CN102132882A - DHA (Docosahexaenoic Acid) emulsion, production method and application thereof - Google Patents
DHA (Docosahexaenoic Acid) emulsion, production method and application thereof Download PDFInfo
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Abstract
The invention discloses DHA (Docosahexaenoic Acid) emulsion, comprising the following components in the mass percentage: 22-27% of DHA algal oil, 27-32% of packaging material, 40-45% of water, 0.02-0.05% of antioxidant, 3.0-5.0% of stabilizing and thickening agent, 0.1-0.3% of emulsifying agent and 2.0-3.0% of adhesive. The DHA emulsion is prepared by the following steps: firstly preparing a water phase and an oil phase, then mixing the materials, emulsifying, homogenizing and finally sterilizing. In application of preparing DHA beverages, the DHA emulsion is used as a nutrition enhancer and added to liquid milk, acid milk, various milk beverages, juice beverages, nutritional and sports beverages and foods in the proportion of 40-180mg/100g. The production process of the DHA emulsion is simple and feasible, the absorption and utilization ratio of DHA in a human body is high. When in use, the DHA emulsion has good dispersing performance, stable light resistance, oxygen resistance, acid and alkaline resistance and the like the functions of enhancing memory and thought and improving intelligence, high nutritional value, as well as extremely wide use range.
Description
Technical field
The present invention relates to a kind of DHA emulsion and production method and application.
Background technology
DHA, DHA, be commonly called as brain gold, be a kind of to the very important polyunsaturated fatty acid of human body, belong to the important member in the Omega-3 unrighted acid family, a series of symptoms be can cause during shortage, growth retardation, the skin abnormality scales of skin that peel off, sterile, dysnoesia etc. comprised.DHA is a kind of essential element that nervous system cell is grown and kept, be brain and amphiblestroid important composition composition, content is up to 20% in the human brain cortex, proportion maximum in eye retina, account for 50%, therefore, to human body, particularly infant intelligence and eyesight are grown most important.
The fragmentation kettle algae (Schizochytrium sp.) of being rich in DHA makes little algae DHA cell mud (being disclosed in the Chinese patent application 200910130628.2) through fermentation, concentrating and separating, through the homogeneous broken wall, carry that oil, crude oil are refining to obtain DHA algae oil, be added into the milk and the dairy products thereof that can obtain high DHA content in milk, goat milk etc. or its dairy products by wet method again.Spray-dried again, the embedding powder of DHA algae oil is added into the milk and the dairy products thereof that also can obtain high DHA content in milk, goat milk etc. or its dairy products by dry method.But DHA algae oil is exposed to very easily oxidation in the air, is vulnerable to the influence of extraneous physics and chemical factor, can not withstand high temperatures, thereby be difficult under its active condition of effective maintenance and directly be used in the various beverages.And for the DHA algae powder of microencapsulation, though comparatively effectively solved the defective of its easy oxidation inactivation, kept DHA activity in use, but also existing to add uses technology loaded down with trivial details, the defective that is difficult to mix, because embedded material is not ideal enough, there is certain limitation in its shelf-life in liquid beverage simultaneously, and energy consumption is high in the process of DHA algae oil microcapsuleization, has increased production cost greatly.
At the application present situation of DHA, the inventor studies it, and DHA algae oil is carried out specially treated, adds liquid milk, sour milk, various milk beverage, fruit drink again to, and in auxotype, sport type beverage and the food, this case produces thus.
Summary of the invention
The purpose of this invention is to provide a kind of DHA emulsion and production method and application, make the production technology simple possible, DHA is the absorption rate height in vivo, stable performance such as good dispersion property, fast light, oxytolerant (anti-oxidant), acid and alkali-resistance in liquid milk and various beverage during use.
In order to reach above-mentioned purpose, the technical solution used in the present invention is as follows:
The DHA emulsion, formulated by mass percentage by following raw materials according: DHA algae oil 22～27%; Packaging material 27～32%, water 40～45%, antioxidant 0.02～0.05% is stablized thickener 3.0～5.0%, emulsifying agent 0.1～0.3%, adhesive 2.0～3.0%.
Described DHA algae oil by the fragmentation kettle algae of being rich in DHA through the homogeneous broken wall, to carry oil, crude oil refining, emulsifying agent is selected polyglyceryl fatty acid ester or sucrose ester for use, stable thickener is selected carragheen, Arabic gum or xanthans for use, antioxidant is selected TBHQ, ascorbyl palmitate, vitamin E or lecithin for use, adhesive is selected corn syrup or white sugar for use, packaging material is selected converted starch for use, and water is the solvent that is used to regulate the dense dilution of batching.
The production method of DHA emulsion, its step is as follows:
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is slowly added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
The 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion.
The application of DHA emulsion in preparation DHA beverage added the DHA emulsion to liquid milk, sour milk, various milk beverage, fruit drink as nutrition fortifier in the ratio of 40～180mg/100g, in auxotype, sport type beverage and the food.
After adopting such scheme, the DHA emulsion content 10%DHA(quality percentage composition that the present invention makes), can be at liquid milk, sour milk, various milk beverage, fruit drink, directly add in auxotype, sport type beverage and the food or use with common interpolation of other batchings, addition is 40～180mg/100g, with the DHA content of fortification system.The use crowd includes but not limited to infant, children, teenager, pregnant woman or women breast-feeding their children.Described DHA emulsion directly interpolation is meant in view of uniformly dispersed energy in the good water of emulsion, can directly add with main mixing of materials in batching, and need not special even mixed dissolution process.
The specific embodiment
DHA emulsion production example
Embodiment 1
Preparation DHA algae oil addition is 22% DHA emulsion, and its each material content is as follows:
DHA algae oil 22Kg
Packaging material 27.88Kg
Water 45Kg
Antioxidant 0.02Kg
Stablize thickener 3Kg
Emulsifying agent 0.1Kg
Adhesive 2Kg
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is slowly added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
In the 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion, the DHA net content is in this DHA emulsion: 88mg/g.
Embodiment 2
Preparation DHA algae oil addition is 23% DHA emulsion, and its each material content is as follows:
DHA algae oil 23Kg
Packaging material 28Kg
Water 43.37Kg
Antioxidant 0.03Kg
Stablize thickener 3Kg
Emulsifying agent 0.1Kg
Adhesive 2.5Kg
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is slowly added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
In the 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion, the DHA net content is in this DHA emulsion: 92mg/g.
Embodiment 3
Preparation DHA algae oil addition is 25% DHA emulsion, and its each material content is as follows:
DHA algae oil 25Kg
Packaging material 28.56Kg
Water 40Kg
Antioxidant 0.04Kg
Stablize thickener 3.5Kg
Emulsifying agent 0.2Kg
Adhesive 2.7Kg
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is slowly added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
In the 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion, the DHA net content is in this DHA emulsion: 100mg/g.
Embodiment 4
Preparation DHA algae oil addition is 27% DHA emulsion, and its each material content is as follows:
DHA algae oil 27Kg
Packaging material 27.15Kg
Water 40Kg
Antioxidant 0.05Kg
Stablize thickener 3Kg
Emulsifying agent 0.3g
Adhesive 2.5g
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is slowly added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
In the 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion, the DHA net content is in this DHA emulsion: 108mg/g.
The emulsion Application Example
Embodiment 1
Preparation contains the fruit drink of DHA, and its each material content is as follows:
Fruit juice 86.89Kg
DHA emulsion 1.00Kg
Fatty acid glyceride 0.06Kg
Propylene glycol alginate 0.05Kg
Xylitol 12.00Kg
The step of fruit drink that contains DHA with above-mentioned feedstock production the present invention is as follows:
(1) 1.00kg DHA emulsion is dissolved in the 5kg fruit juice, and adds fatty acid glyceride 0.06kg, propylene glycol alginate 0.05kg, make the solution that contains DHA.
(2) add and remaining 81.89kg fruit juice and 12kg xylitol.
(3) adopt 125 ℃ of high-temperature sterilizations to handle sterilization in 10 seconds.
(4) the above-mentioned fruit drink that contains DHA being carried out homogeneous by high pressure homogenizer under the pressure of 20～30Mpa handles.
(7) packing.
Embodiment 2
Preparation contains the milk beverage of DHA, and its each material content is as follows:
Fresh milk 55 kg
DHA emulsion 1 kg
Fatty acid glyceride 0.06 kg
Propylene glycol alginate 0.05 kg
Xylitol 12 kg
Fruit juice 31.89 kg
The step of milk beverage that contains DHA with above-mentioned feedstock production the present invention is as follows:
(1) fresh milk is carried out standardization, make fat content wherein be not less than 3.0%, protein content is not less than 2.9%.
(2) the DHA emulsion with 1 kg is dissolved in the 5 kg fruit juice, and adds fatty acid glyceride 0.06 kg, propylene glycol alginate 0.05 kg, makes the solution that contains DHA.
(3) milk 55 kg that step (1) handled add solution and the mixing that contains DHA.
(4) add remaining 26.89 kg fruit juice.
(5) adopt 125 ℃ of high-temperature sterilizations to handle sterilization in 10 seconds.
(6) the above-mentioned milk beverage that contains DHA being carried out homogeneous by high pressure homogenizer under the pressure of 20～30 Mpa handles.
(7) packing.
Embodiment 3
Preparation contains the liquid milk of DHA, and its each material content is as follows:
(1) milk 98.6 kg
(2) fatty acid glyceride 0.4 kg
(3) DHA emulsion 1.0 kg
The preparation method of described DHA liquid milk comprises the steps:
(1) raw material is checked and accepted
Milk carries out standardization through coarse filtration, centrifugal clean breast.Be stored in temperature and be the mixing tank about 4 ℃.
(2) batching
The emulsion stabilizer fatty acid glyceride is mixing more than 45 ℃, adds mixing tank.
(3) stirring, mixing, constant volume
Material in the mixing tank was stirred 20 minutes fully mixing, and additional soft water, constant volume.
(4) preheating and homogeneous
Preheating: with the material in the mixing tank 90 ℃ of following preheatings.
Homogeneous: with the material homogeneous in the mixing tank, homogenization pressure: gross pressure is 25Mpa, and first class pressure is 20Mpa, and secondary pressure is 10Mpa.
(5) sterilization
Sterilized 2 seconds down for 142 ℃ in temperature.
(6) cooling
Material after the sterilization is cooled to ℃.Add aseptic jar.
(7) aseptic interpolation
For thermal sensitivity nutrition composition DHA emulsion, select online adding technology (sterilization back adding technology).
(8) sterile filling
Sterile filling obtains described liquid milk to packing.
Embodiment 4
Preparation contains the dried ice cream mix of DHA, and its each material content is as follows:
(1) β-ring is stuck with paste 45 kg
(2) vegetable fat powder 35 kg
(3) whole milk powder 15 kg
(4) PURE WHEY 1.5 kg
(5) DHA emulsion 1.0 kg
(6) flavoring essence 0.5 kg
(7) xanthans 1.0 kg
(8) fatty acid glyceride 0.5 kg
(9) vitamin E 0.5 kg
Above raw material is poured in the container, evenly mix, drying and packaging gets final product then.
When the present invention uses, only need in clean container, add the normal temperature drinking water, while stirring dried ice cream mix is slowly poured into, what will stir then left standstill the ice cream powder slurry 15 minutes at normal temperatures, the ice cream powder slurry is poured into after will leaving standstill then is soft with in the cream machine, and start shooting got final product in 15 minutes.
Embodiment 5
Preparation contains the sour milk of DHA, and its each material content is as follows:
(1) fatty acid glyceride 0.3 kg
(2) white granulated sugar 7.0 kg
(3) inulin 0.1 kg
(4) DHA emulsion 1.0 kg
(5) rare cream 2.0 kg
(6) milk 89.6 kg
0.3 kg fatty acid glyceride is mixed with the white granulated sugar of 1.5 kg, use 30 kg, the dissolving of 70～75 ℃ of milk liquid, and stir 10～20 min, and add 5.5 kg sugar and 0.1 kg inulin, 1 kg DHA and the rare cream of 2 kg again, stir 5～15 min, standby.
Add remaining milk, be cooled to before the sterilization below 10 ℃.
Homogeneous, sterilization: material carries out homogeneous under ℃ condition of 18～20 Mpa/65～70, sterilization under 95 ℃/200～300s condition.
Material is cooled to 42 ℃, is sprinkled into direct putting type powder bacterial classification 250u(streptococcus thermophilus, lactobacillus bulgaricus), mix 10 min.
42 ℃ of condition bottom fermentations, terminal point acidity is controlled at 70
0T.
Turn over cylinder, cooling.After acidity reaches requirement, open frozen water, start agitator 30 s, turn over cylinder to surge tank, temperature is controlled at 18 ℃.
Can, storage.Product can after being cooled to 18 ℃, the finished product after the can place 4 ℃ of refrigerations down immediately in 15 min.
Claims (4)
1. the DHA emulsion is characterized in that: formulated by mass percentage by following raw materials according: DHA algae oil 22～27%; Packaging material 27～32%, water 40～45%, antioxidant 0.02～0.05% is stablized thickener 3.0～5.0%, emulsifying agent 0.1～0.3%, adhesive 2.0～3.0%.
2. DHA emulsion as claimed in claim 1, it is characterized in that: described DHA algae oil by the fragmentation kettle algae of being rich in DHA through the homogeneous broken wall, to carry oil, crude oil refining, emulsifying agent is selected polyglyceryl fatty acid ester or sucrose ester for use, stable thickener is selected carragheen, Arabic gum or xanthans for use, antioxidant is selected TBHQ, ascorbyl palmitate, vitamin E or lecithin for use, adhesive is selected corn syrup or white sugar for use, and packaging material is selected converted starch for use, and water is the solvent that is used to regulate the dense dilution of batching.
3. DHA emulsion as claimed in claim 1 is characterized in that: the production method step is as follows:
The first step, make water: with packaging material, emulsifying agent, stablize thickener, adhesive stirring soluble in water 5 minutes ± 1 minute, import emulsification after the stirring and dissolving and shear 68 ± 5 ℃ of jar heating, emulsification shearing 10～20 minutes makes the complete gelatinization of packaging material;
And, make oil phase: antioxidant is joined in the DHA algae oil, stir;
In second step, batch mixing emulsification: in whipping process oil phase is added aqueous phase, stir, whole process wants constant temperature at 50～60 ℃, emulsification 10 minutes;
The 3rd step, homogeneous: under pressure 20～30MPa condition, homogeneous once, homogeneous is once under 10MPa again;
The 4th step, sterilization: product is carried out pasteurize, ultra high temperature short time sterilization, and add the antistaling agent anti-rot and fresh-keeping method, promptly make the DHA emulsion.
4. the application of DHA emulsion as claimed in claim 1 in preparation DHA beverage, add the DHA emulsion to liquid milk, sour milk, various milk beverage, fruit drink as nutrition fortifier in the ratio of 40～180mg/100g, in auxotype, sport type beverage and the food.
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| CN103416759A (en) * | 2012-05-24 | 2013-12-04 | 内蒙古蒙牛乳业（集团）股份有限公司 | DHA emulsion, preparation method thereof and applications thereof in UHT liquid milk |
| WO2015058703A1 (en) * | 2013-10-25 | 2015-04-30 | Wilmar (Shanghai) Biotechnology Research & Development Center Co., Ltd. | Modified algal oil bodies and methods for stabilizing algal oil bodies and improving the oxidation resistance of the same |
| CN105379843A (en) * | 2015-11-11 | 2016-03-09 | 嘉必优生物技术（武汉）股份有限公司 | Preparation method of milk powder containing multi-unsaturated fatty acid grease |
| EP3001916A1 (en) * | 2014-10-02 | 2016-04-06 | Nikken Kagaku Co., Ltd. | Food or drink comprising an algae extract oil |
| CN110140771A (en) * | 2019-06-13 | 2019-08-20 | 武汉轻工大学 | A kind of peanut yoghourt and preparation method thereof containing DHA |
| CN115697088A (en) * | 2020-05-02 | 2023-02-03 | 鲍斯生命科学Pvt有限公司 | Oil dispersion preparation rich in omega fatty acid |
| CN115918760A (en) * | 2022-12-12 | 2023-04-07 | 江苏亿超健康科技有限公司 | Fishy smell-free soft sweets and preparation method thereof |
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| CN103416759A (en) * | 2012-05-24 | 2013-12-04 | 内蒙古蒙牛乳业（集团）股份有限公司 | DHA emulsion, preparation method thereof and applications thereof in UHT liquid milk |
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| CN110140771A (en) * | 2019-06-13 | 2019-08-20 | 武汉轻工大学 | A kind of peanut yoghourt and preparation method thereof containing DHA |
| CN115697088A (en) * | 2020-05-02 | 2023-02-03 | 鲍斯生命科学Pvt有限公司 | Oil dispersion preparation rich in omega fatty acid |
| CN115918760A (en) * | 2022-12-12 | 2023-04-07 | 江苏亿超健康科技有限公司 | Fishy smell-free soft sweets and preparation method thereof |
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Application publication date: 20110727 |