully understand the present invention, still, the present invention can also adopt other to be different from other modes described here and implement, and therefore, the present invention is not limited to the restriction of following public specific embodiment.
Fig. 1, Fig. 2, Fig. 3 are the flow charts that the preparation method is sent out in emulation according to an embodiment of the invention.
As shown in Figure 1, the invention provides the preparation method that a kind of antibiotic emulation is sent out, comprising:
The concrete implementing procedure figure of 106 keratin surfactant among Fig. 2 Fig. 1.
As shown in Figure 2, the preparation flow of keratin surfactant comprises:
Wherein, organic slat solution is by anion and cation composition, and anion is chlorion or acetate ion, and CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole;
In technique scheme, preferably, in the step 108, the keratin surfactant concentrations is 15%～16%, and oscillator is a ultrasonic oscillator, and the vibration temperature is 50 ℃ ± 2 ℃.
In technique scheme, preferably, in the step 110, solidify program and be: the chemical fiber hairs goods are immersed 30% (NH
4)
2SO
4In the solidification liquid, make angle liquid albumen become solid.
In technique scheme, preferably, in the step 110, cure and comprise: baked in following 2 minutes 100 ℃ of prebakes in following 30 minutes with at 120 ℃.
Fig. 3 is the post processing flow chart in 110 among Fig. 1.
As shown in Figure 3, the flow process of post processing comprises:
Step 200 is cleaned chemical fibre product with soft water;
Post-treatment agent of the present invention is a silicone softening agent, main component is a dimethyl silicone polymer, it is the grease that water white transparency, nontoxic nothing are smelt, have good heat resistance, high temperature resistant, resistance to low temperature, be desirable liquid spring, emulation of the present invention sent out possessed submissive, resilient characteristics.
In technique scheme, a specific embodiment of described step 108, described step 110 is:
The keratin surfactant solution of the chemical fiber hairs goods being put into concentration 15%～16% floods, under 50 ℃ ± 2 ℃ of temperature, handle through ultrasonic oscillation, after making keratin protein be adsorbed in chemical fibre silk surface, shift out chemical fibre silk or chemical fibre product,, clean with soft water then through 100 ℃ of following preliminary dryings of 30 minutes with 120 ℃ of following 2 minutes bake, carry out the post processing oven dry with after treatment aid, promptly get high submissive antibiotic emulation and send out product.
The present invention also provides a kind of emulation hair products of producing by technique scheme, as shown in Figure 4, comprising: chemical fiber hairs 1 reaches attached to its surperficial keratin 2.
In technique scheme, preferably, make keratin 2 absorption, be fixed on the surface of chemical fiber hairs 1 by ultrasonic oscillator.
According to technical scheme provided by the invention, the high submissive antibiotic emulation of being produced is sent out, both kept that chemical fiber hairs is processed easily, the anti-good advantage of intensity of drawing of finished product, possessed again the hygroscopicity that natural human is sent out, gas permeability, with the performance of human body compatibility excellence, remedy the shortcoming of chemical fiber hairs hygroscopicity on the present market, gas permeability and human body compatibility difference, and improved the binding ability of keratin and chemical fiber hairs.
The above is the preferred embodiments of the present invention only, is not limited to the present invention, and for a person skilled in the art, the present invention can have various changes and variation.Within the spirit and principles in the present invention all, any modification of being done, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. the preparation method that antibiotic emulation is sent out is characterized in that, comprising:
Step 106, preparation keratin surfactant;
Step 108 is put into described keratin surfactant with chemical fiber hairs, by conduction, the vibration of oscillator, makes keratin absorption, is fixed on the chemical fiber hairs, obtains the chemical fiber hairs goods;
Step 110 is taken out the chemical fiber hairs goods, solidifies, cures, washing, post processing, obtains antibiotic emulation and sends out.
2. preparation method according to claim 1 is characterized in that, in described step 106, the preparation flow of described keratin surfactant comprises:
Step 101 is with impurity removing, washing, oven dry;
Step 102 is dissolved raw material in organic slat solution, and removal of impurities, decolouring, obtains keratolysis liquid;
Wherein, described organic slat solution is by anion and cation composition, and described anion is chlorion or acetate ion, and described CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole;
Step 103 by dialysis device dialysis twice, is removed the keratin protein of molecular weight M＞10000 and molecular weight M＜3000 with the gained lysate, and the acquisition molecular weight is the keratin solution of 3000≤M≤10000;
Step 104, the pH value of regulating step 103 gained solution are 7.5～9.0 and add 0.8～1.2% antiseptic, obtain described keratin surfactant.
3. preparation method according to claim 1 is characterized in that, in the described step 108, described keratin surfactant concentrations is 15%～16%, and described oscillator is a ultrasonic oscillator, and the vibration temperature is 50 ℃ ± 2 ℃.
4. preparation method according to claim 1 is characterized in that, in the described step 110, the described program of solidifying is: the chemical fiber hairs goods are immersed 30% (NH
4)
2SO
4In the solidification liquid, make angle liquid albumen become solid.
5. preparation method according to claim 1 is characterized in that, in the described step 110, described curing comprises: 80～105 ℃ down 20～30 minutes prebake and 115～120 ℃ of 1～3 minute bake down.
6. preparation method according to claim 1 is characterized in that, in the described step 110, described post processing comprises:
Step 200 is cleaned chemical fibre product with soft water;
Step 202 is carried out the post processing oven dry with post-treatment agent.
7. according to each described preparation method in the claim 1 to 6, it is characterized in that described post-treatment agent is a silicone softening agent, the composition of described silicone softening agent comprises dimethyl silicone polymer.
8. emulation hair products that obtain by each described preparation method in the claim 1 to 7 is characterized in that, comprising: chemical fiber hairs reaches attached to its surperficial keratin.
9. emulation hair products according to claim 8 is characterized in that, make keratin absorption, be fixed on the surface of chemical fiber hairs by ultrasonic oscillator.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029338.6A CN102174742B (en) | 2011-01-27 | 2011-01-27 | Antibacterial simulation hair preparation method and simulation hair product |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029338.6A CN102174742B (en) | 2011-01-27 | 2011-01-27 | Antibacterial simulation hair preparation method and simulation hair product |
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| Publication Number | Publication Date |
|---|---|
| CN102174742A true CN102174742A (en) | 2011-09-07 |
| CN102174742B CN102174742B (en) | 2012-12-19 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201110029338.6A Active CN102174742B (en) | 2011-01-27 | 2011-01-27 | Antibacterial simulation hair preparation method and simulation hair product |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103222703A (en) * | 2013-05-20 | 2013-07-31 | 青岛海森林进出口有限公司 | Manufacturing method of antibacterial flexible glue head hair extension beam |
| CN106245156A (en) * | 2016-08-23 | 2016-12-21 | 河北见喜新材料科技股份有限公司 | Flame-retardant antibacterial imitated wig and manufacturing method thereof |
| CN115094531A (en) * | 2022-08-11 | 2022-09-23 | 青岛融美发制品集团有限公司 | Preparation process of antibacterial shape memory simulation hair |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08226017A (en) * | 1995-02-17 | 1996-09-03 | Kanegafuchi Chem Ind Co Ltd | Composite fiber and its production |
| CN101877976A (en) * | 2007-11-30 | 2010-11-03 | 株式会社钟化 | Antibacterial artificial hair and antibacterial coating agent for artificial hair |
-
2011
- 2011-01-27 CN CN201110029338.6A patent/CN102174742B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08226017A (en) * | 1995-02-17 | 1996-09-03 | Kanegafuchi Chem Ind Co Ltd | Composite fiber and its production |
| CN101877976A (en) * | 2007-11-30 | 2010-11-03 | 株式会社钟化 | Antibacterial artificial hair and antibacterial coating agent for artificial hair |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103222703A (en) * | 2013-05-20 | 2013-07-31 | 青岛海森林进出口有限公司 | Manufacturing method of antibacterial flexible glue head hair extension beam |
| CN103222703B (en) * | 2013-05-20 | 2016-04-27 | 青岛海森林进出口有限公司 | The preparation method of antibacterial flexible glue head hair extension beam |
| CN106245156A (en) * | 2016-08-23 | 2016-12-21 | 河北见喜新材料科技股份有限公司 | Flame-retardant antibacterial imitated wig and manufacturing method thereof |
| CN115094531A (en) * | 2022-08-11 | 2022-09-23 | 青岛融美发制品集团有限公司 | Preparation process of antibacterial shape memory simulation hair |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102174742B (en) | 2012-12-19 |
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