CN102174741A - Methods for preparing keratin surfactant and wigs - Google Patents
Methods for preparing keratin surfactant and wigs Download PDFInfo
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- CN102174741A CN102174741A CN2011100293352A CN201110029335A CN102174741A CN 102174741 A CN102174741 A CN 102174741A CN 2011100293352 A CN2011100293352 A CN 2011100293352A CN 201110029335 A CN201110029335 A CN 201110029335A CN 102174741 A CN102174741 A CN 102174741A
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- keratin
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- lysate
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Abstract
The invention provides a method for preparing a keratin surfactant. The method comprises the following steps: 102. dissolving keratin with organic salt to obtain dissolved solution; 104. removing impurities from the dissolved solution and decoloring the dissolved solution and then dialyzing the dissolved solution; and 106. adjusting the pH value of the treated dissolved solution and adding 0.8-1.2% of antibacterial agent to obtain the keratin surfactant. The invention also provides a method for preparing wigs. By using the technical scheme provided by the invention, a layer of keratin with the same chemical ingredients as the human hairs can be adhered to the surfaces of the wigs, so that the wigs become as soft and smooth as the human hairs and have good affinity to human bodies and good health care effect.
Description
Technical field
The present invention relates to the hairpiece preparation field, more specifically, relate to the preparation method of a kind of keratin surfactant and wig.
Background technology
Along with the continuous development and the growth of hair product industry, people's hair plait raw material is fewer and feweri, and domestic stranger sends out resource and peters out, and presses for to seek the substitute that a kind of people sends out resource.
Some enterprises substitute with animal ceratin fibers such as long ox hair, oxtail, long wool, horse hair, horse-hairs, but because the growth cycle of these animal ceratin fibers is grown, yielded poorly, far can not satisfy the wilderness demand in market.
In recent years, occurred the chemical fibre silk that makes with chemical fibre on the market, substituted natural hair and make hair products, because the chemical fibre silk is cheap and easy to get, so it has obtained fast development.Though chemical fiber hairs can substitute natural hair at aspects such as shape, dyeability and Nai La intensity, but its chemical composition and natural hair are completely different, when producing hair products, alternative people has some problems, relatively poor as its hygroscopicity, gas permeability, warmth retention property, and can not show a candle to natural human with the compatibility of human body sends out, people's long periods of wear can be felt sulks, not bulk, not submissive, even skin disease can occur, influences the application and the development of chemical fiber hairs.
Also useful at home and abroad in the recent period animal/vegetable protein and chemical fibre macromolecular compound mix, make spinning solution and carry out wire drawing, make the chemical fibre azelon and produce hair products, but because the chemical fibre macromolecular compound in this product mostly concentrates on the surface of product, so it still exists absorption of perspiration, gas permeability poor, do not possess the shortcoming of the affine health care of human body.
Summary of the invention
Send out in order to solve above-mentioned existing people that the substitute absorption of perspiration is poor, gas permeability, warmth retention property are poor, sulks, not bulk, not submissive, with problem such as human body compatibility difference or one of at least, the invention provides a kind of preparation method of wig, improve the moisture absorption of chemical fiber hairs, ventilative, thermal property, and with the affinity of human body.
In view of this, the invention provides a kind of method for preparing the keratin surfactant, comprising: step 102, use organic salt dissolving keratin to obtain lysate; Step 104 is carried out removal of impurities and decolouring processing to described lysate, more described lysate is carried out dialysis and handles; Step 106, regulate the pH value of the described lysate of handling, and add 0.8%～1.2% antiseptic and obtain the keratin surfactant, wherein, described organic salt comprises anion and CATION, described anion is chlorion or acetate ion, and described CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole.
In technique scheme, preferably, described dialysis is twice dialysis, is respectively applied for the keratin protein of removing molecular weight M＞10000 in the described lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
In technique scheme, preferably, the pH value of regulating the described lysate of described processing is 7.5～9.0.
In technique scheme, preferably, described keratin comprise following one of at least or its combination: the people sends out, animal hair and/or livestock angle hoof chip.
The present invention also provides a kind of method for preparing wig, comprising: step 202, immerse chemical fiber hairs in the described keratin surfactant; Step 204 has the described keratin surfactant of described chemical fiber hairs to be placed in the ultrasonic device immersion; Step 206, after the ultrasonic vibration that described ultrasonic device sends, described keratin is adsorbed in described chemical fiber hairs surface, obtains wig.
In technique scheme, preferably, the concentration of described keratin surfactant is 15%～16%.
In technique scheme, preferably, be that 48 ℃～52 ℃ keratin surfactants that will be soaked with described chemical fiber hairs down carry out ultrasonic in temperature.
In technique scheme, preferably, comprise that also it is 25%～35% (NH that described wig is immersed concentration
4)
2SO
4In the solidification liquid.
In technique scheme, preferably, described wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes, preliminary drying after finishing bakes described wig, under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards described wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
According to the method for preparing wig provided by the invention, make wig surface attachment one deck and people send out the identical keratin protein of chemical composition, the wig silk is become with the people send out to have the wig that softness, smooth and easy and human body have good affinity and health properties the same.
Description of drawings
Fig. 1 is the flow chart for preparing the method for keratin surfactant according to an embodiment of the invention;
Fig. 2 is the flow chart for preparing the method for wig according to an embodiment of the invention.
The specific embodiment
In order more to be expressly understood above-mentioned purpose of the present invention, feature and advantage, the present invention is further described in detail below in conjunction with the drawings and specific embodiments.
Set forth a lot of details in the following description so that fully understand the present invention, still, the present invention can also adopt other to be different from other modes described here and implement, and therefore, the present invention is not limited to the restriction of following public specific embodiment.
Fig. 1 is the flow chart for preparing the method for keratin surfactant according to an embodiment of the invention.
As shown in Figure 1, the invention provides a kind of method for preparing the keratin surfactant, comprising: step 102, use organic salt dissolving keratin to obtain lysate; Step 104 is carried out removal of impurities and decolouring processing to lysate, again lysate is carried out dialysis and handles; Step 106, regulate the pH value of the lysate of handling, and add 0.8%～1.2% antiseptic and obtain the keratin surfactant, wherein, organic salt comprises anion and CATION, anion is chlorion or acetate ion, and CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole.
In technique scheme, dialysis is twice dialysis, is respectively applied for the keratin protein of removing molecular weight M＞10000 in the lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
In technique scheme, the pH value of regulating the lysate of handling is 7.5～9.0.
In technique scheme, described keratin comprises one or more in the following combination: the people sends out, animal hair and/or livestock angle hoof chip.
The present invention also provides a kind of method for preparing wig, comprising: step 202, immerse chemical fiber hairs in the described keratin surfactant; Step 204 has the described keratin surfactant of chemical fiber hairs to be placed in the ultrasonic device immersion; Step 206, after the ultrasonic vibration that ultrasonic device sends, described keratin is adsorbed in described chemical fiber hairs surface, obtains wig.
In technique scheme, the concentration of described keratin surfactant is 15%～16%.
In technique scheme, be that 48 ℃～52 ℃ keratin surfactants that will be soaked with chemical fiber hairs down carry out ultrasonic in temperature.
In technique scheme, comprise that also it is 25%～35% (NH that wig is immersed concentration
4)
2SO
4In the solidification liquid.
In technique scheme, wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes, preliminary drying after finishing bakes wig, under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
Post-treatment agent of the present invention is a silicone softening agent, main component is a dimethyl silicone polymer, it is the grease that water white transparency, nontoxic nothing are smelt, have good heat resistance, high temperature resistant, resistance to low temperature, be desirable liquid spring, emulation of the present invention sent out possessed submissive, resilient characteristics.
A specific embodiment for preparing the method for wig provided by the invention is:
The keratin surfactant solution of the chemical fiber hairs goods being put into concentration 15% floods, under 50 ℃ of temperature, handle through ultrasonic oscillation, after making keratin protein be adsorbed in chemical fibre silk surface, shift out chemical fibre silk or chemical fibre product,, clean with soft water then through 100 ℃ of following preliminary dryings of 30 minutes with 120 ℃ of following 2 minutes bake, carry out the post processing oven dry with after treatment aid, promptly get high submissive antibiotic wig product.
According to the method for preparing wig provided by the invention, make wig surface attachment one deck and people send out the identical keratin protein of chemical composition, the wig silk is become with the people send out to have the wig that softness, smooth and easy and human body have good affinity and health properties the same.
The above is the preferred embodiments of the present invention only, is not limited to the present invention, and for a person skilled in the art, the present invention can have various changes and variation.Within the spirit and principles in the present invention all, any modification of being done, be equal to replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. a method for preparing the keratin surfactant is characterized in that, comprising:
Step 102 uses organic salt dissolving keratin to obtain lysate;
Step 104 is carried out removal of impurities and decolouring processing to described lysate, more described lysate is carried out dialysis and handles;
Step 106 is regulated the pH value of the described lysate of handling, and adds 0.8%～1.2% antiseptic, obtains the keratin surfactant,
Wherein, described organic salt comprises anion and CATION, and described anion is chlorion or acetate ion, and described CATION is N-N-methylimidazole, 1-2 base or 3-methylimidazole.
2. the method for preparing the keratin surfactant according to claim 1, it is characterized in that, described dialysis is twice dialysis, be respectively applied for the keratin protein of removing molecular weight M＞10000 in the described lysate and the keratin protein of molecular weight M＜3000, to obtain the keratin protein of molecular weight 3000≤M≤10000.
3. the method for preparing the keratin surfactant according to claim 2 is characterized in that, the pH value of regulating the described lysate of described processing is 7.5～9.0.
4. the method for preparing the keratin surfactant according to claim 3 is characterized in that, described keratin comprises that the people sends out, animal hair and/or livestock angle hoof chip.
5. a method for preparing wig is characterized in that, comprising:
Step 202 immerses chemical fiber hairs as in each described keratin surfactant of claim 1 to 4;
Step 204 has the described keratin surfactant of described chemical fiber hairs to be placed in the ultrasonic device immersion;
Step 206, after the ultrasonic vibration that described ultrasonic device sends, described keratin is adsorbed in described chemical fiber hairs surface, obtains wig.
6. the method for preparing wig according to claim 5 is characterized in that, the concentration of described keratin surfactant is 15%～16%.
7. the method for preparing wig according to claim 6 is characterized in that, is that 48 ℃～52 ℃ keratin surfactants that will be soaked with described chemical fiber hairs down carry out ultrasonic in temperature.
8. the method for preparing wig according to claim 7 is characterized in that, comprises that also it is 25%～35% (NH that described wig is immersed concentration
4)
2SO
4In the solidification liquid.
9. according to each described method for preparing wig in the claim 5 to 8, it is characterized in that, described wig is carried out preliminary drying, 100 ℃ of following preliminary dryings 20 to 40 minutes, preliminary drying after finishing bakes described wig, under 120 ℃, baked 1 to 3 minute, and baked and finish afterwards described wig to be cleaned with soft water, handle oven dry with post-treatment agent after clean the end.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029335.2A CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201110029335.2A CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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| Publication Number | Publication Date |
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| CN102174741A true CN102174741A (en) | 2011-09-07 |
| CN102174741B CN102174741B (en) | 2012-12-12 |
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| CN201110029335.2A Active CN102174741B (en) | 2011-01-27 | 2011-01-27 | Methods for preparing keratin surfactant and wigs |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103710978A (en) * | 2013-11-25 | 2014-04-09 | 中原工学院 | Preparation method of green multifunctional pure cotton fabric |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08226017A (en) * | 1995-02-17 | 1996-09-03 | Kanegafuchi Chem Ind Co Ltd | Composite fiber and its production |
| CN1660901A (en) * | 2004-12-24 | 2005-08-31 | 中国科学院长春应用化学研究所 | Method for preparing solution of keratin |
| CN1699646A (en) * | 2005-06-06 | 2005-11-23 | 保利源(南通)实业有限公司 | Animal protein artificial hair and its production method |
-
2011
- 2011-01-27 CN CN201110029335.2A patent/CN102174741B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH08226017A (en) * | 1995-02-17 | 1996-09-03 | Kanegafuchi Chem Ind Co Ltd | Composite fiber and its production |
| CN1660901A (en) * | 2004-12-24 | 2005-08-31 | 中国科学院长春应用化学研究所 | Method for preparing solution of keratin |
| CN1699646A (en) * | 2005-06-06 | 2005-11-23 | 保利源(南通)实业有限公司 | Animal protein artificial hair and its production method |
Non-Patent Citations (2)
| Title |
|---|
| 《武汉科技学院学报》 20060228 郭艺雯等 "羊毛溶解再利用的研究现状" 第25-29页 1-9 第19卷, 第2期 * |
| 《牲骨的综合利用》 19821231 彭德智 "可溶角蛋白的制取和用途" 第175-176页 1-9 , 第1版 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103710978A (en) * | 2013-11-25 | 2014-04-09 | 中原工学院 | Preparation method of green multifunctional pure cotton fabric |
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| CN102174741B (en) | 2012-12-12 |
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