CN109098014A - A kind of reactive dye ink of digital inking printing and preparation method thereof - Google Patents
A kind of reactive dye ink of digital inking printing and preparation method thereof Download PDFInfo
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- CN109098014A CN109098014A CN201810904298.7A CN201810904298A CN109098014A CN 109098014 A CN109098014 A CN 109098014A CN 201810904298 A CN201810904298 A CN 201810904298A CN 109098014 A CN109098014 A CN 109098014A
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- reactive dye
- dye ink
- digital inking
- inking printing
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/36—Inkjet printing inks based on non-aqueous solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/645—Aliphatic, araliphatic or cycloaliphatic compounds containing amino groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/10—Material containing basic nitrogen containing amide groups using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
- D06P3/66—Natural or regenerated cellulose using reactive dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses reactive dye ink of a kind of digital inking printing and preparation method thereof, which includes the following substance measured according to the mass fraction: active colorant 5-15 parts, 20-40 parts of organic solvent, 5-12 parts of water hyacinth clear liquid, 3-5 parts of surfactant, 1-3 parts of fungicide, 3-8 parts of auxiliary agent, 1-3 parts of PH regulator, 40-80 parts of deionized water.The present invention is a kind of reactive dye ink suitable for protein fibre fabric and cellulose base fiber fabric, have it is bright in luster, dye-uptake is high, storage stability is good, be not susceptible to hydrolysis, printing fluency it is good, the good advantage of using effect.
Description
Technical field
The present invention relates to printing in textiles field, in particular to the reactive dye ink and its system of a kind of digital inking printing
Preparation Method.
Background technique
With China's expanding economy, the improvement of people's living standards, major transformation has occurred for piece market consumption concept,
People are growing day by day to the consumption demand of " personalization, multi items, short cycle, cultural creative and environmental protection " textile.Digital ink-jet
Stamp has abandoned the mask-making technology of Conventional decal complexity, in addition to can satisfy market to stamp small lot, multi-color and personalization
Demand outside, it is a kind of that occupation area of equipment is small, and printing technology more saves dye material and water resource compared to Conventional decal
The clearer production technology of ecological environment-friendly type is able to satisfy the requirement of dyeing environmental protection low-carbon sustainable development.As it can be seen that ink-jet printed
The propensity to consume for having agreed with people, is rapidly developed.
The demand of the natural fibers such as cotton and silk kind fabric in recent years increases year by year, and reactive dye ink is cellulose fiber
Colorant is commonly used on peacekeeping protein fibre, has the characteristics that Printing color fastness is high, chromatography is complete and bright in colour.With number
The sustainable development of the ink-jet printed technology of code, market constantly increases the demand of reactive dye ink.However, current active dyestuff
There are still some drawbacks, such as dyestuff, and hydrolysis, poor storage stability, stamp process not high to the dye-uptake of fabric easily occurs for ink
Middle generation spray head blocks, printing fluency is low etc..
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of reactive dye ink of digital inking printing and its preparations
Method, by improveing to ink composition, solving current active dye ink, there are dyestuffs, and hydrolysis, stable storing easily occurs
Property poor, not high to the dye-uptake of fabric, stamp during spray head blocking occurs, the problem of printing fluency is low etc..
In order to achieve the above objectives, technical scheme is as follows: a kind of reactive dye ink of digital inking printing, packet
Include the following substance measured according to the mass fraction:
As a preferred solution of the present invention, after the water hyacinth clear liquid is by pulverizing water hyacinth, slurries are filtered to obtain,
Then by being obtained after membrane filtration 2 times of 0.5-1 μm.
As a preferred solution of the present invention, the auxiliary agent includes defoaming agent, moisturizer, viscosity modifier and infiltration
Agent.
As a preferred solution of the present invention, the organic solvent is polyethylene glycol, diethylene glycol (DEG), propylene glycol with mass ratio
For the mixed solvent of 2:1:1 mixing.
As a preferred solution of the present invention, the surfactant is glycols or naphthalene sulfonic acids class surfactant.
As a preferred solution of the present invention, the PH regulator be trimethylamine, triethanolamine, ammonium hydroxide, sodium citrate,
One of sodium bicarbonate.
A kind of preparation method of the reactive dye ink of digital inking printing described in claim 1, comprising the following steps:
Step 1, water hyacinth is pulverized into grinding, filtering residue obtains slurries, then by after membrane filtration 2 times of 0.5-1 μm
Obtain the water hyacinth clear liquid；
Step 2, active colorant is added in water hyacinth clear liquid and is stirred evenly, added the organic solvent, stir evenly,
Other substances of the reactive dye ink are added later, is uniformly mixed, passes through 2 μm of membrane filtration；
Step 3, the filtered filtrate of step 2 is heated, is heated to 50-60 DEG C, is then cooled in 2-3min
15-20 DEG C, then removal of impurities, finished product are successively filtered by the filter membrane of 0.5 μm, 0.1 μm.
Through the above technical solutions, the significant beneficial effect of technical solution of the present invention is: the present invention is a kind of suitable for egg
The reactive dye ink of white matter fiber fabric and cellulose base fiber fabric, with bright in luster, dye-uptake is high, storage stability
Good, it is good to be not susceptible to hydrolysis, printing fluency, the good advantage of using effect.The present invention uses the organic solvent of mixed type, can
Collaboration facilitation is played, contains hydrophobic alkyl in organic solvent, hydrogen bond can be formed with dyestuff in water, make dye ions
Surface formed hydrated ion protective layer, prevent dye molecule agglomerate and intermolecular interaction, promote dyestuff ionization and
Dissolution, increases its solvability, the addition of polyethylene glycol can significantly improve the solubility of dyestuff；And diethylene glycol (DEG) is matched with propylene glycol
It closes, dye molecule can be made to form micella in water, there is preferable dispersibility, and can also make that there is polar dyestuff to constitute glue
At the netted solubilising of model between the solvent molecule of beam, to form uniform apparent dissolution phenomena, dissolubility is improved；Water is added
Cucurbit clear liquid helps to improve the permeability of ink, can effectively improve the dye-uptake of dyestuff, while keeping color more bright-coloured, no
Fugitive color.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
The invention discloses a kind of reactive dye inks of digital inking printing, including the following object measured according to the mass fraction
Matter:
Wherein, after the water hyacinth clear liquid is by pulverizing water hyacinth, slurries are filtered to obtain, then pass through 0.5 μm of filter membrane
It is obtained after filtering 2 times.The organic solvent be polyethylene glycol, diethylene glycol (DEG), propylene glycol with mass ratio be 2:1:1 mixing mixing it is molten
Agent.
The preparation method of the reactive dye ink of above-mentioned digital inking printing, comprising the following steps:
Step 1, water hyacinth is pulverized into grinding, filtering residue obtains slurries, then by obtaining after membrane filtration 2 times of 0.5 μm
To the water hyacinth clear liquid；
Step 2, active colorant is added in water hyacinth clear liquid and is stirred evenly, added the organic solvent, stir evenly,
Other substances of above-mentioned reactive dye ink are added later, is uniformly mixed, passes through 2 μm of membrane filtration；
Step 3, the filtered filtrate of step 2 is heated, is heated to 50-60 DEG C, is then cooled in 2-3min
15-20 DEG C, then removal of impurities, finished product are successively filtered by the filter membrane of 0.5 μm, 0.1 μm.
Embodiment 2
A kind of reactive dye ink of digital inking printing, including the following substance measured according to the mass fraction:
Wherein, after the water hyacinth clear liquid is by pulverizing water hyacinth, slurries are filtered to obtain, then pass through 1 μm of filter membrane mistake
It is obtained after filter 2 times.The auxiliary agent includes defoaming agent, moisturizer, viscosity modifier and bleeding agent.The organic solvent is poly- second two
Alcohol, diethylene glycol (DEG), propylene glycol are with the mixed solvent that mass ratio is that 2:1:1 is mixed.The surfactant is glycols.The PH
Regulator is trimethylamine.
The preparation method of the reactive dye ink of above-mentioned digital inking printing, comprising the following steps:
Step 1, water hyacinth is pulverized into grinding, filtering residue obtains slurries, then by obtaining after membrane filtration 2 times of 1 μm
The water hyacinth clear liquid；
Step 2, active colorant is added in water hyacinth clear liquid and is stirred evenly, added the organic solvent, stir evenly,
Other substances of above-mentioned reactive dye ink are added later, is uniformly mixed, passes through 2 μm of membrane filtration；
Step 3, the filtered filtrate of step 2 is heated, is heated to 50-60 DEG C, is then cooled in 2-3min
15-20 DEG C, then removal of impurities, finished product are successively filtered by the filter membrane of 0.5 μm, 0.1 μm.
Embodiment 3
A kind of reactive dye ink of digital inking printing, including the following substance measured according to the mass fraction:
Wherein, after the water hyacinth clear liquid is by pulverizing water hyacinth, slurries are filtered to obtain, then pass through 0.5-1 μm of filter
Film obtains after filtering 2 times.The auxiliary agent includes defoaming agent, moisturizer, viscosity modifier and bleeding agent.The organic solvent is poly-
Ethylene glycol, diethylene glycol (DEG), propylene glycol are with the mixed solvent that mass ratio is that 2:1:1 is mixed.The surfactant is glycols or naphthalene
Sulphonic acids surfactant.The PH regulator is triethanolamine.
The preparation method of the reactive dye ink of above-mentioned digital inking printing, comprising the following steps:
Step 1, water hyacinth is pulverized into grinding, filtering residue obtains slurries, then by after membrane filtration 2 times of 0.5-1 μm
Obtain the water hyacinth clear liquid；
Step 2, active colorant is added in water hyacinth clear liquid and is stirred evenly, added the organic solvent, stir evenly,
Other substances of the reactive dye ink are added later, is uniformly mixed, passes through 2 μm of membrane filtration；
Step 3, the filtered filtrate of step 2 is heated, is heated to 50-60 DEG C, is then cooled in 2-3min
15-20 DEG C, then removal of impurities, finished product are successively filtered by the filter membrane of 0.5 μm, 0.1 μm.
Embodiment 1, embodiment 2 and embodiment 3 are tested, reactive dye ink stability all at 8 months or more, is knitted
The object surface treating agent shelf-life at 1 year or more, the ink-jet printed product color fastness of resistance to dry friction >=4 grade, moisture-proof colorfastness to rubbing >=3
Grade, color fastness to water (staining, discoloration) >=4 grades.
By above-mentioned specific embodiment, the beneficial effects of the present invention are: the present invention is that one kind is knitted suitable for protein fibre
The reactive dye ink of object and cellulose base fiber fabric, have it is bright in luster, dye-uptake is high, storage stability is good, is not susceptible to
Hydrolysis, printing fluency are good, the good advantage of using effect.The present invention uses the organic solvent of mixed type, can play collaboration and promote
Into effect, hydrophobic alkyl is contained in organic solvent, hydrogen bond can be formed with dyestuff in water, dye ions surface is made to form water
Ion protective layer is closed, dye molecule cohesion and intermolecular interaction is prevented, promotes the ionization and dissolution of dyestuff, increase it
Solvability, the addition of polyethylene glycol can significantly improve the solubility of dyestuff；And diethylene glycol (DEG) and propylene glycol cooperate, and can make dyestuff
Molecule forms micella in water, has preferable dispersibility, and can also make have polar dyestuff in the solvent point for constituting micella
At the netted solubilising of model between son, to form uniform apparent dissolution phenomena, dissolubility is improved；Water hyacinth clear liquid is added,
The permeability of ink is helped to improve, the dye-uptake of dyestuff can be effectively improved, while keeping color more bright-coloured, not fugitive color.
The foregoing description of the disclosed embodiments enables those skilled in the art to implement or use the present invention.
Various modifications to these embodiments will be readily apparent to those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, of the invention
It is not intended to be limited to the embodiments shown herein, and is to fit to and the principles and novel features disclosed herein phase one
The widest scope of cause.
Claims (7)
1. a kind of reactive dye ink of digital inking printing, which is characterized in that including the following substance measured according to the mass fraction:
2. the reactive dye ink of digital inking printing according to claim 1, which is characterized in that the water hyacinth clear liquid
After pulverizing water hyacinth, slurries are filtered to obtain, then by obtaining after membrane filtration 2 times of 0.5-1 μm.
3. the reactive dye ink of digital inking printing according to claim 2, which is characterized in that the auxiliary agent includes disappearing
Infusion, moisturizer, viscosity modifier and bleeding agent.
4. the reactive dye ink of digital inking printing according to claim 3, which is characterized in that the organic solvent is
Polyethylene glycol, diethylene glycol (DEG), propylene glycol are with the mixed solvent that mass ratio is that 2:1:1 is mixed.
5. the reactive dye ink of digital inking printing according to claim 3, which is characterized in that the surfactant
For glycols or naphthalene sulfonic acids class surfactant.
6. the reactive dye ink of digital inking printing according to claim 3, which is characterized in that the PH regulator is
One of trimethylamine, triethanolamine, ammonium hydroxide, sodium citrate, sodium bicarbonate.
7. a kind of preparation method of the reactive dye ink of digital inking printing described in claim 1, which is characterized in that including
Following steps:
Step 1, water hyacinth is pulverized into grinding, filtering residue obtains slurries, then by obtaining after membrane filtration 2 times of 0.5-1 μm
The water hyacinth clear liquid；
Step 2, active colorant is added in water hyacinth clear liquid and is stirred evenly, added the organic solvent, stir evenly, later
Other substances described in claim 1 are added, is uniformly mixed, passes through 2 μm of membrane filtration；
Step 3, the filtered filtrate of step 2 is heated, is heated to 50-60 DEG C, 15-20 is then cooled in 2-3min
DEG C, then removal of impurities, finished product are successively filtered by the filter membrane of 0.5 μm, 0.1 μm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810904298.7A CN109098014A (en) | 2018-08-09 | 2018-08-09 | A kind of reactive dye ink of digital inking printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810904298.7A CN109098014A (en) | 2018-08-09 | 2018-08-09 | A kind of reactive dye ink of digital inking printing and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109098014A true CN109098014A (en) | 2018-12-28 |
Family
ID=64849110
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810904298.7A Pending CN109098014A (en) | 2018-08-09 | 2018-08-09 | A kind of reactive dye ink of digital inking printing and preparation method thereof |
Country Status (1)
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| CN (1) | CN109098014A (en) |
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