Summary of the invention
The purpose of this invention is to provide a kind of is primary raw material with mung bean, red bean, black soya bean, compound cold-type yellow (clear) beverage that chrysanthemum, the fruit of Chinese wolfberry, dried orange peel, Radix Glycyrrhizae etc. produce for auxiliary material and preparation method thereof.
Three beans cold drinks provided by the present invention; By the raw material infuse of following mass parts after flavor mixing process: mung bean, red bean and black soya bean three beans leach 100 parts in clear juice; Chrysanthemum 0.5~1.0g part, 1.0~2.0 parts of the fruits of Chinese wolfberry, 0.5~1.0 part in 1.0~2.0 parts of dried orange peels and Radix Glycyrrhizae; The mass ratio that said three beans leach the clear juice of mung bean in the clear juice, the clear juice of red bean and the clear juice of black soya bean is (0.5~2): (0.5~2): (0.5~2).
Prepare the method for three beans cold drinks, comprise the steps:
1) with the clear juice of mung bean, the clear juice of red bean and the clear juice of black soya bean according to mass ratio (0.5~2): (0.5~2): the mixed of (0.5~2) obtains three beans and leaches clear juice;
2) chrysanthemum, the fruit of Chinese wolfberry, dried orange peel and Radix Glycyrrhizae are mixed according to above-mentioned mass parts, three beans that add said mass parts leach and carry out lixiviate, filtration in the clear juice, collect filtrating; Said filtrating is carried out flavor mixing, obtain three beans cold drinks through can and sterilization again.
Wherein, The clear juice of mung bean described in the step 1), the clear juice of red bean and the clear juice of black soya bean all prepare according to following method: mung bean or red bean or black soya bean are placed the water lixiviate; Filter then and collect leaching liquor, promptly obtain clear juice of mung bean or the clear juice of red bean or the clear juice of black soya bean.
Actual conditions to the mung bean lixiviate is following: the mass ratio of mung bean and water is 1: 5~1: 6, and temperature is 55~75 ℃, and the processing time is 1.5~2h; Actual conditions to the red bean lixiviate is following: the mass ratio of red bean and water is 1: 5~1: 6, and temperature is 55~75 ℃, and the processing time is 3.0~4.0h; Actual conditions to the black soya bean lixiviate is following: the mass ratio of black soya bean and water is 1: 5~1: 6, and temperature is 55~75 ℃, and the processing time is 2.0~3.0h.
After soaking, also need carry out the separating treatment of beans, juice, soon beans, juice blend are crossed 50 mesh sieves, collect the clear juice of mung bean, red bean and black soya bean respectively.
The condition of lixiviate step 2) is following: extraction temperature is 95~100 ℃, and extraction time is 15~35min.
The mode of filtering step 2) is a vacuum filtration.
After filtering, also should carry out flavor mixing to collected leaching liquor and handle.(100%, processing w/v) makes said leaching liquor pol reach 6~9% (Brix) to take to add an amount of high concentration rock sugar solution.
In the said process, after said allotment, also tackle product and carry out can and sterilization processing, the mode of said can and sterilization does not limit, specifically can be with reference to the concerned drink product.
The present invention is a base-material with three beans extracts, other be aided with chrysanthemum, the fruit of Chinese wolfberry, dried orange peel, Radix Glycyrrhizae etc. have the clearing liver of making eye bright, nourishing liver and kidney, invigorate the spleen and benefit qi, the medicinal food materials of effect such as clearing heat and detoxicating, through fully making the compound cold drink of three beans after the lixiviate.Product is brown, supernatant liquid, and local flavor is mellow, cool, thirst-quenching, and is comparatively close with the existing cold tea class drink form in market.But because of draw materials and be common raw-food material, security is higher.This product has improved its convenience and storage performance through incorporating modern food processing technology in addition, and product has market competition advantage and development prospect preferably.
The specific embodiment
The present invention will be described through specific embodiment below, but the present invention is not limited thereto.
Method described in the following embodiment like no specified otherwise, is conventional method; Said material like no specified otherwise, all can obtain from commercial sources.
Embodiment 1, three beans cold drinks and preparation method thereof
1) pretreatment of raw material
Take by weighing mung bean, red bean, each 100g of black soya bean respectively, flushing with clean water is clean.
2) lixiviate
Mung bean, red bean, the black soya bean cleaned are placed container, add the 500mL pure water respectively; In 60 ℃ of water-baths difference lixiviate 2.0h, 3.5h and 2.5h.
3) once filter and the filtrating merging
After a lixiviate, mung bean, red bean, black soya bean and leaching liquor are separately made separating treatment, adopt the screen filtration mode, sieve number is 50 orders, collects the clear juice of mung bean, red bean and black soya bean respectively; Said mung bean, red bean and black soya bean extractive juice are pressed 1: 1: 1 mass ratio of mass ratio and are mixed.
4) secondary lixiviate
With the clear juice of three beans that mixes, the ratio that adds 0.5g chrysanthemum, the 1.5g fruit of Chinese wolfberry, 1.0g dried orange peel, 0.5g Radix Glycyrrhizae according to every 100mL is prepared burden; The temperature of secondary lixiviate is 95 ℃, time 30min.
5) secondary filter
Secondary lixiviate material is removed big solid contents such as chrysanthemum earlier through coarse filtration; Remove a small amount of tiny residue through smart filter (200 order) again.
6) allotment
Collected lixiviate filtrating is carried out flavor mixing.(100%, w/v), every 100mL filtrating is added 6~7mL rock sugar solution to compounding high concentration rock sugar solution, and assurance final products pol is advisable at 6~9% (Brix).
7) can, sterilization
The product that allotment is good pours in the vial, and the sterilization of autoclave hydro-thermal, 121 ℃ of process for sterilizing, 15min are adopted in the sealing back; Cooling obtains final products.
Product quality and functional characteristics:
Organoleptic quality: this product is a dark brown clear liquid, and mouthfeel is sweet and tasty, and special beany flavour is arranged, and postpone for a long time possibly produce the microprecipitation that does not influence quality.
Nutrition and function quality: every this product of 100g heat content value >=24kcal, total solids content >=7.0g/100g, TAC are 6.65mmol/g, it is 90.2% that 10 times of dilutions are removed the DPPH free radical activity.
Experimental technique is following:
1) TAC test experiments: adopt TAC detection kit (FRAP method) to measure, this kit buying is biotechnology research institute (product serial number S0116) from the green skies.The method principle can be reduced Fe for polyphenoils under acid condition
3+(Ferric-tripyridyltriazine writes a Chinese character in simplified form Fe to-three pyridines three azines
3+The Fe of-TPTZ) generation blueness
2+-TPTZ measures blue Fe at 593nm
2+-TPTZ can obtain the TAC of this sample.Concrete operation method is seen the kit specification.The TAC of sample is with every mM Fe
2+The every gram sample of-TPTZ/ representes that unit is mmol/g.
2) remove the experiment of DPPH free radical activity:
With hexichol for bitter taste diazanyl free radical (DPPH, Technical grade, Sigma company, catalog number 43180) as target substance.Concrete assay method is: make 0.1mM DPPH solution with 95% ethanol (analyzing pure), add the 1.5ml testing sample in 1.5ml DPPH solution, with the vibration of whirlpool mixed instrument evenly, in room temperature held 30min, measure absorbance at the 517nm place, note is made A
1Substitute DPPH as reagent blank with 95% ethanol, record the absorbance note and make A
2Substitute sample as sample blank with 95% ethanol, record the absorbance note and make A
3Do the instrument zeroing with 95% ethanolic solution.Sample DPPH free radical scavenging activity computing formula is following:
DPPH free radical scavenging activity=(1-(A
1-A
2)/A
3) * 100%
A wherein
1: the DPPH+ sample; A
2: sample+95% ethanol; A
3: DPPH+95% ethanol.
Embodiment 2, a kind of three beans cold drinks and preparation method thereof
1) pretreatment of raw material
Take by weighing mung bean, red bean, black soya bean 500g, 500g, 250g respectively, flushing with clean water is clean.
2) lixiviate
Mung bean, red bean, the black soya bean cleaned are placed container, add 3000mL, 3000mL, 1500mL pure water respectively; In 75 ℃ of water-baths difference lixiviate 1.5h, 3.0h and 2.0h.
3) once filter and the filtrating merging
After a lixiviate, mung bean, red bean, black soya bean and leaching liquor are separately made separating treatment, adopt the screen filtration mode, sieve number is 50 orders, collects the clear juice of mung bean, red bean and black soya bean respectively; Said mung bean, red bean and black soya bean extractive juice mix by 1: 1: 0.5 mass ratio.
4) secondary lixiviate
With the clear juice of three beans that mixes, the ratio that adds 1.0g chrysanthemum, the 2.0g fruit of Chinese wolfberry, 1.5g dried orange peel, 1.0g Radix Glycyrrhizae according to every 100mL is prepared burden; The temperature of secondary lixiviate is 100 ℃, time 20min.
5) secondary filter is with consistent described in the embodiment 1.
6) allotment
Collected lixiviate filtrating is carried out flavor mixing.(100%, w/v), every 100mL filtrating is added 7~8mL rock sugar solution to compounding high concentration rock sugar solution, and assurance final products pol is advisable at 6~9% (Brix).
7) can, sterilization
With having allocated solution behind 150 ℃, the ultra high temperature short time sterilization of 4s, sterile filling is in Tetra Pak; Cooling obtains final products.
Product quality and functional characteristics:
Organoleptic quality: this product is a dark brown clear liquid, and mouthfeel is sweet and tasty, and special beany flavour is arranged, and postpone for a long time possibly produce the microprecipitation that does not influence quality.
Nutrition and function quality: every this product of 100g heat content value >=24kcal, total solids content >=7.0g/100g, TAC are 6.43mmol/g, it is 82.0% that 10 times of dilutions are removed the DPPH free radical activity.
Experimental technique is with embodiment 1 said unanimity.
Embodiment 3, a kind of three beans cold drinks and preparation method thereof
1) pretreatment of raw material
Take by weighing mung bean, red bean, black soya bean 1000g, 500g, 250g respectively, flushing with clean water is clean.
2) lixiviate
Mung bean, red bean, the black soya bean cleaned are placed container, add 5000mL, 2500mL, 1250mL pure water respectively; In 55 ℃ of water-baths difference lixiviate 2.0h, 4.0h and 3.0h.
3) once filter and the filtrating merging
After a lixiviate, mung bean, red bean, black soya bean and leaching liquor are separately made separating treatment, adopt the screen filtration mode, sieve number is 50 orders, collects the clear juice of mung bean, red bean and black soya bean respectively; Said mung bean, red bean and black soya bean extractive juice were by 2: 1: 0.5 mixed.
4) secondary lixiviate
With the clear juice of three beans that mixes, the ratio that adds 0.5g chrysanthemum, the 1.5g fruit of Chinese wolfberry, 1.5g dried orange peel, 0.8g Radix Glycyrrhizae according to every 100mL is prepared burden; The temperature of secondary lixiviate is 98 ℃, time 22min.
5) secondary filter is with consistent described in the embodiment 1.
6) allotment is with consistent described in the embodiment 1.
7) can, sterilization
With having allocated solution behind 135 ℃, the ultra high temperature short time sterilization of 8s, sterile filling is in Tetra Pak; Cooling obtains final products.
Product quality and functional characteristics:
Organoleptic quality: this product is a brown clear liquid, and mouthfeel is sweet and tasty, and special beany flavour is arranged, and postpone for a long time possibly produce the microprecipitation that does not influence quality.
Nutrition and function quality: every this product of 100g heat content value >=24kcal, total solids content >=7.0g/100g, TAC are 5.85mmol/g, it is 79.5% that 10 times of dilutions are removed the DPPH free radical activity.
Experimental technique is with embodiment 1 said unanimity.
Embodiment 4, a kind of three beans cold drinks and preparation method thereof
1) pretreatment of raw material
Take by weighing mung bean, red bean, each 5kg of black soya bean respectively, flushing with clean water is clean.
2) lixiviate
Mung bean, red bean, the black soya bean cleaned are placed container, add the 25L pure water respectively; In 65 ℃ of water-baths difference lixiviate 1.5h, 3.0h and 2.5h.
3) once filter and the filtrating merging
After a lixiviate, mung bean, red bean, black soya bean and leaching liquor are separately made separating treatment, adopt the screen filtration mode, sieve number is 50 orders, collects the clear juice of mung bean, red bean and black soya bean respectively; Said mung bean, red bean and black soya bean extractive juice were by 1: 1: 1 mixed.
4) secondary lixiviate
With the clear juice of three beans that mixes, the ratio that adds 0.8g chrysanthemum, the 1.5g fruit of Chinese wolfberry, 1.0g dried orange peel, 0.6g Radix Glycyrrhizae according to every 100mL is prepared burden; The temperature of secondary lixiviate is 95 ℃, time 35min.
5) secondary filter is with consistent described in the embodiment 1.
6) allotment is with consistent described in the embodiment 1.
7) can, sterilization are with consistent described in the embodiment 1.
Product quality and functional characteristics:
Organoleptic quality: this product is a dark brown clear liquid, and mouthfeel is sweet and tasty, and special beany flavour is arranged, and postpone for a long time possibly produce the microprecipitation that does not influence quality.
Nutrition and function quality: every this product of 100g heat content value >=24kcal, total solids content >=7.0g/100g, TAC are 7.15mmol/g, it is 87.9% that 10 times of dilutions are removed the DPPH free radical activity.
Experimental technique is with embodiment 1 said unanimity.
Embodiment 5, three beans cold drinks and preparation method thereof
1) pretreatment of raw material
Take by weighing mung bean, red bean, black soya bean 10kg, 5kg, 5kg respectively, flushing with clean water is clean.
2) lixiviate
Mung bean, red bean, the black soya bean cleaned are placed container, add 60L, 30L, 30L pure water respectively; In 75 ℃ of water-baths difference lixiviate 1.5h, 3.0h and 2.0h.
3) once filter and the filtrating merging
After a lixiviate, mung bean, red bean, black soya bean and leaching liquor are separately made separating treatment, adopt the screen filtration mode, sieve number is 50 orders, collects the clear juice of mung bean, red bean and black soya bean respectively; Said mung bean, red bean and black soya bean extractive juice were by 2: 1: 1 mixed.
4) secondary lixiviate
With the clear juice of three beans that mixes, the ratio that adds 1.0g chrysanthemum, the 2.0g fruit of Chinese wolfberry, 2.0g dried orange peel, 1.0g Radix Glycyrrhizae according to every 100mL is prepared burden; The temperature of secondary lixiviate is 95 ℃, time 35min.
5) secondary filter is with consistent described in the embodiment 1.
6) allotment is with consistent described in the embodiment 1.
7) can, sterilization are with consistent described in the embodiment 2.
Product quality and functional characteristics:
Organoleptic quality: this product is a dark brown clear liquid, and mouthfeel is sweet and tasty, and special beany flavour is arranged, and postpone for a long time possibly produce the microprecipitation that does not influence quality.
Nutrition and function quality: every this product of 100g heat content value >=24kcal, total solids content >=7.0g/100g, TAC are 6.55mmol/g, it is 79.3% that 10 times of dilutions are removed the DPPH free radical activity.
Experimental technique is with embodiment 1 said unanimity.