CN102174741B - Methods for preparing keratin surfactant and wigs - Google Patents
Methods for preparing keratin surfactant and wigs Download PDFInfo
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- CN102174741B CN102174741B CN201110029335.2A CN201110029335A CN102174741B CN 102174741 B CN102174741 B CN 102174741B CN 201110029335 A CN201110029335 A CN 201110029335A CN 102174741 B CN102174741 B CN 102174741B
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Abstract
The invention provides a method for preparing a keratin surfactant. The method comprises the following steps: 102. dissolving keratin with organic salt to obtain dissolved solution; 104. removing impurities from the dissolved solution and decoloring the dissolved solution and then dialyzing the dissolved solution; and 106. adjusting the pH value of the treated dissolved solution and adding 0.8-1.2% of antibacterial agent to obtain the keratin surfactant. The invention also provides a method for preparing wigs. By using the technical scheme provided by the invention, a layer of keratin with the same chemical ingredients as the human hairs can be adhered to the surfaces of the wigs, so that the wigs become as soft and smooth as the human hairs and have good affinity to human bodies and good health care effect.
Description
Technical field
The present invention relates to the hairpiece field, more specifically, relate to the preparation method of a kind of keratin surfactant and wig.
Background technology
Along with the continuous development and the growth of hair product industry, people's hair plait raw material is fewer and feweri, and domestic stranger sends out resource and peters out, and presses for to seek the substitute that a kind of people sends out resource.
Some enterprises substitute with animal ceratin fibers such as long ox hair, oxtail, long wool, horse hair, horse-hairs, but because the growth cycle of these animal ceratin fibers is grown, yielded poorly, far can not satisfy the wilderness demand in market.
In recent years, occurred the chemical fibre silk that makes with chemical fibre on the market, substituted natural hair and make hair products, because the chemical fibre silk is cheap and easy to get, so it has obtained fast development.Though chemical fiber hairs can substitute natural hair at aspects such as shape, dyeability and Nai La intensity; But its chemical composition and natural hair are completely different, when alternative people produces hair products, have some problems, and be relatively poor like its hygroscopicity, gas permeability, warmth retention property; And can not show a candle to natural human with the compatibility of human body sends out; People's long periods of wear can be felt sulks, not bulk, not submissive, even skin disease can occur, influences the application and the development of chemical fiber hairs.
Also useful at home and abroad in the recent period animal/vegetable protein and chemical fibre macromolecular compound mix; Make spinning solution and carry out wire drawing; Make the chemical fibre azelon and produce hair products; But,, do not possess the shortcoming of the affine health care of human body so it still exists absorption of perspiration, gas permeability poor because the chemical fibre macromolecular compound in this product mostly concentrates on the surface of product.
Summary of the invention
Send out in order to solve above-mentioned existing people that the substitute absorption of perspiration is poor, gas permeability, warmth retention property are poor, sulks, not bulk, not submissive, with problem such as human body compatibility difference or one of at least; The present invention provides a kind of preparation method of wig; Improve the moisture absorption of chemical fiber hairs, ventilative, thermal property, and with the affinity of human body.
In view of this, the invention provides a kind of method for preparing the keratin surfactant, comprising: step 102, use organic salt dissolving keratin to obtain lysate; Step 104 is carried out removal of impurities to said lysate and is handled with decolouring, more said lysate is carried out dialysis and handles; Step 106; Regulate the pH value of the said lysate of handling; And add 0.8%～1.2% antiseptic and obtain the keratin surfactant, wherein, said organic salt comprises anion and CATION; Said anion is chlorion or acetate ion, and said CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole.
In technique scheme, preferably, said dialysis is twice dialysis, is respectively applied for the keratin protein of removing molecular weight M＞10000 in the said lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
In technique scheme, preferably, the pH value of regulating the said lysate of said processing is 7.5～9.0.
In technique scheme, preferably, said keratin comprise following one of at least or its combination: the people sends out, animal hair and/or livestock angle hoof chip.
The present invention also provides a kind of method for preparing wig, comprising: step 202, immerse chemical fiber hairs in the described keratin surfactant; Step 204 has the said keratin surfactant of said chemical fiber hairs to be placed in the ultrasonic device immersion; Step 206, after the ultrasonic vibration that said ultrasonic device sends, said keratin is adsorbed in said chemical fiber hairs surface, obtains wig.
In technique scheme, preferably, the concentration of said keratin surfactant is 15%～16%.
In technique scheme, preferably, be that 48 ℃～52 ℃ keratin surfactants that will be soaked with said chemical fiber hairs down carry out ultrasonic in temperature.
In technique scheme, preferably, comprise that also it is 25%～35% (NH that said wig is immersed concentration
4)
2SO
4In the solidification liquid.
In technique scheme; Preferably, said wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes said wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards said wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
According to the method for preparing wig provided by the invention, make wig surface attachment one deck and people send out the identical keratin protein of chemical composition, the wig silk is become with the people send out to have the wig that softness, smooth and easy and human body have good affinity and health properties the same.
Description of drawings
Fig. 1 is the flow chart for preparing the method for keratin surfactant according to an embodiment of the invention;
Fig. 2 is the flow chart for preparing the method for wig according to an embodiment of the invention.
The specific embodiment
In order more to be expressly understood above-mentioned purpose of the present invention, feature and advantage, the present invention is further described in detail below in conjunction with the accompanying drawing and the specific embodiment.
Set forth a lot of details in the following description so that make much of the present invention, still, the present invention can also adopt other to be different from other modes described here and implement, and therefore, the present invention is not limited to the restriction of following disclosed specific embodiment.
Fig. 1 is the flow chart for preparing the method for keratin surfactant according to an embodiment of the invention.
As shown in Figure 1, the invention provides a kind of method for preparing the keratin surfactant, comprising: step 102, use organic salt dissolving keratin to obtain lysate; Step 104 is carried out removal of impurities to lysate and is handled with decolouring, again lysate is carried out dialysis and handles; Step 106; Regulate the pH value of the lysate of handling; And add 0.8%～1.2% antiseptic and obtain the keratin surfactant, wherein, organic salt comprises anion and CATION; Anion is chlorion or acetate ion, and CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole.
In technique scheme, dialysis is twice dialysis, is respectively applied for the keratin protein of removing molecular weight M＞10000 in the lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
In technique scheme, the pH value of regulating the lysate of handling is 7.5～9.0.
In technique scheme, said keratin comprises one or more in the following combination: the people sends out, animal hair and/or livestock angle hoof chip.
The present invention also provides a kind of method for preparing wig, comprising: step 202, immerse chemical fiber hairs in the described keratin surfactant; Step 204 has the said keratin surfactant of chemical fiber hairs to be placed in the ultrasonic device immersion; Step 206, after the ultrasonic vibration that ultrasonic device sends, said keratin is adsorbed in said chemical fiber hairs surface, obtains wig.
In technique scheme, the concentration of said keratin surfactant is 15%～16%.
In technique scheme, be that 48 ℃～52 ℃ keratin surfactants that will be soaked with chemical fiber hairs down carry out ultrasonic in temperature.
In technique scheme, comprise that also it is 25%～35% (NH that wig is immersed concentration
4)
2SO
4In the solidification liquid.
In technique scheme, wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
The post-treatment agent that the present invention adopted is a silicone softening agent; Main component is a dimethyl silicone polymer; It is the grease that water white transparency, nontoxic nothing are smelt; Having good heat resistance, high temperature resistant, resistance to low temperature, is desirable liquid spring, emulation of the present invention is sent out possessed submissive, resilient characteristics.
A specific embodiment for preparing the method for wig provided by the invention is:
The keratin surfactant solution of putting into the chemical fiber hairs goods concentration 15% floods, and under 50 ℃ of temperature, handles through ultrasonic oscillation; After making keratin protein be adsorbed in chemical fibre silk surface; Shift out chemical fibre silk or chemical fibre product,, clean with soft water then through 100 ℃ of following preliminary dryings of 30 minutes with 120 ℃ of following 2 minutes bake; Carry out the post processing oven dry with after treatment aid, promptly get high submissive antibiotic wig product.
According to the method for preparing wig provided by the invention, make wig surface attachment one deck and people send out the identical keratin protein of chemical composition, the wig silk is become with the people send out to have the wig that softness, smooth and easy and human body have good affinity and health properties the same.
The above is merely the preferred embodiments of the present invention, is not limited to the present invention, and for a person skilled in the art, the present invention can have various changes and variation.All within spirit of the present invention and principle, any modification of being done, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a method for preparing wig is characterized in that, comprising:
Step 202 immerses chemical fiber hairs in the keratin surfactant;
Step 204 has the said keratin surfactant of said chemical fiber hairs to be placed in the ultrasonic device immersion;
Step 206, after the ultrasonic vibration that said ultrasonic device sends, said keratin is adsorbed in said chemical fiber hairs surface, obtains wig;
Wherein said keratin surfactant obtains through following steps:
Step 102 uses organic salt dissolving keratin to obtain lysate;
Step 104 is carried out removal of impurities to said lysate and is handled with decolouring, more said lysate is carried out dialysis and handles;
Step 106 is regulated the pH value of the said lysate of handling, and adds 0.8%～1.2% antiseptic, obtains the keratin surfactant;
Wherein, said organic salt comprises anion and CATION, and said anion is chlorion or acetate ion, and said CATION is N, N-methylimidazole ion, and the pH value of regulating the said lysate of said processing is 7.5～9.0.
2. the method for preparing wig according to claim 1; It is characterized in that; Said dialysis is twice dialysis, is respectively applied for the keratin protein of removing molecular weight M＞10000 in the said lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
3. the method for preparing wig according to claim 1 is characterized in that, said keratin comprises that the people sends out, animal hair and/or livestock angle hoof chip.
4. according to each described method for preparing wig in the claim 1 to 3, it is characterized in that the concentration of said keratin surfactant is 15%～16%.
5. the method for preparing wig according to claim 4 is characterized in that, is that 48 ℃～52 ℃ keratin surfactants that will be soaked with said chemical fiber hairs down carry out ultrasonic in temperature.
6. the method for preparing wig according to claim 5 is characterized in that, comprises that also it is 25%～35% (NH that said wig is immersed concentration
4)
2SO
4In the solidification liquid.
7. according to each described method for preparing wig in the claim 1 to 3; It is characterized in that, said wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes said wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards said wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
8. the method for preparing wig according to claim 4; It is characterized in that, said wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes said wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards said wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
9. the method for preparing wig according to claim 5; It is characterized in that, said wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes said wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards said wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
10. the method for preparing wig according to claim 6; It is characterized in that, said wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes; Preliminary drying after finishing bakes said wig; Under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards said wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029335.2A CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029335.2A CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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| Publication Number | Publication Date |
|---|---|
| CN102174741A CN102174741A (en) | 2011-09-07 |
| CN102174741B true CN102174741B (en) | 2012-12-12 |
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| CN201110029335.2A Active CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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| CN103710978A (en) * | 2013-11-25 | 2014-04-09 | 中原工学院 | Preparation method of green multifunctional pure cotton fabric |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1660901A (en) * | 2004-12-24 | 2005-08-31 | 中国科学院长春应用化学研究所 | Method for preparing solution of keratin |
| CN1699646A (en) * | 2005-06-06 | 2005-11-23 | 保利源(南通)实业有限公司 | Animal protein artificial hair and its production method |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08226017A (en) * | 1995-02-17 | 1996-09-03 | Kanegafuchi Chem Ind Co Ltd | Composite fiber and its production |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1660901A (en) * | 2004-12-24 | 2005-08-31 | 中国科学院长春应用化学研究所 | Method for preparing solution of keratin |
| CN1699646A (en) * | 2005-06-06 | 2005-11-23 | 保利源(南通)实业有限公司 | Animal protein artificial hair and its production method |
Non-Patent Citations (3)
| Title |
|---|
| JP特开平8-226017A 1996.09.03 |
| 彭德智."可溶角蛋白的制取和用途".《牲骨的综合利用》.1982,(第1版),第175-176页. |
| 郭艺雯等."羊毛溶解再利用的研究现状".《武汉科技学院学报》.2006,第19卷(第2期),第25-29页. |
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| CN102174741A (en) | 2011-09-07 |
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