CN106245118A - The production method of anion Bombyxmori Linnaeus silk flosssilk wadding - Google Patents
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding Download PDFInfo
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- CN106245118A CN106245118A CN201610622601.5A CN201610622601A CN106245118A CN 106245118 A CN106245118 A CN 106245118A CN 201610622601 A CN201610622601 A CN 201610622601A CN 106245118 A CN106245118 A CN 106245118A
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01B—MECHANICAL TREATMENT OF NATURAL FIBROUS OR FILAMENTARY MATERIAL TO OBTAIN FIBRES OF FILAMENTS, e.g. FOR SPINNING
- D01B7/00—Obtaining silk fibres or filaments
- D01B7/02—Cleaning or classifying silk cocoons
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01C—CHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
- D01C3/00—Treatment of animal material, e.g. chemical scouring of wool
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Abstract
The present invention discloses the production method of a kind of anion Bombyxmori Linnaeus silk flosssilk wadding, comprises the following steps that: (1) Bombyx bombycis remove impurity；(2) silk floss is played: used by Bombyx bombycis and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60 70 DEG C, concentration expressed in percentage by weight be 3 5% sodium hydroxide solution carry out boiling continuous 23 hours, boil silk floss and terminate first 35 minutes, in boiling continuous solution, add anionic finishing agent；(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting in fermentation vat immersion 12 hours, has softening agent and nertralizer in fermentation vat；(5) last phase tidying up；(6) high-temperature sterilization；(7) Product checking: guarantee that the pH value of silk flosssilk wadding sheet, oil content, impure amount and water content all meet international standard, get final product packaging and warehousing.The present invention produces that the silk cotton anion burst size that obtains is big, is uniformly dispersed.
Description
Technical field
The present invention relates to Textile Engineering technical field, specifically contain the production method of the Bombyxmori Linnaeus silk flosssilk wadding of electronegative ion.
Background technology
Anion, to the health of people, long-lived and ecological significant impact, has been that domestic and international medical circle expert is by clinical real
Trample and verified.Contemporary science has opened bioelectric secret, and each cell of organism is exactly a micro cell, in cell membrane
Having outward the potential difference of 50-90mv, supplement if " cell battery " can not get sufficient electric charge, the electric process of body is difficult to continue
Continuous maintenance, thus have influence on the normal activity of body, produce aging and senilism.
Polluting few place in forest, beach, waterfall, countryside etc., containing substantial amounts of anion air, its concentration is for polluting
Serious urban hundred times, here people can feel with fresh air, breathe happy, relaxation and happiness, relaxed and joyful, here it is many
The effect that many anion air produce.Therefore anion air is referred to as " long-lived element " or " air vitamin " by people.
Anionic additive, is the principle of human use's nature generation anion, synthetic or the one of proportioning
Complex mineral, is to be processed through refinement polymerization, extra-fine grinding by natural minerals, and typically all tourmaline powder adds lanthanide series
Or rare earth element.Surfactant can be added make liquid additive with after infrared ray radiation；Pottery can also be made an addition to
In goods, make product have under resting state and excite the function discharging high-concentration anion, make tourmaline, can effectively reduce water
Matter oxidation-reduction potential, to reach sterilization, sterilization, neutralize the effects such as pH value.
The effect of anionic additive is mainly reflected in: the negative aeroion generating function that (1) is permanent: in air, gas divides
The mechanism of son ionization, mainly by the extraneous ionizer result to gas effect, ionizer has ultraviolet, lonizing radiation, photoelectric effect
Deng.Composition in anionic additive has pyroelectricity and a piezoelectricity, therefore in the case of having temperature and pressure change (even if
Small change) electric potential difference between composition crystal can be caused, this electrostatic is up to 1,000,000 electron-volts, so that air is sent out
Raw ionization, that is hit is electronically attached to neighbouring water and oxygen molecule and makes it be converted into negative aeroion, i.e. negative oxygen ion.
(2) stronger far-infrared transmitting function: the composition in anionic additive be characterized with boracic aluminum, sodium, ferrum, the ring-type knot of lithium
The silicate material of structure, isomorph is grown, because of its pyroelectricity and piezoelectricity so that it is polar ion draws in equilbrium position vibration
Play dipole moment change and produce the electromagnetic radiation of far infrared band, if adding (such as fiber) in product by a certain percentage to so that it is
Produce radiation by the free ion of self, impurity ion and ionic substance, impurity and two, three phonon sympathetic responses, affected
The ionic bond polarity vibration that machine interlinks with inorganic molecule, defines stronger radiation broadband, according to test anionic additive to far
Infrared emissivity is more than 90%.The far infrared performance of anionic additive the health care of human body and other effect are mainly had with
Under several aspectsFar infrared can accelerate moisture movement, makes light water become activated water, so that the penetration of water, diffusion
Power, dissolving power, metabolism power strengthen, and produce water conservation film.Far infrared, for blood circulation, can play expansion blood capillary,
Strengthen blood circulation, enhance metabolism, strengthen the effect of lymph circulation.Far infrared, for cell tissue, can make cell live
Changing, make the excretion of old dead cell or give regeneration capacity, can strengthen cellular energy, function and the vigor etc. that strengthen cell act on.(3)
Excellent antibiotic and sterilizing function: the negative oxygen ion produced in anionic additive has higher activity, has the strongest oxidation also
Original work cell membrane or the activity of cellular plasm organized enzyme that can destroy antibacterial, thus reach the purpose of antibiotic and sterilizing.
The purposes of anionic additive is presented as: (1) purificationization air: the anion in anionic additive is in atmosphere
Movement presents " Z " font.And carrying negative charge to antibacterial, dust, smoke particles and water droplet etc., this is micro-for electric charge and this
Grain combines and is polymerized to ball and sinks, thus reaches to purify the purpose of air.(2) foreign flavor indoors and various harmful gas are eliminated:
In benzene, formaldehyde, ketone, the irritative gas such as ammonia and daily life that the art work used during interior decoration evaporates
Leftovers leftovers acid smell, abnormal flavour that people is originally harmful to by medicated cigarette etc., with the wall cloth containing anionic additive, curtain etc. or containing anion
The coating of additive, the negative aeroion of its release can be eliminated effectively.(3) health-care effect: add through negative-ion fiber
The fabric of work such as clothes, sheet and the wallpaper of indoor decoration, carpet, or the coating etc. containing anionic additive, all have guarantor
Strong and environmental protection dual-use function, such as, make fabric in automobile with negative-ion fiber, can eliminate abnormal flavour in automobile, purify air, tune
The joint neural excitement of driver and inhibitory state, improve the mental status that cerebral cortex function keeps good.(4) at water
Reason: add filtering material with anionic additive and be used for water dispenser filtration core, antibacterial in water can be killed, increase oxygen in water,
Make bathroom towel with negative-ion fiber or process for bathroom water, moisture movement can be accelerated, make light water become activated water.
Increase energy, easily remove human body dirt, allaying tiredness.Treated water, for the load training of high-grade green plants indoor, can carry
The survival rate of high plant, and shorten the period of maturation, it is sprayed onto the blade face of flowers, the freshness date of flowers can be made to extend 5-10 times.Bear from
Other purposes of sub-additive: there is the effect purifying air, eliminating human-body fatigue, promote health.Additionally, this series is produced
Product also have antibacterial, degermation, and have obvious deodorization functions.This product can be used for fiber, with this weaving medicated clothing dress
When the person, it is possible to excite anion to human body continuously, human body is made to keep energetic；On the other hand again can be constantly
Eliminated internal discharged various internal rubbish by human body, meanwhile, have this function dress ornament will not because of the many reason of washing,
And reduce its effect.Additionally, this product can be additionally used in the coating of indoor, paint, it is possible to be placed directly in room as special
Plant air cleaner, deodorizer uses.
Silkworm silk is to integrate natural fiber light, soft, carefully in nature, have the good reputation of " human body Second Skin ", quilt
Industry is referred to as " fiber queen ".It is mainly composed of pure natural animal protein fibre, includes the necessary aminoacid of multiple human body, has
Radix Saposhnikoviae, dehumidify, calm the nerves, nourish and effect of balanced human's skin.Silkworm silk compliance and warmth retention property are splendid, and are prone to absorb and saturating
The antiperspirant gas that the health of analysis people produces in deep sleep.Silkworm silk is smooth, ventilative, soft, moisture absorption, the most perverse itch and the feature such as antistatic
Become make underclothes superior material for making clothes, and using silkworm silk as the silkworm silk quilt of endoplasm have more next to the skin warming, fluffy gently
Advantageous quality and the advantages such as soft, Breathable healthcare.
Along with society industrialization degree raising day by day, the pollution of air is increasingly severe, and the progress of science and technology and
Socioeconomic development enhances again the health care consciousness of people.Especially day by day seen clearly it when the mechanism of action of negative aeroion
After, a kind of fiber with anion function, attract domestic and international as the functional fibre that truly can improve environment
It is researched and developed by person.
Final finishing technology commonly used, continually developing of anion-generating material, significantly widen Negative ionic textile
Application.Anionic additive is added in silk cotton by people, allows silk cotton have effect of anion.Open source literature
Also the production method of some anion silk cottons is reported, such as:
1, Chinese patent: a kind of method of preparing silk by anion technology and the application in home textile product thereof, the applying date:
2009.7.16, application number: 200910054874.4, applicant: Shanghai Shuixing Domestic Textile Co., Ltd, address: 201401
Xi Du Shanghai-Hangzhou, south bridge town, Senior Residents in Fengxian District of Shanghai highway 1487, inventor: Li Yugao, easypro morning and evening, summary: this invention relates to weaving
Applied technical field, is specifically related to method and the application thereof of a kind of preparing silk by anion technology, in order to solve inorganic matter bear from
There is microgranule dispersing uniformity in silkworm silk, fastness, problem that durability is the highest in son, the invention provides a kind of with negative
Ion technology prepares the method for silkworm silk, and the method is with 100% Bombyxmori Linnaeus long filament as raw material, in Final finishing recombination process, adds and combines
Conjunction property anion generation auxiliary agent, uses the silkworm silk that this inventive method prepares, can effectively solve above-mentioned technical problem.
2, Chinese patent: a kind of novel negative ion regenerated silk fiber and preparation method thereof, application number:
201510056071.8, the applying date: 2015.02.03, applicant: Huzhou Jichang Silk Co., Ltd., address: 313026 Zhejiang
Province's Huzhou City Nanxun District and inspire confidence in Heng Gang village, town, inventor: Ren Xingen, summary: this disclosure of the invention a kind of novel negative ion regeneration
Silk fiber and preparation method thereof, the method comprises the following steps: after silkworm silk goes the removal of impurity, greasy dirt and degumming, through dissolving thoroughly
Analysis is concentrated to give regenerated silk fibroin solution, is mixed with anion whisker solution by regenerated silk fibroin solution, regulation solution
PH value, adds thickening agent, concentrates stirring and obtains spinning solution, and spinning solution obtains nascent fibroin fiber through dry spinning,
Fibroin fiber of finally coming into being processes through alcohol steam hot-stretch and obtains novel negative ion regenerated silk fiber.This invention is
Being fixed on inside silk fiber by anion crystal whisker materials, anion crystal whisker materials replaces the foldable structure in natural silk fiber
And persistently produce anion, novel negative ion regenerated silk fiber prepared by the method have with natural silk fiber-like as
Microstructure, and health-care effect is more preferably, the comfortable softness of fabric therefore prepared, air-moisture-permeable, and pro-skin keeps healthy.
It has been investigated that, in the existing functional fiber containing anionic additive, although be also added with a certain amount of negative
Ionic additive, but the air ion solubility that its product produces is the highest, and effect is the most lasting.
Summary of the invention
It is an object of the present invention to provide that a kind of anion burst size is big, be uniformly dispersed, anion Bombyxmori Linnaeus silk flosssilk wadding that effect is lasting
Production method.
It is an object of the invention to be achieved through the following technical solutions:
A kind of production method of anion Bombyxmori Linnaeus silk flosssilk wadding, it comprises the following steps that:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；Silkworm cocoon de-burring machine is Chinese patent, its Application No.: 200520092092.7, applicant: Yu Qingchun, address:
114300 autonomous county of the Manchu of Xiuyan, Liaoning Province Xiuyans town, silkworm cocoon de-burring machine, is by shell, screen cloth, aerofoil, stripping pawl, cylinder, skin
Tape handler, support shaft, driving motor, discharging opening, dust-exhausting port, feeding mouth are constituted, and the shell made iron plate is built with circle
Tubular screen cloth, in the axle center of screen cloth equipped with rotatable cylinder, the appearance at cylinder is mounted equidistant four rows vertically and shells pawl, in rolling
The aerofoil that one end installation has a length of 50～100cm, height is 5～10cm and spiral angle is 5～10 ° of cylinder, cylinder warp
Support shaft, belt gear, by driving driven by motor to rotate, are arranged over feeding mouth in the side of shell one end, shell another
The side-lower of end is provided with discharging opening, and surface is provided with dust-exhausting port；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；Make continuous machine from Tongxiang City tonneau
Machining factory buys, address: territory North Street, territory town, Zhejiang Province, China province Jiaxing City Tongxiang City 25；Network address: http: //
shop.cnsb.cn/introduce-1479980.html；Beating continuous 2-3 minute, the rotating speed of first minute scutcher is 300-350
Rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-
The sodium hydroxide solution of 5% carries out boiling continuous 2-3 hour, boils silk floss and terminates first 3-5 minute, adds anion finishing in boiling continuous solution
Agent；The addition of anionic finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；Described softness
Agent is that TF-404A, TF-404A buy from Tongxiang City chemical industry light textile Co., Ltd, address: Tongxiang City, Tongxiang City, Zhejiang is revived
South No.188, Road, network address: http://hcws0000148482.b2b.hc360.com.Described nertralizer is glacial acetic acid.
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection
Metal impurities also go the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet GB with water content, get final product packaging and warehousing.
Described anionic finishing agent can be bought from Shanghai Huan Gu new material development in science and technology company limited, network address:
Https: //bbaxx2002.1688.com, address: Room, No. 245 No. 3 buildings 703～706 of Shanghai, Xuhui District of Shanghai Jia Chuanlu.
Described anionic finishing agent can also be prepared voluntarily, and it is made up of the raw material of following parts by weight:
Tripolit 15～20 parts；
Opal 15～25 parts；
Tourmaline 12～13 parts；
Maifanitum 5～10 parts；
Gull rock 5～8 parts；
Rare earth 3～5 parts；
Hokutolite 2～4 parts；
Aluminium sesquioxide 2～3 parts；
Zirconium oxide 2～3 parts；
Sodium silicate 2～3 parts.
The preparation process of described anionic finishing agent is:
(1) tripolit 15～20 parts, opal 15～25 parts, tourmaline 12～13 parts, Maifanitum 5～10 are taken by weight
Part, gull rock 5～8 parts, rare earth 3～5 parts, hokutolite 2～4 parts, aluminium sesquioxide 2～3 parts, zirconium oxide 2～3 parts and sodium silicate
2～3 parts, it is then respectively adding in grinding equipment and carries out superfine grinding, until particle diameter distribution is 50～80nm；
(2) by the tripolit after superfine grinding, opal, tourmaline, Maifanitum, rare earth, hokutolite, aluminium sesquioxide, oxidation
Zirconium and sodium silicate mix homogeneously, then use infrared lamp to irradiate 3～5 minutes, obtain mixed powder；
(3) mixed powder is put in container, and add dehydrated alcohol and carry out ultrasound wave high-speed stirred, obtain suspension, then use
Infrared lamp irradiates 20 clocks～25 minutes,
(4) add clear water, lauryl alcohol and quaternary ammonium base the most in a reservoir, after stirring 1-1.5 hour, seal and preserve and get final product；Mixed powder
It is (3-5) with the weight ratio of clear water, lauryl alcohol and quaternary ammonium base: (10-15): 0.2:0.1.
The prominent substantive distinguishing features of the present invention with significantly progress is:
The production method of the anion Bombyxmori Linnaeus silk flosssilk wadding of the present invention is simple to operate, and labor intensity is low, can be processed into by Bombyx bombycis high-quality
Silk floss, the pH value of the silk floss obtained, oil content, impure amount, water content are all far superior to national standard.The anion of the present invention
The production method of Bombyxmori Linnaeus silk flosssilk wadding produces the silk floss ratio obtained and uses other method to process the high grade of silk floss obtained.The present invention
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding be to add anionic finishing agent in 3-5 minute before boiling silk floss and terminating, anion permeable arrives
In silk floss, be uniformly dispersed, enable mulberry silk to preserve anion for a long time so that negative ion concentration remain at one higher
Concentration, ion solubility is high, and effect is lasting.The present invention adds anionic finishing agent in 3-5 minute before boiling silk floss and terminating, and ratio processes
The high 200/cm of negative ion concentration of anion is added again after silk floss3Above, than the anion at other operation interpolation anion
The high 150/cm of concentration3Above, the holding time of anion is longer than traditional method more than 3 months.
Accompanying drawing explanation
Fig. 1 is the product of the anionic finishing agent that the Shanghai Huan Gu new material development in science and technology company limited that the present invention uses produces
Product figure；
Fig. 2 is to utilize the method for the present invention to produce the Bombyxmori Linnaeus silk flosssilk wadding the obtained examining report containing negative ion amount.
Detailed description of the invention
In order to make technical scheme and advantage clearer, below in conjunction with embodiments of the invention, to the present invention
Technical scheme be clearly and completely described.
Embodiment 1
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 3 minutes, adds anionic finishing agent in boiling continuous solution；Bear from
The addition of sub-finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent uses the anion finishing that Shanghai Huan Gu new material development in science and technology company limited produces
Agent.
Embodiment 2
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 4 minutes, adds anionic finishing agent in boiling continuous solution；Bear from
The addition of sub-finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent uses the anion finishing that Shanghai Huan Gu new material development in science and technology company limited produces
Agent.
Embodiment 3
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 5 minutes, adds anionic finishing agent in boiling continuous solution；Bear from
The addition of sub-finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent uses the anion finishing that Shanghai Huan Gu new material development in science and technology company limited produces
Agent.
Embodiment 4
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 3 minutes, adds anionic finishing agent in boiling continuous solution；Bear from
The addition of sub-finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent is made up of the raw material of following parts by weight:
Tripolit 15 parts；
15 parts of opal；
12 parts of tourmaline；
Maifanitum 5 parts；
Gull rock 5 parts；
Rare earth 3 parts；
Hokutolite 2 parts；
Aluminium sesquioxide 2 parts；
Zirconium oxide 2 parts；
Sodium silicate 2 parts.
The preparation process of described anionic finishing agent is:
(1) tripolit 15 parts, 15 parts of opal, 12 parts of tourmaline, Maifanitum 5 parts, gull rock 5 parts, rare earth 3 are taken by weight
Part, hokutolite 2 parts, aluminium sesquioxide 2 parts, zirconium oxide 2 parts and sodium silicate 2 parts, be then respectively adding in grinding equipment and surpass
It is finely divided, until particle diameter distribution is 50～80nm；
(2) by the tripolit after superfine grinding, opal, tourmaline, Maifanitum, rare earth, hokutolite, aluminium sesquioxide, oxidation
Zirconium and sodium silicate mix homogeneously, then use infrared lamp to irradiate 3～5 minutes, obtain mixed powder；
(3) mixed powder is put in container, and add dehydrated alcohol and carry out ultrasound wave high-speed stirred, obtain suspension, then use
Infrared lamp irradiates 20 clocks～25 minutes,
(4) add clear water, lauryl alcohol and quaternary ammonium base the most in a reservoir, after stirring 1-1.5 hour, seal and preserve and get final product；Mixed powder
It is 3:10:0.2:0.1 with the weight ratio of clear water, lauryl alcohol and quaternary ammonium base.
Embodiment 5
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 4 minutes, adds anionic finishing agent in boiling continuous solution；Bear from
The addition of sub-finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent is made up of the raw material of following parts by weight:
Tripolit 18 parts；
20 parts of opal；
12.5 parts of tourmaline；
Maifanitum 8 parts；
Gull rock 7 parts；
Rare earth 4 parts；
Hokutolite 3 parts；
Aluminium sesquioxide 2.5 parts；
Zirconium oxide 2.5 parts；
Sodium silicate 2.5 parts.
The preparation process of described anionic finishing agent is:
(1) tripolit 18 parts, 20 parts of opal, 12.5 parts of tourmaline, Maifanitum 8 parts, gull rock 7 parts, dilute is taken by weight
4 parts of soil, hokutolite 3 parts, aluminium sesquioxide 2.5 parts, zirconium oxide 2.5 parts and sodium silicate 2.5 parts, be then respectively adding grinding equipment
In carry out superfine grinding, until particle diameter distribution is 50～80nm；
(2) by the tripolit after superfine grinding, opal, tourmaline, Maifanitum, rare earth, hokutolite, aluminium sesquioxide, oxidation
Zirconium and sodium silicate mix homogeneously, then use infrared lamp to irradiate 3～5 minutes, obtain mixed powder；
(3) mixed powder is put in container, and add dehydrated alcohol and carry out ultrasound wave high-speed stirred, obtain suspension, then use
Infrared lamp irradiates 20 clocks～25 minutes,
(4) add clear water, lauryl alcohol and quaternary ammonium base the most in a reservoir, after stirring 1-1.5 hour, seal and preserve and get final product；Mixed powder
It is 4:12:0.2:0.1 with the weight ratio of clear water, lauryl alcohol and quaternary ammonium base.
Embodiment 6
Use following steps to produce and obtain anion Bombyxmori Linnaeus silk flosssilk wadding:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 3-5 minute, adds anionic finishing agent in boiling continuous solution；Negative
The addition of ion finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
Described softening agent is TF-404A.
Described nertralizer is glacial acetic acid.
Described silk floss of beating is to use to make continuous machine and carry out Bombyx bombycis playing silk floss 2-3 minute, and the rotating speed of first minute scutcher is
300-350 rpm, the rotating speed of remaining time scutcher is 1500-1800 rpm.
Described anionic finishing agent is made up of the raw material of following parts by weight:
Tripolit 20 parts；
25 parts of opal；
13 parts of tourmaline；
Maifanitum 10 parts；
Gull rock 8 parts；
Rare earth 5 parts；
Hokutolite 4 parts；
Aluminium sesquioxide 3 parts；
Zirconium oxide 3 parts；
Sodium silicate 3 parts.
The preparation process of described anionic finishing agent is:
(1) tripolit 20 parts, 25 parts of opal, 13 parts of tourmaline, Maifanitum 10 parts, gull rock 8 parts, rare earth are taken by weight
5 parts, hokutolite 4 parts, aluminium sesquioxide 3 parts, zirconium oxide 3 parts and sodium silicate 3 parts, be then respectively adding in grinding equipment and surpass
It is finely divided, until particle diameter distribution is 50～80nm；
(2) by the tripolit after superfine grinding, opal, tourmaline, Maifanitum, rare earth, hokutolite, aluminium sesquioxide, oxidation
Zirconium and sodium silicate mix homogeneously, then use infrared lamp to irradiate 5 minutes, obtain mixed powder；
(3) mixed powder is put in container, and add dehydrated alcohol and carry out ultrasound wave high-speed stirred, obtain suspension, then use
Infrared lamp irradiates 20 clocks～25 minutes,
(4) add clear water, lauryl alcohol and quaternary ammonium base the most in a reservoir, after stirring 1-1.5 hour, seal and preserve and get final product；Mixed powder
It is 5:15:0.2:0.1 with the weight ratio of clear water, lauryl alcohol and quaternary ammonium base.
Application Example
1, Yizhou, Guangxi company, uses the method for the present invention that Bombyx bombycis is processed into high-quality mulberry silk, the mulberry silk obtained
Continuous pH value, oil content, impure amount and each index of water content are all up to state standards, and obtain than other method processing of use
The high grade of silk floss, 200/cm higher than the negative ion concentration adding anion after processing silk floss again3Above, ratio is at it
Its operation adds the high 150/cm of negative ion concentration of anion3Above, and can preserve anion for a long time, negative ion concentration begins
It is maintained at a higher concentration eventually.
Described above is not limitation of the present invention, and the present invention is also not limited to examples detailed above, the art general
Logical technical staff, in the essential scope of the present invention, the change made, retrofits, adds or replaces, should belong to the guarantor of the present invention
Protect scope.
Claims (7)
1. the production method of an anion Bombyxmori Linnaeus silk flosssilk wadding, it is characterised in that: comprise the following steps that:
(1) Bombyx bombycis remove impurity: utilize silkworm cocoon de-burring machine to combine the most artificial selected remove impurity so that the Bombyx bombycis impurity content of production is the lowest
In GB；
(2) silk floss is played: used by the Bombyx bombycis after the most selected and make continuous machine and carry out dozen silk floss and obtain silk floss sheet；
(3) boil silk floss: re-use after silk floss sheet clean water is dehydrated temperature be 60-70 DEG C, concentration expressed in percentage by weight be 3-5%'s
Sodium hydroxide solution carries out boiling continuous 2-3 hour, boils silk floss and terminates first 3-5 minute, adds anionic finishing agent in boiling continuous solution；Negative
The addition of ion finishing agent is boil continuous liquor capacity 3%；
(4) dehydration is cleaned: boils after silk floss terminates, is first dehydrated by silk floss sheet, then through twice washing and be dehydrated, is finally putting into fermentation vat
Middle immersion 1-2 hour, the volume ratio having softening agent and nertralizer, softening agent and nertralizer in fermentation vat is 1:2；
(5) last phase tidying up: soak and after terminating, silk floss sheet is dehydrated, then by the most selected except rib, machine detection metal
Impurity also goes the removal of impurity；
(6) high-temperature sterilization: guarantee that each silk floss sheet produced is all after detection is qualified, then carry out high-temperature sterilization, sterilization temperature
Degree is for 250-300 DEG C, and the time is the 15-20 second；
(7) Product checking: the silk floss sheet after high-temperature sterilization is detected, it is ensured that the pH value of silk flosssilk wadding sheet, oil content, impure amount
All meet international standard with water content, get final product packaging and warehousing.
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 1, it is characterised in that: described softening agent is
TF-404A。
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 1, it is characterised in that: described nertralizer is ice
Acetic acid.
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 1, it is characterised in that: described silk floss of beating is to use
Making continuous machine to carry out Bombyx bombycis beating continuous 2-3 minute, the rotating speed of first minute scutcher is 300-350 rpm, the remaining time
The rotating speed of scutcher is 1500-1800 rpm.
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 1, it is characterised in that: described anion finishing
Agent uses the anionic finishing agent that Shanghai Huan Gu new material development in science and technology company limited produces.
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 1, it is characterised in that: described anion finishing
Agent is made up of the raw material of following parts by weight:
Tripolit 15～20 parts；
Opal 15～25 parts；
Tourmaline 12～13 parts；
Maifanitum 5～10 parts；
Gull rock 5～8 parts；
Rare earth 3～5 parts；
Hokutolite 2～4 parts；
Aluminium sesquioxide 2～3 parts；
Zirconium oxide 2～3 parts；
Sodium silicate 2～3 parts.
The production method of anion Bombyxmori Linnaeus silk flosssilk wadding the most according to claim 6, it is characterised in that: described anion finishing
The preparation process of agent is:
(1) tripolit 15～20 parts, opal 15～25 parts, tourmaline 12～13 parts, Maifanitum 5～10 are taken by weight
Part, gull rock 5～8 parts, rare earth 3～5 parts, hokutolite 2～4 parts, aluminium sesquioxide 2～3 parts, zirconium oxide 2～3 parts and sodium silicate
2～3 parts, it is then respectively adding in grinding equipment and carries out superfine grinding, until particle diameter distribution is 50～80nm；
(2) by the tripolit after superfine grinding, opal, tourmaline, Maifanitum, rare earth, hokutolite, aluminium sesquioxide, oxidation
Zirconium and sodium silicate mix homogeneously, then use infrared lamp to irradiate 3～5 minutes, obtain mixed powder；
(3) mixed powder is put in container, and add dehydrated alcohol and carry out ultrasound wave high-speed stirred, obtain suspension, then use
Infrared lamp irradiates 20 clocks～25 minutes,
(4) add clear water, lauryl alcohol and quaternary ammonium base the most in a reservoir, after stirring 1-1.5 hour, seal and preserve and get final product；Mixed powder
It is (3-5) with the weight ratio of clear water, lauryl alcohol and quaternary ammonium base: (10-15): 0.2:0.1.
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| CN106498623A (en) * | 2017-01-03 | 2017-03-15 | 兴化市大地蓝绢纺有限公司 | A kind of preparation method of Sang Mianqiu |
| CN106724480A (en) * | 2017-01-03 | 2017-05-31 | 兴化市大地蓝绢纺有限公司 | A kind of preparation method of silk wadding quilt |
| CN107348885A (en) * | 2017-07-13 | 2017-11-17 | 芜湖慧宇商贸有限公司 | A kind of preparation method of fibroin albumen towel |
| CN108754857A (en) * | 2018-05-15 | 2018-11-06 | 苏州先蚕丝绸有限公司 | Functional silk quilt |
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| CN115491898A (en) * | 2022-10-27 | 2022-12-20 | 浙江蚕缘家纺股份有限公司 | Manufacturing process of spring silk |
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Application publication date: 20161221 |