CN102113985A - Shampoo product and preparation method thereof - Google Patents
Shampoo product and preparation method thereof Download PDFInfo
- Publication number
- CN102113985A CN102113985A CN 201110046165 CN201110046165A CN102113985A CN 102113985 A CN102113985 A CN 102113985A CN 201110046165 CN201110046165 CN 201110046165 CN 201110046165 A CN201110046165 A CN 201110046165A CN 102113985 A CN102113985 A CN 102113985A
- Authority
- CN
- China
- Prior art keywords
- hair
- preparation
- alopecia
- water
- extractum
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 229940095673 shampoo product Drugs 0.000 title abstract 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 27
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000001914 filtration Methods 0.000 claims abstract description 22
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims abstract description 9
- 239000002253 acid Substances 0.000 claims abstract description 9
- 239000000706 filtrate Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 238000005303 weighing Methods 0.000 claims abstract description 7
- 208000001840 Dandruff Diseases 0.000 claims abstract description 5
- 210000004209 hair Anatomy 0.000 claims description 60
- 239000002453 shampoo Substances 0.000 claims description 33
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims description 8
- 239000004141 Sodium laurylsulphate Substances 0.000 claims description 8
- 230000003779 hair growth Effects 0.000 claims description 8
- 235000019333 sodium laurylsulphate Nutrition 0.000 claims description 8
- 239000006071 cream Substances 0.000 claims description 7
- 239000002244 precipitate Substances 0.000 claims description 6
- 230000001737 promoting effect Effects 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 239000006185 dispersion Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 14
- 238000000034 method Methods 0.000 abstract description 4
- XDIAMRVROCPPBK-UHFFFAOYSA-N 2,2-dimethylpropan-1-amine Chemical compound CC(C)(C)CN XDIAMRVROCPPBK-UHFFFAOYSA-N 0.000 abstract 1
- 244000141218 Alpinia officinarum Species 0.000 abstract 1
- 241000233866 Fungi Species 0.000 abstract 1
- 235000003332 Ilex aquifolium Nutrition 0.000 abstract 1
- 235000002296 Ilex sandwicensis Nutrition 0.000 abstract 1
- 235000002294 Ilex volkensiana Nutrition 0.000 abstract 1
- 235000011187 glycerol Nutrition 0.000 abstract 1
- 231100000956 nontoxicity Toxicity 0.000 abstract 1
- 238000001556 precipitation Methods 0.000 abstract 1
- 201000004384 Alopecia Diseases 0.000 description 48
- 231100000360 alopecia Toxicity 0.000 description 48
- 201000010099 disease Diseases 0.000 description 7
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 7
- 208000004631 alopecia areata Diseases 0.000 description 6
- 239000003814 drug Substances 0.000 description 6
- 241001465754 Metazoa Species 0.000 description 5
- 208000003251 Pruritus Diseases 0.000 description 5
- 210000003128 head Anatomy 0.000 description 5
- 230000010354 integration Effects 0.000 description 5
- 238000011161 development Methods 0.000 description 4
- 238000005406 washing Methods 0.000 description 4
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 206010061218 Inflammation Diseases 0.000 description 2
- 239000004677 Nylon Substances 0.000 description 2
- 208000008589 Obesity Diseases 0.000 description 2
- 241000194017 Streptococcus Species 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000002932 luster Substances 0.000 description 2
- 206010025482 malaise Diseases 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 229920001778 nylon Polymers 0.000 description 2
- 235000020824 obesity Nutrition 0.000 description 2
- 230000001575 pathological effect Effects 0.000 description 2
- 230000000704 physical effect Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 210000004761 scalp Anatomy 0.000 description 2
- 210000002374 sebum Anatomy 0.000 description 2
- 230000028327 secretion Effects 0.000 description 2
- 210000003491 skin Anatomy 0.000 description 2
- 206010001766 Alopecia totalis Diseases 0.000 description 1
- 206010001767 Alopecia universalis Diseases 0.000 description 1
- 206010003694 Atrophy Diseases 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000186216 Corynebacterium Species 0.000 description 1
- 206010012504 Dermatophytosis Diseases 0.000 description 1
- 241000588724 Escherichia coli Species 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 206010020772 Hypertension Diseases 0.000 description 1
- 208000002720 Malnutrition Diseases 0.000 description 1
- 241000192041 Micrococcus Species 0.000 description 1
- 241001460074 Microsporum distortum Species 0.000 description 1
- 241000589517 Pseudomonas aeruginosa Species 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
- 201000004239 Secondary hypertension Diseases 0.000 description 1
- 241000191967 Staphylococcus aureus Species 0.000 description 1
- 241000193998 Streptococcus pneumoniae Species 0.000 description 1
- 208000007271 Substance Withdrawal Syndrome Diseases 0.000 description 1
- 208000002474 Tinea Diseases 0.000 description 1
- LEHOTFFKMJEONL-UHFFFAOYSA-N Uric Acid Chemical compound N1C(=O)NC(=O)C2=C1NC(=O)N2 LEHOTFFKMJEONL-UHFFFAOYSA-N 0.000 description 1
- TVWHNULVHGKJHS-UHFFFAOYSA-N Uric acid Natural products N1C(=O)NC(=O)C2NC(=O)NC21 TVWHNULVHGKJHS-UHFFFAOYSA-N 0.000 description 1
- 229930003270 Vitamin B Natural products 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 208000032775 alopecia universalis congenita Diseases 0.000 description 1
- 230000037444 atrophy Effects 0.000 description 1
- 230000003385 bacteriostatic effect Effects 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000001684 chronic effect Effects 0.000 description 1
- 210000000589 cicatrix Anatomy 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 206010012601 diabetes mellitus Diseases 0.000 description 1
- 238000003745 diagnosis Methods 0.000 description 1
- 230000035487 diastolic blood pressure Effects 0.000 description 1
- 235000005911 diet Nutrition 0.000 description 1
- 230000037213 diet Effects 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 206010013023 diphtheria Diseases 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 208000001848 dysentery Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 230000002124 endocrine Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 210000004709 eyebrow Anatomy 0.000 description 1
- 210000000887 face Anatomy 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 210000001061 forehead Anatomy 0.000 description 1
- 230000002068 genetic effect Effects 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000003394 haemopoietic effect Effects 0.000 description 1
- 239000000118 hair dye Substances 0.000 description 1
- 210000003780 hair follicle Anatomy 0.000 description 1
- 239000005556 hormone Substances 0.000 description 1
- 229940088597 hormone Drugs 0.000 description 1
- 230000003752 improving hair Effects 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000010985 leather Substances 0.000 description 1
- 230000001071 malnutrition Effects 0.000 description 1
- 235000000824 malnutrition Nutrition 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 208000015380 nutritional deficiency disease Diseases 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000004321 preservation Methods 0.000 description 1
- 230000001012 protector Effects 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000000452 restraining effect Effects 0.000 description 1
- 230000033764 rhythmic process Effects 0.000 description 1
- 230000001932 seasonal effect Effects 0.000 description 1
- 208000008742 seborrheic dermatitis Diseases 0.000 description 1
- 230000035943 smell Effects 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 210000002784 stomach Anatomy 0.000 description 1
- 229940031000 streptococcus pneumoniae Drugs 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 238000001356 surgical procedure Methods 0.000 description 1
- 208000024891 symptom Diseases 0.000 description 1
- 230000009885 systemic effect Effects 0.000 description 1
- 230000035488 systolic blood pressure Effects 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 238000012549 training Methods 0.000 description 1
- 229930182493 triterpene saponin Natural products 0.000 description 1
- 229940116269 uric acid Drugs 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of a shampoo product, which comprises the following steps: firstly, weighing the following raw materials in parts by weight: 1-8 parts of broadleaf holly leaf and 1-6 parts of lesser galangal rhizome, adding water for decocting for 20 minutes to 50 minutes and then filtering; and then performing alcohol precipitation on filtrate and collecting clear solution which is concentrated to obtain liquid extract with the relative density of 1.15-1.23g/cm-1 at the temperature of 25 DEG C; and secondly, uniformly mixing all the following components: 10%-30% of the liquid extract in the step (1), 0.01-0.05% of potassium hydroxide, 0.01%-0.1% of trimethyl ethylamine acid, 1%-10% of sodium dodecyl sulfate, 0.1%-2% of glycerin and the balance of water, so that the shampoo product is produced. The invention further discloses the shampoo product prepared by the method, which has the purposes of removing dandruff and killing fungi, and further is characterized by being definite and stable in efficacy and good in effects, having no toxicity or side effects, and the like.
Description
Technical field
The present invention relates to bath accessory technical field in the daily product, especially a kind of hair shampoo article, and preparation method thereof.
Background technology
Because the influence of factors such as the quickening of rhythm of life, and living environment at present causes people's alopecia phenomenon comparatively general.Data shows that nearly in the world fifty percent adult man is subjected to the puzzlement of alopecia at present, has four one-tenth in Hong Kong in 25 years old to 54 years old man and faces bareheaded problem.The average attack rate of Chinese city adult male alopecia is about 25%, and with respect to the yellow, white alopecia sickness rate is higher, 25% white man alopecia after 25 years old, to 50 years old alopecia sickness rate up to 50%.According to present scientific research, the reason of alopecia has a lot, the alopecia that the alopecia that the improper alopecia that causes of nervous alopecia, endocrine hormone, body malnutrition and the pathobolism that causes as stress causes and other disease are brought etc.
The reason that produces alopecia also has a lot, as seborrhea, pathologic, chemical, physical property, obesity-related etc., also has factors such as gene genetic and nerve.At different alopecia reasons, the medicine of existing treatment alopecia also has difference, and it is light to be careful in one's diet as seborrheic alopecia, eats irritable food less, eats fruit, green vegetable or vitamin B for oral administration more
6, B
2Deng; The pathologic alopecia then more has a rest, and hair can grow again after physical rehabilitation or the drug withdrawal; Alopecia of chemical origin does not then use the strong hair dye of zest, agent for permanent hair waving and hair shampoo article inferior; The physical property alopecia is not then used and is easily produced electrostatic nylon comb and nylon head brush, wears head protector and hair washing in time at the with serious pollution environment of air-borne dust; The food that the obesity-related alopecia then consumes oil less and is bored with and weighs strengthens physical training.
The ubiquitous problem of the mode of above-mentioned treatment alopecia be weak effect, the course of treatment shortcoming such as length, expense height.
Summary of the invention
The present invention is directed to deficiency, propose a kind of preparation method of hair shampoo article, prepared hair shampoo article has the hair growth promoting effect, and effective, is suitable for the alopecia person of various age brackets.
In order to realize the foregoing invention purpose, the invention provides following technical scheme: a kind of preparation method of hair shampoo article may further comprise the steps:
1., by weight take by weighing raw material: 1～8 part of Folium Ilicis, 1～6 part of Rhizoma Alpiniae Officinarum, add in the entry and decoct, 20min～50min after-filtration, the filtrate precipitate with ethanol is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.15～1.23 extractum;
2., by following each component of weight percentage mixing, promptly obtain hair shampoo article:
Step is extractum 10%～30% 1.
Potassium hydroxide 0.01%～0.05%
Trimethyl ethamine acid 0.01%～0.1%
Sodium lauryl sulphate 1%～10%
Glycerol 0.1%～2%
All the other are water.
Preferably, the component of step in 2. also comprises an amount of essence, the abnormal smells from the patient that adopts conventional essence and conventional amount used thereof to improve hair shampoo article.
Preferably, the weight proportion of each component of step in 2. is:
Step is extractum 20% 1.
Potassium hydroxide 0.02%
Trimethyl ethamine acid 0.01%
Sodium lauryl sulphate 1%
Glycerol 0.5%
All the other are water.
Preferably, the weight portion of 1. middle Folium Ilicis of step and Rhizoma Alpiniae Officinarum is respectively 2 parts and 1 part.
Preferably, step 2. in, earlier with 1. extractum of part aqueous dispersion step, again with all the other component mixings.
Preferably, the filtering residue after the 1. middle filtration of step decocts with water 20min～50min after-filtration; Repeat to decoct and filter 23 merging filtrate.
The present invention also provides the hair shampoo article that is made by above-mentioned preparation method, and this hair shampoo article is used for having one's hair wash in preparation, the application of the compositions of hair growth promoting and the dandruff of dispelling.
Compared with prior art, characteristic part of the present invention is to have adopted effective active composition in Folium Ilicis and the Rhizoma Alpiniae Officinarum as the functional component of hair shampoo article.Because Folium Ilicis has the effect of heat-clearing and toxic substances removing, anti-inflammation and sterilization, the modern pharmacology experimentation shows that also the water extract of Folium Ilicis is for staphylococcus aureus, first streptococcus, streptococcus pneumoniae, second streptococcus, diphtheria corynebacterium, dysentery bacterium, bacillus pyocyaneus, escherichia coli, micrococcus catarrhalis etc. are all had good inhibition effect.The Chemical Constituents shows that Folium Ilicis contains a large amount of triterpene saponin constituents, and these chemical compounds have the effect of surfactant, is natural cleaning agent, emulsifying agent.And Rhizoma Alpiniae Officinarum has the merit that dispersing cold for relieving pain, stomach warming help digestion, and its contained volatile oil has bacteriostatic activity, and the shallow dermatophytosis is had the good restraining effect.In addition, Rhizoma Alpiniae Officinarum also has significantly promotion human body hematopoietic function, thereby the function of hair growth promoting is arranged.Two medicine compatibilities share, and have effects such as hair washing, hair growth promoting and dandruff dispelling.
When using hair cream of the present invention, shampoo, do not mix use with other products.Adopt conventional hair washing method can use hair shampoo article of the present invention, suggestion hair washing method commonly used is: hair is soaked, and it is soft at head to get an amount of hair cream, and water is rinsed well, gets in right amount again and gently rubs at the root of hair place, keeps minutes 10～40 minutes, rinses well to get final product.
Points for attention:
Be not splashed in the eyes when 1, using,, use a large amount of flushing with clean water as early as possible if be splashed into.
2, this product is positioned over shady and cool dry place preservation.
3, can not have hair dyed, perm during the treatment.
The specific embodiment
Describe the present invention below in conjunction with specific embodiment, the description of this part only is exemplary and explanatory, should any restriction not arranged to protection scope of the present invention.
Embodiment 1
A kind of preparation method of hair cream may further comprise the steps:
1., by weight take by weighing raw material: 2 parts of Folium Ilicis, 1 part of Rhizoma Alpiniae Officinarum, decoct with water, the 50min after-filtration, filtrate 50% ethanol precipitate with ethanol is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.15 extractum;
2., by following each component of weight percentage mixing, stir into even paste and promptly get hair cream:
Step is extractum 30% 1.
Potassium hydroxide 0.01%
Trimethyl ethamine acid 0.1%
Sodium lauryl sulphate 1%
Glycerol 2%
All the other are water.
Embodiment 2
A kind of preparation method of shampoo may further comprise the steps:
1., by weight take by weighing raw material: 1 part of Folium Ilicis, 6 parts of Rhizoma Alpiniae Officinarums, decoct with water, 20min after-filtration, filtering residue add water and decoct the 30min after-filtration again, and filtering residue adds water and carries out decoction 40min the 3rd time, filters; Merging filtrate with 65% ethanol precipitate with ethanol, is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.23 extractum;
2., by following each component of weight percentage mixing, promptly get shampoo:
Step is extractum 10% 1.
Potassium hydroxide 0.05%
Trimethyl ethamine acid 0.01%
Sodium lauryl sulphate 10%
Glycerol 0.1%
Essence 0.1%
All the other are water.
Embodiment 3
A kind of preparation method of shampoo may further comprise the steps:
1., by weight take by weighing raw material: 8 parts of Folium Ilicis, 1 part of Rhizoma Alpiniae Officinarum, decoct with water, 30min after-filtration, filtering residue add water and decoct the 20min after-filtration again, and filtering residue adds water and carries out decoction 50min the 3rd time, filters; Merging filtrate with 60% ethanol precipitate with ethanol, is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.18 extractum;
2., by following each component of weight percentage mixing, promptly get shampoo:
Step is extractum 20% 1.
Potassium hydroxide 0.02%
Trimethyl ethamine acid 0.01%
Sodium lauryl sulphate 1%
Glycerol 0.5%
All the other are water.
Embodiment 4
A kind of preparation method of hair cream may further comprise the steps:
1., by weight take by weighing raw material: 2 parts of Folium Ilicis, 1 part of Rhizoma Alpiniae Officinarum, decoct with water, 20min after-filtration, filtering residue add water and decoct the 40min after-filtration again, and filtering residue adds water and carries out decoction 20min the 3rd time, filters; Merging filtrate with 55% ethanol precipitate with ethanol, is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.21 extractum;
2., by following each component of weight percentage mixing, promptly get hair cream:
Step is extractum 20% 1.
Potassium hydroxide 0.02%
Trimethyl ethamine acid 0.01%
Sodium lauryl sulphate 1%
Glycerol 0.5%
All the other are water.
Clinical data
1, physical data
The object of observation is selected from January, 2009～2009 year 10 moon gates example of diagnosing a disease:
30～70 years old seborrheic alopecia patient totally 560 people wherein, wherein male 362 examples, the age was at 30～68 years old; Woman's 198 examples, the age was at 30～62 years old; The course of disease 3 years～10 years.
30～70 years old alopecia areata alopecia patient totally 260 people wherein, wherein male 192 examples, the age was at 30～60 years old; Woman's 68 examples, the age was at 30～55 years old; The course of disease 1 year～3 years.
(1) diagnostic criteria
A, seborrheic alopecia diagnostic criteria are with reference to the diagnostic criteria of the high medical president's state-compiled textbook in People's Health Publisher " Surgery of Chinese Medicine " seborrheic alopecia.Clinical symptoms: earlier from the temples of forehead, through low, hair is soft, sparse gradually, come off, alopecia.Behind the many decades, hair is gone up on the volume and top can take off light fully.Skin smooth, shrinking pore or left over a small amount of fine hair on birds or animals hair, two occipitalias and both sides temples still keep normally.
The diagnostic criteria of b, alopecia areata is compiled " the 3rd volume of new Chinese medicine clinical research guideline " it " clinical research guideline of new Chinese medicine treatment alopecia " according to Ministry of Health of the People's Republic of China and is formulated diagnostic criteria: suddenly or hair flaking in a short time, single-shot or pilosity, even hair all comes off (alopecia totalis), eyebrow, armpit hair, pubes, beard and fine hair on birds or animals hair come off (alopecia universalis).Alopecia district color of the leather is normal, does not have obvious inflammatory reaction.Alopecia district skin is not seen atrophy and cicatrix.
(2) include standard in
1. meet seborrheic alopecia or alopecia areata diagnostic criteria; 2. the age was 30～70 years old outpatient.
(3) exclusion standard
A, the course of disease surpass 5 years, the atrophied patients with terminal of hair follicle;
B, serious systemic disease, Chronic consumptions person are arranged;
C, prescription on individual diagnosis the last fortnight were taken relevant medicine person.
Seasonal alopecia, alopecia medicamentosa, the relevant alopecia of disease.Get rid of secondary hypertension, diabetes.
2, observation caliber
(1) general inspection inquiry medical history and individual ordinary circumstance are measured blood pressure, heart rate, picture of the tongue, pulse condition.
(2) observation item hypertension: systolic pressure 〉=140mmHg, diastolic pressure 〉=90mmHg, blood fat, blood glucose, all normal values that surpasses of blood uric acid are all calculated unusually.
2.3 alopecia is divided into youth, middle age, old three groups from the age.
1. young male group: 25～40 years old (using embodiment 1 hair shampoo article); Middle age group: 41～50 years old (using embodiment 2 hair shampoo articles); Old group 51～68 years old (using embodiment 3 hair shampoo articles).
2. the women is young organizes: 30～40 years old (using embodiment 4 hair shampoo articles); Middle age group: 41～50 years old (using embodiment 3 hair shampoo articles); Old group 51～62 years old (using embodiment 2 hair shampoo articles).
What matched group adopted is conventional hair shampoo article.
(3) observed content and method
A, alopecia do not have alopecia and are designated as 0 fen; A small amount of alopecia (being less than 50 pieces/day) is designated as 2 fens; Moderate alopecia (50～100 pieces/day) is designated as 4 fens; A large amount of alopecias (greater than 100 pieces/day) are designated as 6 fens.
B, pruritus do not have pruritus and are designated as 0 fen; Slightly be designated as 2 fens; Moderate is designated as 4 fens; Severe is designated as 6 fens.
C, greasy scales is moderate is designated as 0 fen; Be designated as 2 fens on a small quantity; Moderate is designated as 4 fens; Obviously be designated as 6 fens.
D, alopecia place of New Development growing state all grow hair, and color and luster and thickness are with normally being designated as 0 fen; The alopecia director goes out 2/3 above New Development, and hair black and white thickness inequality is designated as 2 fens; Grow 1/3 above New Development, hair jewelry, expensive clothing and other valuables, color are white, are designated as 4 fens; No New Development grows or only has a little fine hair on birds or animals staple length to go out to be designated as 6 fens.The per 2 week records of above content once, and adopt scoring with integration what as the index of measurement curative effect.
(4) criterion of therapeutical effect
A, recovery from illness: scalp itch disappears, no dandruff and alopecia, and hair thickness color and luster is normal, and the head sebum secretion is moderate, and integration is zero;
B, produce effects: hair growth is more, and is chequered with black and white, plucked, and scalp itch and greasy scales obviously reduce, and integration descends more than 70%;
C, effective: more fine hair on birds or animals hair growth is arranged, and pruritus and head sebum secretion reduce to some extent, and integration descends 30～70%;
D, invalid: absent hair growth or a little fine hair on birds or animals staple length is arranged after come off again, integration descends less than 30%.
(5) result of the test sees the following form 1 and table 2:
The clinical curative effect relatively (%) of respectively organizing of table 1 seborrheic alopecia
As can be seen from Table 1, the treatment group of each embodiment is being treated seborrheic alopecia apparently higher than matched group, effective percentage (recovery from illness, produce effects and effective shared ratio of three's sum) average out to 81%.Illustrate that hair shampoo article of the present invention has the obvious treatment effect for seborrheic alopecia.
The clinical curative effect relatively (%) of respectively organizing of table 2 alopecia areata alopecia
As can be seen from Table 1, the treatment group of each embodiment at alopecia areata alopecia apparently higher than matched group, effective percentage average out to 78%.Illustrate that hair shampoo article of the present invention has the obvious treatment effect for alopecia areata alopecia.
It below only is preferred implementation of the present invention; should be pointed out that for those skilled in the art, under the prerequisite that does not break away from the principle of the invention; can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (9)
1. the preparation method of a hair shampoo article may further comprise the steps:
1., by weight take by weighing raw material: 1～8 part of Folium Ilicis, 1～6 part of Rhizoma Alpiniae Officinarum, decoct with water, 20min～50min after-filtration, the filtrate precipitate with ethanol is collected clear liquid and is concentrated to such an extent that 25 ℃ of following relative densities are 1.15～1.23g/cm
-1Extractum;
2., by following each component of weight percentage mixing, promptly obtain hair shampoo article:
Step is extractum 10%～30% 1.
Potassium hydroxide 0.01%～0.05%
Trimethyl ethamine acid 0.01%～0.1%
Sodium lauryl sulphate 1%～10%
Glycerol 0.1%～2%
All the other are water.
2. preparation method as claimed in claim 1 is characterized in that: the component of step in 2. also comprises an amount of essence.
3. preparation method as claimed in claim 1 is characterized in that: the weight proportion of each component of step in 2. is:
Step is extractum 20% 1.
Potassium hydroxide 0.02%
Trimethyl ethamine acid 0.01%
Sodium lauryl sulphate 1%
Glycerol 0.5%
All the other are water.
4. preparation method as claimed in claim 1 is characterized in that: the weight portion of 1. middle Folium Ilicis of step and Rhizoma Alpiniae Officinarum is respectively 2 parts and 1 part.
5. preparation method as claimed in claim 1 is characterized in that: step 2. in, earlier with 1. extractum of part aqueous dispersion step, again with all the other component mixings.
6. preparation method as claimed in claim 1 is characterized in that: the filtering residue after the 1. middle filtration of step decocts with water 20min～50min after-filtration; Repeat to decoct and filter 23 merging filtrate.
7. hair shampoo article of making of preparation method according to claim 1.
8. hair shampoo article as claimed in claim 7 is characterized in that: this hair shampoo article is hair cream or shampoo.
A hair shampoo article as claimed in claim 7 be used for having one's hair wash in preparation, the application of the compositions of hair growth promoting and the dandruff of dispelling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110046165 CN102113985B (en) | 2011-02-25 | 2011-02-25 | Shampoo product and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110046165 CN102113985B (en) | 2011-02-25 | 2011-02-25 | Shampoo product and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN102113985A true CN102113985A (en) | 2011-07-06 |
| CN102113985B CN102113985B (en) | 2012-10-31 |
Family
ID=44212986
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201110046165 Expired - Fee Related CN102113985B (en) | 2011-02-25 | 2011-02-25 | Shampoo product and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN102113985B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103933446A (en) * | 2013-01-23 | 2014-07-23 | 中国热带农业科学院热带生物技术研究所 | Application of alpinia officinarum extraction product to treating tinea pedis and tinea manuum and preparation method of alpinia officinarum extract product |
| CN104127327A (en) * | 2014-06-25 | 2014-11-05 | 佛山市安安美容保健品有限公司 | Hair-caring product containing marine biological protein peptide |
| CN106667873A (en) * | 2017-03-22 | 2017-05-17 | 何俊飞 | Plant additive for hair washing and caring shampoo |
| CN114306527A (en) * | 2021-12-31 | 2022-04-12 | 广西养利农业投资开发有限公司 | Compound broadleaf holly leaf traditional Chinese medicine composition and application thereof in preparing shampoo |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3900977B2 (en) * | 2002-03-08 | 2007-04-04 | 丸善製薬株式会社 | Skin cosmetics and beauty food and drink |
| KR20070083337A (en) * | 2006-02-21 | 2007-08-24 | 주식회사 엘지생활건강 | Anti-dandruff hair care cosmetic composition |
| CN101115493A (en) * | 2005-08-12 | 2008-01-30 | 河乃建仁 | Agent for hair growth |
| CN101332165A (en) * | 2007-06-25 | 2008-12-31 | 陈丽妹 | Shampoo |
-
2011
- 2011-02-25 CN CN 201110046165 patent/CN102113985B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3900977B2 (en) * | 2002-03-08 | 2007-04-04 | 丸善製薬株式会社 | Skin cosmetics and beauty food and drink |
| CN101115493A (en) * | 2005-08-12 | 2008-01-30 | 河乃建仁 | Agent for hair growth |
| KR20070083337A (en) * | 2006-02-21 | 2007-08-24 | 주식회사 엘지생활건강 | Anti-dandruff hair care cosmetic composition |
| CN101332165A (en) * | 2007-06-25 | 2008-12-31 | 陈丽妹 | Shampoo |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103933446A (en) * | 2013-01-23 | 2014-07-23 | 中国热带农业科学院热带生物技术研究所 | Application of alpinia officinarum extraction product to treating tinea pedis and tinea manuum and preparation method of alpinia officinarum extract product |
| CN104127327A (en) * | 2014-06-25 | 2014-11-05 | 佛山市安安美容保健品有限公司 | Hair-caring product containing marine biological protein peptide |
| CN106667873A (en) * | 2017-03-22 | 2017-05-17 | 何俊飞 | Plant additive for hair washing and caring shampoo |
| CN114306527A (en) * | 2021-12-31 | 2022-04-12 | 广西养利农业投资开发有限公司 | Compound broadleaf holly leaf traditional Chinese medicine composition and application thereof in preparing shampoo |
Also Published As
| Publication number | Publication date |
|---|---|
| CN102113985B (en) | 2012-10-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102614102B (en) | Dandruff-removing medicinal composition and preparation method thereof | |
| CN106333885A (en) | Plant extract and eye essence liquid | |
| KR102251288B1 (en) | Cosmetic composition for improving blood circulation, including cissus and spring onion fermented extract | |
| CN107468563A (en) | A kind of anti-dandruff silk quality lubrication is without silicone oil shampoo | |
| CN109010236A (en) | A kind of infant's shampoo used also as bath lotion and preparation method thereof | |
| JP4495406B2 (en) | Sendangusa plant extract-containing composition | |
| CN102113985B (en) | Shampoo product and preparation method thereof | |
| CN107913227A (en) | Containing small yellow ginger without silicone oil hair conditioner and its preparation process | |
| CN114053169A (en) | Beauty treatment use of blue algae polysaccharide in water temple | |
| KR102016164B1 (en) | Whitening emulsion cosmetic composition containing a vitamin tree fruit extract and method for manufacturing the same | |
| KR102429343B1 (en) | A cosmetic composition for scalp and hair improvement comprising multiple extract of combined medicinal herbs | |
| JP4615796B2 (en) | Irritation mitigation composition | |
| KR101977456B1 (en) | A cosmetic composition for promoting hair growth and preventing hair loss | |
| CN113398237A (en) | Traditional Chinese medicine composition with antibacterial, itching relieving and dandruff stopping functions and preparation method thereof | |
| Gholve et al. | Formulation and evaluation of polyherbal antidandruff powder shampoo | |
| CN105816718A (en) | External traditional Chinese medicine composition with hair care and hair blackening effects | |
| CN105534815A (en) | Skin-care composition containing lotus active ingredients and preparation method of skin-care composition | |
| JPS63145216A (en) | Hair dressing agent for hair growing, hair nourishing or the like | |
| CN108113953A (en) | A kind of dendrobium candidum honey composite extract with moisture-keeping efficacy and preparation method thereof and the application in skin care item | |
| CN103740511A (en) | Hairy euphorbia medicated soap | |
| KR102071600B1 (en) | Cream composition manufacturing method for preventing of sensitive-skin and skin-trouble | |
| CN106726961A (en) | A kind of cleaning agent for mouth cavity and preparation method thereof | |
| CN106473940A (en) | A kind of multiple-effect bath gel and preparation method thereof | |
| CN106390061A (en) | Hair follicle stem cell awakening factor composition for external use, hair loss prevention, and hair regeneration, and preparation method thereof | |
| CN105997645A (en) | Multi-moisturizing makeup removing lotion and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Effective date: 20110830 Free format text: FORMER OWNER: HAINAN YEXIAN BIO-SCIENCE CO., LTD. |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| C53 | Correction of patent for invention or patent application | ||
| CB03 | Change of inventor or designer information |
Inventor after: Dai Haofu Inventor after: Zuo Wenjian Inventor after: Mei Wenli Inventor after: Wang Hui Inventor before: Dai Haofu Inventor before: Zuo Wenjian Inventor before: Mei Wenli Inventor before: Xiao Yufang Inventor before: Zheng Guozhong |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: DAI HAOFU ZUO WENJIAN MEI WENLI XIAO YUFANG ZHENG GUOZHONG TO: DAI HAOFU ZUO WENJIAN MEI WENLI WANG HUI |
|
| TA01 | Transfer of patent application right |
Effective date of registration: 20110830 Address after: 571101 Xueyuan Road Institute of Tropical Biotechnology, Longhua, Hainan, China,, 4, A502 Applicant after: Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agricultural Sciences Address before: 571101 Xueyuan Road Institute of Tropical Biotechnology, Longhua, Hainan, China,, 4, A502 Applicant before: Institute of Tropical Bioscience and Biotechnology, Chinese Academy of Tropical Agricultural Sciences Co-applicant before: Hainan Yexian Bio-Science Co.,Ltd. |
|
| C53 | Correction of patent for invention or patent application | ||
| CB03 | Change of inventor or designer information |
Inventor after: Zuo Wenjian Inventor after: Dai Haofu Inventor after: Mei Wenli Inventor after: Wang Hui Inventor before: Dai Haofu Inventor before: Zuo Wenjian Inventor before: Mei Wenli Inventor before: Wang Hui |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: DAI HAOFU ZUO WENJIAN MEI WENLI WANG HUI TO: ZUO WENJIAN DAI HAOFU MEI WENLI WANG HUI |
|
| C53 | Correction of patent for invention or patent application | ||
| CB03 | Change of inventor or designer information |
Inventor after: Mei Wenli Inventor after: Dai Haofu Inventor after: Zuo Wenjian Inventor after: Wang Hui Inventor before: Zuo Wenjian Inventor before: Dai Haofu Inventor before: Mei Wenli Inventor before: Wang Hui |
|
| COR | Change of bibliographic data |
Free format text: CORRECT: INVENTOR; FROM: ZUO WENJIAN DAI HAOFU MEI WENLI WANG HUI TO: MEI WENLI DAI HAOFU ZUO WENJIAN WANG HUI |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20121031 Termination date: 20180225 |