CN102113059A - 用于生产不加载体的99Mo 的方法 - Google Patents
用于生产不加载体的99Mo 的方法 Download PDFInfo
- Publication number
- CN102113059A CN102113059A CN2009801303865A CN200980130386A CN102113059A CN 102113059 A CN102113059 A CN 102113059A CN 2009801303865 A CN2009801303865 A CN 2009801303865A CN 200980130386 A CN200980130386 A CN 200980130386A CN 102113059 A CN102113059 A CN 102113059A
- Authority
- CN
- China
- Prior art keywords
- liquid
- compound
- molybdenum
- transferred
- neutron
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 25
- 150000001875 compounds Chemical class 0.000 claims abstract description 34
- 238000000034 method Methods 0.000 claims abstract description 22
- 230000000694 effects Effects 0.000 claims abstract description 16
- 238000000926 separation method Methods 0.000 claims abstract description 5
- MCJGNVYPOGVAJF-UHFFFAOYSA-N quinolin-8-ol Chemical compound C1=CN=C2C(O)=CC=CC2=C1 MCJGNVYPOGVAJF-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims description 29
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 21
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims description 20
- 229910052750 molybdenum Inorganic materials 0.000 claims description 13
- 239000007791 liquid phase Substances 0.000 claims description 6
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 claims description 5
- 239000005695 Ammonium acetate Substances 0.000 claims description 5
- 229940043376 ammonium acetate Drugs 0.000 claims description 5
- 235000019257 ammonium acetate Nutrition 0.000 claims description 5
- 239000000872 buffer Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000012546 transfer Methods 0.000 claims description 2
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 claims 1
- 230000004992 fission Effects 0.000 abstract description 14
- 239000005725 8-Hydroxyquinoline Substances 0.000 abstract description 3
- QXYJCZRRLLQGCR-UHFFFAOYSA-N dioxomolybdenum Chemical compound O=[Mo]=O QXYJCZRRLLQGCR-UHFFFAOYSA-N 0.000 abstract description 3
- 229960003540 oxyquinoline Drugs 0.000 abstract description 3
- 230000004913 activation Effects 0.000 abstract description 2
- 239000011733 molybdenum Substances 0.000 description 12
- 239000000843 powder Substances 0.000 description 12
- 239000000243 solution Substances 0.000 description 12
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
- 239000008346 aqueous phase Substances 0.000 description 7
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 6
- 238000000605 extraction Methods 0.000 description 5
- 238000000638 solvent extraction Methods 0.000 description 5
- 239000011550 stock solution Substances 0.000 description 5
- 239000007853 buffer solution Substances 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000003758 nuclear fuel Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000622 liquid--liquid extraction Methods 0.000 description 3
- XJCQKXPYXRYZQM-UHFFFAOYSA-N [Mo+] Chemical class [Mo+] XJCQKXPYXRYZQM-UHFFFAOYSA-N 0.000 description 2
- 239000003929 acidic solution Substances 0.000 description 2
- QZPSXPBJTPJTSZ-UHFFFAOYSA-N aqua regia Chemical compound Cl.O[N+]([O-])=O QZPSXPBJTPJTSZ-UHFFFAOYSA-N 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000003637 basic solution Substances 0.000 description 2
- 230000005251 gamma ray Effects 0.000 description 2
- 238000002354 inductively-coupled plasma atomic emission spectroscopy Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000005078 molybdenum compound Substances 0.000 description 2
- 150000002752 molybdenum compounds Chemical class 0.000 description 2
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 description 2
- -1 molybdenum(VI) bis(8-hydroxyquinoline) Chemical compound 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 239000012074 organic phase Substances 0.000 description 2
- 230000001590 oxidative effect Effects 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 239000001509 sodium citrate Substances 0.000 description 2
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 description 2
- 239000012086 standard solution Substances 0.000 description 2
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- CSKSYFFRZCALAP-UHFFFAOYSA-N C1(C=CC=C1)[Mo+] Chemical class C1(C=CC=C1)[Mo+] CSKSYFFRZCALAP-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 1
- 229910016006 MoSi Inorganic materials 0.000 description 1
- UIMTYIBFGGHZEP-UHFFFAOYSA-H O=C1OC(C(OC1)C(=O)[O-])=O.[Mo+6].O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O Chemical compound O=C1OC(C(OC1)C(=O)[O-])=O.[Mo+6].O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O.O=C1OC(C(OC1)C(=O)[O-])=O UIMTYIBFGGHZEP-UHFFFAOYSA-H 0.000 description 1
- 240000007817 Olea europaea Species 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 241000339782 Tomares Species 0.000 description 1
- VWVZEGJTBQPYID-UHFFFAOYSA-N [K+].[Mo+6] Chemical compound [K+].[Mo+6] VWVZEGJTBQPYID-UHFFFAOYSA-N 0.000 description 1
- 229910052768 actinide Inorganic materials 0.000 description 1
- 150000001255 actinides Chemical class 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- YXTPWUNVHCYOSP-UHFFFAOYSA-N bis($l^{2}-silanylidene)molybdenum Chemical compound [Si]=[Mo]=[Si] YXTPWUNVHCYOSP-UHFFFAOYSA-N 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000011067 equilibration Methods 0.000 description 1
- 231100001261 hazardous Toxicity 0.000 description 1
- 238000009616 inductively coupled plasma Methods 0.000 description 1
- UETZVSHORCDDTH-UHFFFAOYSA-N iron(2+);hexacyanide Chemical compound [Fe+2].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] UETZVSHORCDDTH-UHFFFAOYSA-N 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052961 molybdenite Inorganic materials 0.000 description 1
- 229910021343 molybdenum disilicide Inorganic materials 0.000 description 1
- 229910052982 molybdenum disulfide Inorganic materials 0.000 description 1
- UMOJXGMTIHBUTN-UHFFFAOYSA-N molybdenum(5+) Chemical class [Mo+5] UMOJXGMTIHBUTN-UHFFFAOYSA-N 0.000 description 1
- 239000002105 nanoparticle Substances 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000002285 radioactive effect Effects 0.000 description 1
- 238000002601 radiography Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21G—CONVERSION OF CHEMICAL ELEMENTS; RADIOACTIVE SOURCES
- G21G1/00—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes
- G21G1/04—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes outside nuclear reactors or particle accelerators
- G21G1/06—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes outside nuclear reactors or particle accelerators by neutron irradiation
-
- G—PHYSICS
- G21—NUCLEAR PHYSICS; NUCLEAR ENGINEERING
- G21G—CONVERSION OF CHEMICAL ELEMENTS; RADIOACTIVE SOURCES
- G21G1/00—Arrangements for converting chemical elements by electromagnetic radiation, corpuscular radiation or particle bombardment, e.g. producing radioactive isotopes
- G21G1/001—Recovery of specific isotopes from irradiated targets
- G21G2001/0036—Molybdenum
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- High Energy & Nuclear Physics (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP08157758A EP2131369A1 (en) | 2008-06-06 | 2008-06-06 | A process for the production of no-carrier added 99Mo |
| EP08157758.7 | 2008-06-06 | ||
| PCT/NL2009/050301 WO2009148306A1 (en) | 2008-06-06 | 2009-06-02 | A process for the production of no-carrier added 99mo |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN102113059A true CN102113059A (zh) | 2011-06-29 |
Family
ID=39870009
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2009801303865A Pending CN102113059A (zh) | 2008-06-06 | 2009-06-02 | 用于生产不加载体的99Mo 的方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US20110118491A1 (https=) |
| EP (2) | EP2131369A1 (https=) |
| JP (1) | JP2011522276A (https=) |
| CN (1) | CN102113059A (https=) |
| AU (1) | AU2009255830A1 (https=) |
| BR (1) | BRPI0914861A2 (https=) |
| CA (1) | CA2727156A1 (https=) |
| RU (1) | RU2010154094A (https=) |
| WO (1) | WO2009148306A1 (https=) |
| ZA (1) | ZA201009139B (https=) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104321827A (zh) * | 2011-12-05 | 2015-01-28 | 威斯康星校友研究基金会 | 用于产生医用同位素的设备和方法 |
| CN106662540A (zh) * | 2014-08-06 | 2017-05-10 | 研究三角协会 | 高效中子俘获产物产生 |
| CN111785407A (zh) * | 2020-07-13 | 2020-10-16 | 中国科学院上海应用物理研究所 | 一种含钼的物质的处理方法 |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9177679B2 (en) * | 2010-02-11 | 2015-11-03 | Uchicago Argonne, Llc | Accelerator-based method of producing isotopes |
| US10930407B2 (en) * | 2014-11-21 | 2021-02-23 | Gary M. Sandquist | Productions of radioisotopes |
| NL2013872B1 (en) * | 2014-11-25 | 2016-10-11 | Univ Delft Tech | Flexible Irradiation Facility. |
| US10804000B2 (en) | 2016-05-18 | 2020-10-13 | The Regents Of The University Of California | High efficiency continuous-flow production of radioisotopes |
| CN106297910B (zh) * | 2016-09-14 | 2018-01-30 | 厦门大学 | 一种核反应堆灰控制棒用钼基氧化铽材料及其应用 |
| JP6712002B1 (ja) * | 2019-11-01 | 2020-06-17 | 株式会社タカハシＲｉラボ | テクネチウム９９ｍ製造システム及びテクネチウム９９ｍ製造方法 |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85109328A (zh) * | 1985-12-26 | 1986-11-05 | 中国原子能科学研究院 | 从铀-235及其裂变产物中分离医用钼-99的方法 |
| WO1998059347A1 (en) * | 1997-06-19 | 1998-12-30 | European Organization For Nuclear Research | Neutron-driven element transmuter |
| CN1234290A (zh) * | 1999-05-25 | 1999-11-10 | 中国核动力研究设计院 | 用医用同位素生产堆生产钼－99的提取与纯化工艺 |
| CN1522448A (zh) * | 2001-06-05 | 2004-08-18 | 医事物理公司 | 靶方法 |
| CN1658938A (zh) * | 2002-04-12 | 2005-08-24 | Pg研究基金会公司 | 制备超纯放射性核素的多柱式反向选择性发生器 |
| US20060023829A1 (en) * | 2004-08-02 | 2006-02-02 | Battelle Memorial Institute | Medical radioisotopes and methods for producing the same |
| WO2006039787A1 (en) * | 2004-10-12 | 2006-04-20 | Mcmaster University | GENERATOR AND METHOD FOR PRODUCTION OF TECHNETIUM-99m |
| WO2008047946A1 (en) * | 2006-10-20 | 2008-04-24 | Japan Atomic Energy Agency | Process for producing radioactive molybdenum, apparatus therefor and radioactive molybdenum produced by the process |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6998052B2 (en) * | 2002-04-12 | 2006-02-14 | Pg Research Foundation | Multicolumn selectivity inversion generator for production of ultrapure radionuclides |
-
2008
- 2008-06-06 EP EP08157758A patent/EP2131369A1/en not_active Withdrawn
-
2009
- 2009-06-02 CN CN2009801303865A patent/CN102113059A/zh active Pending
- 2009-06-02 EP EP09758553A patent/EP2301041A1/en not_active Withdrawn
- 2009-06-02 JP JP2011512400A patent/JP2011522276A/ja active Pending
- 2009-06-02 AU AU2009255830A patent/AU2009255830A1/en not_active Abandoned
- 2009-06-02 BR BRPI0914861A patent/BRPI0914861A2/pt not_active IP Right Cessation
- 2009-06-02 CA CA2727156A patent/CA2727156A1/en not_active Abandoned
- 2009-06-02 WO PCT/NL2009/050301 patent/WO2009148306A1/en not_active Ceased
- 2009-06-02 US US12/996,209 patent/US20110118491A1/en not_active Abandoned
- 2009-06-02 RU RU2010154094/07A patent/RU2010154094A/ru not_active Application Discontinuation
-
2010
- 2010-12-20 ZA ZA2010/09139A patent/ZA201009139B/en unknown
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN85109328A (zh) * | 1985-12-26 | 1986-11-05 | 中国原子能科学研究院 | 从铀-235及其裂变产物中分离医用钼-99的方法 |
| WO1998059347A1 (en) * | 1997-06-19 | 1998-12-30 | European Organization For Nuclear Research | Neutron-driven element transmuter |
| CN1234290A (zh) * | 1999-05-25 | 1999-11-10 | 中国核动力研究设计院 | 用医用同位素生产堆生产钼－99的提取与纯化工艺 |
| CN1522448A (zh) * | 2001-06-05 | 2004-08-18 | 医事物理公司 | 靶方法 |
| CN1658938A (zh) * | 2002-04-12 | 2005-08-24 | Pg研究基金会公司 | 制备超纯放射性核素的多柱式反向选择性发生器 |
| US20060023829A1 (en) * | 2004-08-02 | 2006-02-02 | Battelle Memorial Institute | Medical radioisotopes and methods for producing the same |
| WO2006039787A1 (en) * | 2004-10-12 | 2006-04-20 | Mcmaster University | GENERATOR AND METHOD FOR PRODUCTION OF TECHNETIUM-99m |
| WO2008047946A1 (en) * | 2006-10-20 | 2008-04-24 | Japan Atomic Energy Agency | Process for producing radioactive molybdenum, apparatus therefor and radioactive molybdenum produced by the process |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104321827A (zh) * | 2011-12-05 | 2015-01-28 | 威斯康星校友研究基金会 | 用于产生医用同位素的设备和方法 |
| CN104321827B (zh) * | 2011-12-05 | 2017-02-22 | 威斯康星校友研究基金会 | 用于产生医用同位素的设备和方法 |
| US10332646B2 (en) | 2011-12-05 | 2019-06-25 | Wisconsin Alumni Research Foundation | Apparatus and method for generating medical isotopes |
| CN106662540A (zh) * | 2014-08-06 | 2017-05-10 | 研究三角协会 | 高效中子俘获产物产生 |
| CN111785407A (zh) * | 2020-07-13 | 2020-10-16 | 中国科学院上海应用物理研究所 | 一种含钼的物质的处理方法 |
| CN111785407B (zh) * | 2020-07-13 | 2022-08-16 | 中国科学院上海应用物理研究所 | 一种含钼的物质的处理方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2301041A1 (en) | 2011-03-30 |
| BRPI0914861A2 (pt) | 2015-11-03 |
| RU2010154094A (ru) | 2012-07-20 |
| ZA201009139B (en) | 2012-07-25 |
| US20110118491A1 (en) | 2011-05-19 |
| AU2009255830A1 (en) | 2009-12-10 |
| EP2131369A1 (en) | 2009-12-09 |
| WO2009148306A1 (en) | 2009-12-10 |
| CA2727156A1 (en) | 2009-12-10 |
| JP2011522276A (ja) | 2011-07-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| ASS | Succession or assignment of patent right |
Owner name: MO989 HOLDING B.V. Free format text: FORMER OWNER: TECHNISCHE UNIVERSITEIT DELFT Effective date: 20120309 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20120309 Address after: Delft, Netherlands Applicant after: MO989 Holdings Ltd Address before: Delft Applicant before: Technische Universiteit Delft |
|
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20110629 |