CN106480753A - A kind of real silk blend polyester fabric digit printing ink and preparation method thereof - Google Patents
A kind of real silk blend polyester fabric digit printing ink and preparation method thereof Download PDFInfo
- Publication number
- CN106480753A CN106480753A CN201610762828.XA CN201610762828A CN106480753A CN 106480753 A CN106480753 A CN 106480753A CN 201610762828 A CN201610762828 A CN 201610762828A CN 106480753 A CN106480753 A CN 106480753A
- Authority
- CN
- China
- Prior art keywords
- printing ink
- real silk
- polyester fabric
- schardinger dextrin
- digit printing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000007639 printing Methods 0.000 title claims abstract description 35
- 239000000203 mixture Substances 0.000 title claims abstract description 33
- 239000004744 fabric Substances 0.000 title claims abstract description 28
- 229920000728 polyester Polymers 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims description 12
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical class OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000008367 deionised water Substances 0.000 claims abstract description 22
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 22
- 239000002270 dispersing agent Substances 0.000 claims abstract description 17
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 14
- 239000000985 reactive dye Substances 0.000 claims abstract description 9
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims abstract description 7
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 7
- 239000004202 carbamide Substances 0.000 claims abstract description 7
- 239000010446 mirabilite Substances 0.000 claims abstract description 7
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 7
- 235000017550 sodium carbonate Nutrition 0.000 claims abstract description 7
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 6
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 6
- 239000000661 sodium alginate Substances 0.000 claims abstract description 6
- 238000003756 stirring Methods 0.000 claims description 19
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 15
- 239000002202 Polyethylene glycol Substances 0.000 claims description 10
- 229920001223 polyethylene glycol Polymers 0.000 claims description 10
- 239000000080 wetting agent Substances 0.000 claims description 5
- GPRLSGONYQIRFK-MNYXATJNSA-N triton Chemical compound [3H+] GPRLSGONYQIRFK-MNYXATJNSA-N 0.000 claims 1
- 229920000858 Cyclodextrin Polymers 0.000 abstract description 15
- 108090000623 proteins and genes Proteins 0.000 abstract description 3
- 102000004169 proteins and genes Human genes 0.000 abstract description 3
- 238000003854 Surface Print Methods 0.000 abstract description 2
- 239000002932 luster Substances 0.000 abstract description 2
- 239000001116 FEMA 4028 Substances 0.000 abstract 1
- 235000011175 beta-cyclodextrine Nutrition 0.000 abstract 1
- 229960004853 betadex Drugs 0.000 abstract 1
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 16
- 238000005516 engineering process Methods 0.000 description 8
- 230000002209 hydrophobic effect Effects 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 238000011161 development Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000835 fiber Substances 0.000 description 3
- 125000002791 glucosyl group Chemical group C1([C@H](O)[C@@H](O)[C@H](O)[C@H](O1)CO)* 0.000 description 3
- 238000007641 inkjet printing Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- 241001116389 Aloe Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 108090000790 Enzymes Proteins 0.000 description 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 229920004933 Terylene® Polymers 0.000 description 2
- 235000011399 aloe vera Nutrition 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229920000856 Amylose Polymers 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 101100002917 Caenorhabditis elegans ash-2 gene Proteins 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 125000003535 D-glucopyranosyl group Chemical group [H]OC([H])([H])[C@@]1([H])OC([H])(*)[C@]([H])(O[H])[C@@]([H])(O[H])[C@]1([H])O[H] 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 238000005481 NMR spectroscopy Methods 0.000 description 1
- 102000004357 Transferases Human genes 0.000 description 1
- 108090000992 Transferases Proteins 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000001139 anti-pruritic effect Effects 0.000 description 1
- 239000003908 antipruritic agent Substances 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- -1 cyclic oligosaccharides Chemical class 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010017 direct printing Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000002329 infrared spectrum Methods 0.000 description 1
- 230000002401 inhibitory effect Effects 0.000 description 1
- 229910001872 inorganic gas Inorganic materials 0.000 description 1
- 229910001410 inorganic ion Inorganic materials 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229920001542 oligosaccharide Polymers 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 238000010183 spectrum analysis Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010023 transfer printing Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
- D06P1/6491—(Thio)urea or (cyclic) derivatives
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/82—Textiles which contain different kinds of fibres
- D06P3/8204—Textiles which contain different kinds of fibres fibres of different chemical nature
- D06P3/8209—Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing amide groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Molecular Biology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Coloring (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides a kind of real silk blend polyester fabric digit printing ink, including following main component:Reactive dye, sodium alginate, urea, glauber salt, soda ash, poly ethyldiol modified beta cyclodextrin, dispersant and deionized water, by adding poly ethyldiol modified beta cyclodextrin in traditional printing ink, improve the binding ability of beta cyclodextrin and protein in silk, the Color of reactive dye is greatly improved, to real silk surface printing, bright in luster, color fastness is high.
Description
Technical field
The present invention relates to digital printing technology field, more particularly to a kind of real silk blend polyester fabric digit printing ink
And preparation method thereof.
Background technology
Digital ink-jet printed technology is a big expansion of the inkjet printing in industrial application.Modern computer inkjet printing
When technology is used for printing in textiles, can be with various input mediums such as scanner, digital camera, digital camera etc., need
The pattern that wants with digital input computer, after various mapping software color separation in printing systems are processed, then through computer control
The digital inkjet printing machine of system, is directly ejected into printing ink on various fabrics, the various patterns needed for printing out, this
Plant printing technique and be referred to as digital inking printing.
In recent years, digital printing technology has obtained rapid development.Compared with Conventional decal, digit printing technique is cleaned,
Production process flexibly, can remotely be ordered goods, be included supply chain network, be the direction of following printing in textiles technology development.
At present, digit printing kind includes the fabric of the types such as cotton, hair, chemical fibre, also has the fabrics such as a small amount of design silk, by
In the characteristic of real silk, its surface is relatively smooth, no matter digital direct printing is therefore adopted, or digital transfer printing, can all deposit
Colour vividness is inadequate, fidelity not enough, print off the product quality that comes low;Product color fastness is low, it is impossible to meets washing and requires
Problem, and the continuous development with Modern Textile Industry, terylene imitated silk face fabric are increasingly subject to people's attention, wherein add
Accounting of the imitative silk face fabric of part real silk in silk fabrics is larger, and during stamp, the dyeing of terylene and cocoon fiber is equal
Even property is difficult point.
Content of the invention
In order to solve the problems, such as in background technology, the present invention provides a kind of real silk blend polyester fabric digit printing ink
And preparation method thereof.
A kind of real silk blend polyester fabric digit printing ink, including the composition of following percentage by weight:
Reactive dye 8-15%
Sodium alginate 1-2%
Urea 2-5%
Glauber salt 2-4%
Soda ash 0.5-2%
Poly ethyldiol modified beta-schardinger dextrin 1-3%
Dispersant 0.2-0.5%
Deionized water surplus.
Preferably, described dispersant isX-405 wetting agent.
A kind of real silk blend polyester fabric preparation method of digit printing ink, comprises the following steps:
Under the conditions of A, 60-80 DEG C, poly ethyldiol modified beta-schardinger dextrin is dissolved in deionized water, polyethylene glycol is added, is stirred
After mixing 3-5 hour, room temperature is down to, stands, filter, dry, obtain modified beta-schardinger dextrin;
B, by modified beta-schardinger dextrin, dispersant and deionized water mix after, stir;
C, addition surplus stock, continue stirring, stir.
Preferably, in described step A, the mol ratio of ethylene glycol and beta-schardinger dextrin is 1:(5-7).
Preferably, in described step A, beta-schardinger dextrin is 1 with the mass ratio of deionized water:(20-30).
Preferably, the molecular weight of described polyethylene glycol is 3500-5000.
Cyclodextrin (Cyclodextr in, abbreviation CD) is amylose in the cyclodextrin glucose produced by bacillus
A series of general name of the lower cyclic oligosaccharides for generating of based transferase effect, usually contains 6~12 D- glucopyranose units.Its
Middle study more and be the molecule containing 6,7,8 glucose units with important practical usage, be referred to as
Alpha-, beta- and gama- cyclodextrin.According to the result of X- line crystal diffraction, infrared spectrum and spectral analysis of the nuclear magnetic resonance,
Determine that each D (+)-glucopyranose for constituting cyclodextrin molecular is chair conformation.Each glucose unit is all with Isosorbide-5-Nitrae-glucosides
Bond synthesis ring.As the glycosidic bond for connecting glucose unit can not be rotated freely, cyclodextrin is not cylindric molecule but summary
Tapered annulus.
As the outer rim (Rim) of cyclodextrin is hydrophilic and inner chamber (Cavi ty) is hydrophobic, thus it can provide one as enzyme
Individual hydrophobic binding site, as the various appropriate objects (Guest) of main body (Host) envelope, such as organic molecule, inorganic ions
And gas molecule etc..The hydrophobic and characteristic of external hydrophilic of its inner chamber makes which can be according to Van der Waals force, hydrophobic interaction power, master
Matching effect between guest molecule etc. and many organic and inorganic molecule form inclusion compound and molecular assembled system, become chemistry and
Chemical research person research object interested.This selective tetra-inclusion complex is usually said molecular recognition, and its result is
Form Subjective and Objective inclusion complex (Host-GuestComplex).Cyclodextrin is that the preferable host similar to enzyme for being found so far divides
Son, and itself just has the characteristic of catalator.Therefore, in the fields such as catalysis, separation, food and medicine, cyclodextrin is received
Great attention is arrived and has extensively applied.Due to solubility of the cyclodextrin in water and inclusion ability, change the physics and chemistry of cyclodextrin
Characteristic has become one of free-revving engine of Chemical modified cyclodextrin.
The compound of cyclodextrin is present in natural, it is also possible to artificial synthesized.Industrial, many dyestuffs are made with cyclodextrin
Matrix;And the medicinal plant of not rare medical functions, such as aloe, all contain cyclodextrin complexes.For example in the middle of the gel of aloe
Cyclodextrin complexes, have anti-inflammatory, detumescence, pain relieving, the effectiveness of antipruritic and bacteria growing inhibiting, natural vulnerary can be used as.
Additionally, using cyclodextrin cyclodextrin method be produce hydrogen peroxide the best approach.
By beta-schardinger dextrin with poly ethyldiol modified in the present invention, can not only improve solubility of the beta-schardinger dextrin in water and
Dispersive property, improves the contact surface of beta-schardinger dextrin and silk, and also improves the combination of beta-schardinger dextrin and protein in silk
Performance, is conducive to improving the Color of reactive dye.
The real silk blend polyester fabric digit printing ink of the present invention, including following main component:Reactive dye, marine alga
Sour sodium, urea, glauber salt, soda ash, poly ethyldiol modified beta-schardinger dextrin, dispersant and deionized water, by traditional stamp
Poly ethyldiol modified beta-schardinger dextrin is added in ink, improves the binding ability of beta-schardinger dextrin and protein in silk, activity dye
The Color of material is greatly improved, to real silk surface printing, bright in luster, and color fastness is high, especially fine to real silk blend polyester
The dyeing uniformity of dimension is very good.
Specific implementation method
Embodiment 1
A kind of real silk blend polyester fabric digit printing ink, including the composition of following percentage by weight:
Reactive dye 12%
Sodium alginate 1.5%
Urea 3%
Glauber salt 3%
Soda ash 1.2%
Poly ethyldiol modified beta-schardinger dextrin 1.5%
Dispersant 0.3%
Deionized water surplus;
Described dispersant isX-405 wetting agent;
A kind of real silk blend polyester fabric preparation method of digit printing ink, comprises the following steps:
A, under the conditions of 75 DEG C, poly ethyldiol modified beta-schardinger dextrin is dissolved in deionized water, adds polyethylene glycol, stirring
After 3.5 hours, room temperature is down to, stands, filter, dry, obtain modified beta-schardinger dextrin;
B, by modified beta-schardinger dextrin, dispersant and deionized water mix after, stir;
C, addition surplus stock, continue stirring, stir;
In described step A, the mol ratio of ethylene glycol and beta-schardinger dextrin is 1:6;
In described step A, beta-schardinger dextrin is 1 with the mass ratio of deionized water:25;
The molecular weight of described polyethylene glycol is 3500-5000.
Embodiment 2
A kind of real silk blend polyester fabric digit printing ink, including the composition of following percentage by weight:
Reactive dye 15%
Sodium alginate 1%
Urea 5%
Glauber salt 2%
Soda ash 0.5%
Poly ethyldiol modified beta-schardinger dextrin 3%
Dispersant 0.2%
Deionized water surplus;
Described dispersant isX-405 wetting agent;
A kind of real silk blend polyester fabric preparation method of digit printing ink, comprises the following steps:
A, under the conditions of 80 DEG C, poly ethyldiol modified beta-schardinger dextrin is dissolved in deionized water, adds polyethylene glycol, stirring 3
After hour, room temperature is down to, stands, filter, dry, obtain modified beta-schardinger dextrin;
B, by modified beta-schardinger dextrin, dispersant and deionized water mix after, stir;
C, addition surplus stock, continue stirring, stir;
In described step A, the mol ratio of ethylene glycol and beta-schardinger dextrin is 1:7;
In described step A, beta-schardinger dextrin is 1 with the mass ratio of deionized water:20;
The molecular weight of described polyethylene glycol is 3500-5000.
Embodiment 3
A kind of real silk blend polyester fabric digit printing ink, including the composition of following percentage by weight:
Reactive dye 8%
Sodium alginate 2%
Urea 2%
Glauber salt 4%
Soda ash 2%
Poly ethyldiol modified beta-schardinger dextrin 1%
Dispersant 0.5%
Deionized water surplus;
Described dispersant isX-405 wetting agent;
A kind of real silk blend polyester fabric preparation method of digit printing ink, comprises the following steps:
A, under the conditions of 60 DEG C, poly ethyldiol modified beta-schardinger dextrin is dissolved in deionized water, adds polyethylene glycol, stirring 5
After hour, room temperature is down to, stands, filter, dry, obtain modified beta-schardinger dextrin;
B, by modified beta-schardinger dextrin, dispersant and deionized water mix after, stir;
C, addition surplus stock, continue stirring, stir;
In described step A, the mol ratio of ethylene glycol and beta-schardinger dextrin is 1:5;
In described step A, beta-schardinger dextrin is 1 with the mass ratio of deionized water:30;
The molecular weight of described polyethylene glycol is 3500-5000.
Real silk blend polyester fabric to embodiment 1-3 carries out spray printing with digit printing ink, and the resistance to of test fabric is soaped
Color fastness, colour fastness to rubbing, fastness to light are tested, and the results are shown in Table 1.
Table 1:
By test data it is recognised that the printing ink made of the present invention, for real silk blend polyester fiber stamp, color jail
Degree is high, even across being cleaned multiple times, remain to colour-fast, fade, keep original color and vividness.
The above, the only present invention preferably specific embodiment, but protection scope of the present invention is not limited thereto,
Any those familiar with the art the invention discloses technical scope in, technology according to the present invention scheme and its
Inventive concept equivalent or change in addition, should all be included within the scope of the present invention.
Claims (6)
1. a kind of real silk blend polyester fabric digit printing ink, it is characterised in that including the composition of following percentage by weight:
Reactive dye 8-15%
Sodium alginate 1-2%
Urea 2-5%
Glauber salt 2-4%
Soda ash 0.5-2%
Poly ethyldiol modified beta-schardinger dextrin 1-3%
Dispersant 0.2-0.5%
Deionized water surplus.
2. real silk blend polyester fabric digit printing ink as claimed in claim 1, it is characterised in that described dispersant
For TRITON X-405 wetting agent.
3. a kind of real silk blend polyester fabric preparation method of digit printing ink, it is characterised in that comprise the following steps:
Under the conditions of A, 60-80 DEG C, poly ethyldiol modified beta-schardinger dextrin is dissolved in deionized water, polyethylene glycol is added, stir 3-5
After hour, room temperature is down to, stands, filter, dry, obtain modified beta-schardinger dextrin;
B, by modified beta-schardinger dextrin, dispersant and deionized water mix after, stir;
C, addition surplus stock, continue stirring, stir.
4. the real silk blend polyester fabric as claimed in claim 3 preparation method of digit printing ink, it is characterised in that institute
In the step of stating A, the mol ratio of ethylene glycol and beta-schardinger dextrin is 1:(5-7).
5. the real silk blend polyester fabric as claimed in claim 3 preparation method of digit printing ink, it is characterised in that institute
In the step of stating A, beta-schardinger dextrin is 1 with the mass ratio of deionized water:(20-30).
6. the real silk blend polyester fabric as claimed in claim 3 preparation method of digit printing ink, it is characterised in that institute
The molecular weight of the polyethylene glycol that states is 3500-5000.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610762828.XA CN106480753B (en) | 2016-08-31 | 2016-08-31 | A kind of silk blend polyester fabric digit printing ink and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201610762828.XA CN106480753B (en) | 2016-08-31 | 2016-08-31 | A kind of silk blend polyester fabric digit printing ink and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106480753A true CN106480753A (en) | 2017-03-08 |
CN106480753B CN106480753B (en) | 2019-04-12 |
Family
ID=58273940
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201610762828.XA Expired - Fee Related CN106480753B (en) | 2016-08-31 | 2016-08-31 | A kind of silk blend polyester fabric digit printing ink and preparation method thereof |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106480753B (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109097980A (en) * | 2018-07-23 | 2018-12-28 | 含山县海达服饰有限公司 | A kind for the treatment of process improving swimming trunks polyester fabric equalization |
CN113774691A (en) * | 2021-09-17 | 2021-12-10 | 浙江迎丰科技股份有限公司 | Printing ink auxiliary agent and preparation method thereof |
CN115595809A (en) * | 2022-10-25 | 2023-01-13 | 东莞市伊时针织印花有限公司(Cn) | Acid dye for protein fiber fabric and preparation method thereof |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101280526A (en) * | 2008-05-26 | 2008-10-08 | 东华大学 | Method for dyeing mercerization baffeta with deep color on reactive dyes |
CN102108641A (en) * | 2011-01-12 | 2011-06-29 | 郑州鸿盛数码科技股份有限公司 | Digital printing active dye jet ink |
CN102408751A (en) * | 2010-09-26 | 2012-04-11 | 大丰市千采精细化工有限公司 | Acid dye |
CN103642190A (en) * | 2013-12-12 | 2014-03-19 | 东华大学 | Polyethylene glycol modified cyclodextrin, as well as preparation and application thereof |
CN103774464A (en) * | 2013-12-31 | 2014-05-07 | 吉林中粮生化有限公司 | Application of mycose-contained cyclodextrin inclusion compound in dyeing |
CN104726956A (en) * | 2015-03-13 | 2015-06-24 | 东华大学 | Preparation method of cyclodextrin compound modified polyurethane elastic fibers |
CN105008468A (en) * | 2013-03-07 | 2015-10-28 | 奥西-技术有限公司 | Ink composition |
CN105369652A (en) * | 2015-10-08 | 2016-03-02 | 深圳市墨库图文技术有限公司 | Ink and preparing method thereof |
CN105803827A (en) * | 2016-04-01 | 2016-07-27 | 华南师范大学 | Ink-jet ink and application thereof |
CN105860668A (en) * | 2016-06-07 | 2016-08-17 | 湖北科亿华科技有限公司 | Manufacturing method of edible printing ink for ink jet printing and using method thereof |
-
2016
- 2016-08-31 CN CN201610762828.XA patent/CN106480753B/en not_active Expired - Fee Related
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101280526A (en) * | 2008-05-26 | 2008-10-08 | 东华大学 | Method for dyeing mercerization baffeta with deep color on reactive dyes |
CN102408751A (en) * | 2010-09-26 | 2012-04-11 | 大丰市千采精细化工有限公司 | Acid dye |
CN102108641A (en) * | 2011-01-12 | 2011-06-29 | 郑州鸿盛数码科技股份有限公司 | Digital printing active dye jet ink |
CN105008468A (en) * | 2013-03-07 | 2015-10-28 | 奥西-技术有限公司 | Ink composition |
CN103642190A (en) * | 2013-12-12 | 2014-03-19 | 东华大学 | Polyethylene glycol modified cyclodextrin, as well as preparation and application thereof |
CN103774464A (en) * | 2013-12-31 | 2014-05-07 | 吉林中粮生化有限公司 | Application of mycose-contained cyclodextrin inclusion compound in dyeing |
CN104726956A (en) * | 2015-03-13 | 2015-06-24 | 东华大学 | Preparation method of cyclodextrin compound modified polyurethane elastic fibers |
CN105369652A (en) * | 2015-10-08 | 2016-03-02 | 深圳市墨库图文技术有限公司 | Ink and preparing method thereof |
CN105803827A (en) * | 2016-04-01 | 2016-07-27 | 华南师范大学 | Ink-jet ink and application thereof |
CN105860668A (en) * | 2016-06-07 | 2016-08-17 | 湖北科亿华科技有限公司 | Manufacturing method of edible printing ink for ink jet printing and using method thereof |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109097980A (en) * | 2018-07-23 | 2018-12-28 | 含山县海达服饰有限公司 | A kind for the treatment of process improving swimming trunks polyester fabric equalization |
CN113774691A (en) * | 2021-09-17 | 2021-12-10 | 浙江迎丰科技股份有限公司 | Printing ink auxiliary agent and preparation method thereof |
CN113774691B (en) * | 2021-09-17 | 2023-08-08 | 浙江迎丰科技股份有限公司 | Printing ink auxiliary agent and preparation method thereof |
CN115595809A (en) * | 2022-10-25 | 2023-01-13 | 东莞市伊时针织印花有限公司(Cn) | Acid dye for protein fiber fabric and preparation method thereof |
Also Published As
Publication number | Publication date |
---|---|
CN106480753B (en) | 2019-04-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP2597194B1 (en) | Cold transfer printing paste, printing colorant thereof, and preparation method thereof | |
CN106480753A (en) | A kind of real silk blend polyester fabric digit printing ink and preparation method thereof | |
CN101408003B (en) | Environment protection type coating discharge printing pulp and discharge printing process thereof | |
CN101314920B (en) | Complex printing gum for reactive dye and preparation method thereof | |
CN102978971B (en) | Disperse dye printing gum | |
CN101768877A (en) | Sodium alginate composite printing paste and application thereof | |
CN107142750A (en) | A kind of preparation method of Disperse Printing composite paste material | |
CN101158119A (en) | Non-formaldehyde dischargeable protoplasm and preparation method and usage thereof | |
CN106468024B (en) | A kind of silk digit printing ink and preparation method thereof | |
CN109853262A (en) | A kind of ink-jet printed method of the method for enzymatically treating and wool fabric of wool fabric | |
Yıldırım et al. | Printing with sustainable natural dyes and pigments | |
CN110863373B (en) | Active digital printing thickener composition and preparation method thereof | |
CN104480746B (en) | A kind of cotton and polyamide fibre blending or interwoven fabric one-bath one-step dyeing dyeing | |
CN112176743B (en) | Modified chitin paste for polyamide fabric vat dye printing and preparation method and application thereof | |
Chaudhary et al. | Eco-Friendly Tamarind Kernel Thickener for Printing of Polyester Using Disperse Dyes | |
CN107869068A (en) | Carded hair rubber cement pigment printing fabric | |
CN106243834A (en) | One is printed upon non-fading ink and application process thereof on cotton | |
CN104988729A (en) | Purified cotton starching agent and preparation technology thereof | |
CN105862464B (en) | A kind of print paste of silk fabric and the printing technology using the print paste | |
Li et al. | Novel transfer printing paper for silk printing with reactive dye | |
CN106835753B (en) | Printing gum and the printing method for using it | |
CN112111175A (en) | Black dye for leather and preparation method thereof | |
CN108642920A (en) | A kind of fabric printing process of water-fastness anti-dropout | |
CN114855473B (en) | Dyeing method of cellulose fiber material | |
CN108530941A (en) | A kind of dark blue reactive dye and application thereof |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A digital printing ink for silk polyester blended fabric and its preparation method Effective date of registration: 20210702 Granted publication date: 20190412 Pledgee: Agricultural Bank of China Limited Deqing County sub branch Pledgor: ZHEJIANG DEYU IMPORT & EXPORT Co.,Ltd. Registration number: Y2021330000794 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20190412 |