CN102108641A - Digital printing active dye jet ink - Google Patents
Digital printing active dye jet ink Download PDFInfo
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- CN102108641A CN102108641A CN2011100060210A CN201110006021A CN102108641A CN 102108641 A CN102108641 A CN 102108641A CN 2011100060210 A CN2011100060210 A CN 2011100060210A CN 201110006021 A CN201110006021 A CN 201110006021A CN 102108641 A CN102108641 A CN 102108641A
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Abstract
The invention discloses digital printing active dye jet ink, comprising the following ingredients in percentage by weight: 1.0-20% of active dye, 10-40% of viscosity regulator, 0.2-2% of surface tension regulator, 0.1-3.0% of pH value control agent, 0.3-1.5% of sterilizer and the balance of de-ionized water. The digital printing active dye jet ink provided by the invention is suitable for printing and dyeing textiles, such as real silk, pure cotton, numb, viscose and mixed fiber thereof, and especially has the advantages of better chromaticity, color fastness and color repeatability on wool textiles.
Description
Technical field
The present invention relates to a kind of digit printing REACTIVE DYES ink-jet ink.
Background technology
In recent years, the digital printing of textiles technology need not plate-making because production procedure is short, and is novel convenient, to the dye utilization rate height, do not have waste material to produce, and becomes a kind of high-quality, low cost, eco-friendly printing in textiles production method.The field of digital inking printing is constantly expanded, and industrialized scale constantly enlarges, and demonstrates good industrial prospect.
REACTIVE DYES belongs to water-soluble dye, its feature is to have water soluble group and reactive group, in the dyeing course active group can with fiber generation covalent bonds, thereby easily generation hydrolysis and alcoholysis in water, can not long preservation, thereby reduced the printing in textiles COLOR FASTNESS, ink easily decomposes, and stops up shower nozzle easily.
Chinese patent CN 100381634C discloses a kind of textiles digit printing REACTIVE DYES ink-jet ink and production technology thereof, comprising REACTIVE DYES, humectant, scale remover, bactericide, pH value conditioning agent, bleeding agent, deionized water, but because this textiles digit printing REACTIVE DYES ink-jet ink non-selected suitable pH value scope and dye composite, its look dynamics, COLOR FASTNESS and color rendition that is applied on real silk, cotton textiles, fiber crops, the viscose, particularly wool fabric is not good.
Summary of the invention
The objective of the invention is to solve problems of the prior art, provide look dynamics, COLOR FASTNESS and color rendition on a kind of suitable real silk, cotton textiles, fiber crops, the viscose, particularly wool fabric all good digit printing REACTIVE DYES ink-jet ink.
Technical scheme of the present invention is: a kind of digit printing REACTIVE DYES ink-jet ink, and it is composed of the following components by weight percentage:
REACTIVE DYES 1.0～20%;
Viscosity modifier 10～40%;
Surface tension modifier 0.2～2%;
PH value controlling agent 0.1～3.0%;
Bactericide 0.3～1.5%;
Its surplus of deionized water.
Described REACTIVE DYES is one or more in C.I. reactive black 5, C.I. reactive black 39, the active palm fibre 2 of C.I., the active palm fibre 11 of C.I., C.I. reactive blue 49, C.I. reactive blue 14, C.I. reactive blue 72, C.I. active blue 19 8, C.I. reactive red 15, C.I. REACTIVE RED 31, C.I. reactive red 245, C.I. reactive red 495, C.I. reactive red 281, C.I. reactive yellow 95, C.I. REACTIVE YELLOW 18 1, C.I. REACTIVE ORANGE 12, the C.I. REACTIVE ORANGE 13.
Described viscosity modifier is 1,5-pentanediol, 1, the mixture of one or more in 2-propylene glycol, dimethyl sulfoxide (DMSO), ethylene glycol benzyl oxide, dimethylacetylamide, triethylene glycol, diethylene glycol ether, the cetomacrogol 1000.
Described surface tension modifier is that alcohol alcoxylates is or/and polyether-modified dimethyl silicone polymer.
Described pH value controlling agent is one or more the mixture in NaOH, sodium carbonate, sodium bicarbonate, sodium dihydrogen phosphate, sodium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, triethanolamine, diethanol amine, monoethanolamine, lactic acid, citric acid, sulfuric acid, the hydrochloric acid.
Preferably, described bactericide is 5-chloro-2-methyl-4-isothiazoline-3-ketone.
The invention has the beneficial effects as follows: the digit printing REACTIVE DYES ink-jet ink that the present invention makes is suitable for printed fabrics, the fabric of real silk, cotton textiles, fiber crops, viscose and blended fiber thereof for example, particularly look dynamics, COLOR FASTNESS and the color rendition on wool fabric is better.
The specific embodiment
Embodiment 1
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: the active palm fibre 2 1% of C.I. reactive black 39 18%, C.I., the active palm fibre 11 1% of C.I., diethylene glycol ether 5%, cetomacrogol 1000 1%, triethylene glycol 4%, EH-3 surface tension modifier 0.1%, BYK-345 surface tension modifier 0.1%, sodium dihydrogen phosphate 0.05%, sodium hydrogen phosphate 0.05%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 1.5%, all the other are deionized water; Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-345 surface tension modifier that Bi Ke chemical company produces.
Embodiment 2
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. reactive blue 72 3%, C.I. reactive blue 14 8%, 1,5-pentanediol 15%, dimethylacetylamide 5%, ethylene glycol benzyl oxide 6%, EH-3 surface tension modifier 0.3%, BYK-348 surface tension modifier 0.5%, citric acid 2%, triethanolamine 1%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.3%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
Embodiment 3
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. reactive red 245 10%, C.I. REACTIVE RED 31 2%, 1,5-pentanediol 10%, triethylene glycol 10%, ethylene glycol benzyl oxide 5%, BYK-348 surface tension modifier 1.2%, EH-3 surface tension modifier 0.8%, lactic acid 0.5%, triethanolamine 0.3%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.5%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
Embodiment 4
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. reactive yellow 95 12%, C.I. REACTIVE YELLOW 18 1 1.5%, dimethylacetylamide 10%, 1,2-propylene glycol 5%, 1,5-pentanediol 3%, EH-6 surface tension modifier 0.5%, BYK-345 surface tension modifier 0.3%, sodium hydrogen phosphate 0.06%, potassium dihydrogen phosphate 0.04%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.6%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-6 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-345 surface tension modifier that Bi Ke chemical company produces.
Embodiment 5
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: the active palm fibre 2 0.1% of C.I. reactive black 39 0.9%, C.I., ethylene glycol benzyl oxide 15%, diethylene glycol ether 15%, dimethyl sulfoxide (DMSO) 10%, BYK-345 surface tension modifier 1%, EH-3 surface tension modifier 0.3%, lactic acid 0.3%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.3%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-345 surface tension modifier that Bi Ke chemical company produces.
Embodiment 6
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. reactive red 15 7%, C.I. reactive red 495 5%, 1,5-pentanediol 7%, triethylene glycol 15%, BYK-348 surface tension modifier 0.5%, EH-3 surface tension modifier 0.2%, triethanolamine 0.2%, lactic acid 0.4%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 1.2%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
Embodiment 7
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. active blue 19 8 5%, C.I. reactive yellow 95 6%, cetomacrogol 1000 2%, 1,2-propylene glycol 16%, BYK-348 surface tension modifier 0.4%, EH-3 surface tension modifier 0.2%, triethanolamine 0.1%, citric acid 0.3%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.8%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-3 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
Embodiment 8
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. reactive blue 49 10%, 1,2-propylene glycol 10%, diethylene glycol ether 10%, BYK-348 surface tension modifier 0.4%, EH-6 surface tension modifier 0.1%, triethanolamine 0.3%, lactic acid 0.6%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.7%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-6 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
Embodiment 9
Digit printing REACTIVE DYES ink-jet ink, it comprises following component by weight percentage: C.I. REACTIVE ORANGE 13 8%, C.I. REACTIVE ORANGE 12 4%, cetomacrogol 1000 3%, diethylene glycol ether 10%, 1,2-propylene glycol 10%, BYK-348 surface tension modifier 0.5%, EH-6 surface tension modifier 0.1%, triethanolamine 0.2%, citric acid 0.5%, 5-chloro-2-methyl-4-isothiazoline-3-ketone 0.8%, all the other are deionized water.Said components is mixed in proportion after 0.22 micron membrane filtration can make digit printing REACTIVE DYES ink-jet ink.The EH-6 surface tension modifier that the preferred LG-DOW of present embodiment company produces, the BYK-348 surface tension modifier that Bi Ke chemical company produces.
The digit printing REACTIVE DYES ink-jet ink that provides among the present invention may be used on minute-pressure electricity, heat foamable printer; Stay in grade can store for a long time, meets the light industry standard QB/T 2730-2005 of the People's Republic of China (PRC), and the product evaluation of the embodiment of the invention 1～embodiment 9 preparations the results are shown in table 1.
Table 1
The digit printing REACTIVE DYES ink-jet ink that embodiment 1～embodiment 9 is made is 60 ℃ of one weeks of environmental aging: the digit printing REACTIVE DYES ink-jet ink that embodiment 1～embodiment 5 makes is via the following pre-treatment composition of mass percent: guar gum 4%, urea 4%, sodium carbonate 2%, print monochromatic color lump on the cotton fabrics after sodium bicarbonate 2% is handled, the digit printing REACTIVE DYES ink-jet ink that embodiment 6～embodiment 9 makes is via the following pre-treatment composition of mass percent: guar gum 4%, urea 4%, sodium carbonate 2%, print monochromatic color lump on the wool fabric after sodium bicarbonate 2% is handled, the fastness before and after contrast is aging and the reappearance of look dynamics, the look dynamics represents that with L*a*b comparing result is listed in table 2.
Table 2
Claims (6)
1. digit printing REACTIVE DYES ink-jet ink, it is characterized in that: it is composed of the following components by weight percentage:
REACTIVE DYES 1.0～20%;
Viscosity modifier 10～40%;
Surface tension modifier 0.2～2%;
PH value controlling agent 0.1～3.0%;
Bactericide 0.3～1.5%;
Its surplus of deionized water.
2. digit printing REACTIVE DYES ink-jet ink according to claim 1 is characterized in that: described REACTIVE DYES is one or more in C.I. reactive black 5, C.I. reactive black 39, the active palm fibre 2 of C.I., the active palm fibre 11 of C.I., C.I. reactive blue 49, C.I. reactive blue 14, C.I. reactive blue 72, C.I. active blue 19 8, C.I. reactive red 15, C.I. REACTIVE RED 31, C.I. reactive red 245, C.I. reactive red 495, C.I. reactive red 281, C.I. reactive yellow 95, C.I. REACTIVE YELLOW 18 1, C.I. REACTIVE ORANGE 12, the C.I. REACTIVE ORANGE 13.
3. digit printing REACTIVE DYES ink-jet ink according to claim 1, it is characterized in that: described viscosity modifier is 1,5-pentanediol, 1, the mixture of one or more in 2-propylene glycol, dimethyl sulfoxide (DMSO), ethylene glycol benzyl oxide, dimethylacetylamide, triethylene glycol, diethylene glycol ether, the cetomacrogol 1000.
4. digit printing REACTIVE DYES ink-jet ink according to claim 1 is characterized in that: described surface tension modifier is that alcohol alcoxylates is or/and polyether-modified dimethyl silicone polymer.
5. digit printing REACTIVE DYES ink-jet ink according to claim 1 is characterized in that: described pH value controlling agent is one or more the mixture in NaOH, sodium carbonate, sodium bicarbonate, sodium dihydrogen phosphate, sodium hydrogen phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, triethanolamine, diethanol amine, monoethanolamine, lactic acid, citric acid, sulfuric acid, the hydrochloric acid.
6. digit printing REACTIVE DYES ink-jet ink according to claim 1 is characterized in that: described bactericide is 5-chloro-2-methyl-4-isothiazoline-3-ketone.
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| CN102352571A (en) * | 2011-09-30 | 2012-02-15 | 郑州鸿盛数码科技股份有限公司 | Jet ink for digit printing of blend fabrics |
| CN102352569A (en) * | 2011-09-30 | 2012-02-15 | 郑州鸿盛数码科技股份有限公司 | Ink-jet ink for water-borne digital printing and production process thereof |
| CN102391722A (en) * | 2011-09-30 | 2012-03-28 | 郑州鸿盛数码科技股份有限公司 | Ink with metal luster |
| CN102936434A (en) * | 2012-02-10 | 2013-02-20 | 日冠(福建)针纺织机械有限公司 | Digital ink-jet ink applied to cellulose fiber fabric |
| JP2015078346A (en) * | 2013-09-12 | 2015-04-23 | 日本化薬株式会社 | Ink composition and printing method for fiber |
| CN105442348A (en) * | 2014-09-15 | 2016-03-30 | 珠海保税区天然宝杰数码科技材料有限公司 | Digital printing active ink |
| CN105603778A (en) * | 2016-02-19 | 2016-05-25 | 太仓市鑫泰针织有限公司 | Active ink for real silk fabric embroidery |
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| CN110878480A (en) * | 2019-05-31 | 2020-03-13 | 浙江工业大学 | Active ink for digital printing and preparation method thereof |
| CN110878480B (en) * | 2019-05-31 | 2022-06-21 | 浙江工业大学 | Active ink for digital printing and preparation method thereof |
| CN110437675A (en) * | 2019-08-07 | 2019-11-12 | 中纺院（浙江）技术研究院有限公司 | A kind of digital printing method of active ink and multi-component fiber fabric |
| CN113106767A (en) * | 2021-04-23 | 2021-07-13 | 广东溢达纺织有限公司 | Method for dyeing fabric |
| CN113354986A (en) * | 2021-06-28 | 2021-09-07 | 青岛英杰泰新材料有限公司 | Navy blue colorant for ink-jet printing and preparation method thereof |
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| CN102108641B (en) | 2012-09-05 |
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Denomination of invention: A reactive dye inkjet ink for digital printing Effective date of registration: 20221230 Granted publication date: 20120905 Pledgee: Bank of Zhengzhou Co.,Ltd. Zhongyuan Science and Technology City Sub branch Pledgor: HONGSAM DIGITAL SCIENCE & TECHNOLOGY Co.,Ltd. Registration number: Y2022980029740 |
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