CN102078280B - Micro emulsion toning lotion added with pearl hydrolysate liposome - Google Patents
Micro emulsion toning lotion added with pearl hydrolysate liposome Download PDFInfo
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- CN102078280B CN102078280B CN2010106235197A CN201010623519A CN102078280B CN 102078280 B CN102078280 B CN 102078280B CN 2010106235197 A CN2010106235197 A CN 2010106235197A CN 201010623519 A CN201010623519 A CN 201010623519A CN 102078280 B CN102078280 B CN 102078280B
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- deionized water
- pearl hydrolysate
- hydrolysate liposome
- butanediol
- glycine
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Abstract
The invention relates to a micro emulsion toning lotion added with pearl hydrolysate liposome, prepared by mixing and then carrying out high speed homogenizing on xanthan gum, butanediol, methylparaben, glycerol, pearl hydrolysate liposome, allantion, C20-22 phosphate/C20-22 fatty alcohol, 1-methyl hydantoin-2-imide, trimethyl glycine, triethanolamine, dicaprylyl carbonate, polydimethylsiloxane, phenoxyethanol, caprylylglycine, hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer, polyquaternium-51, essence and deionized water. The process in the invention is simple, the active ingredients and active substances in the pearl are effectively utilized, multiple active ingredients are organically combined, thus melanin can be lightened, skin colour can be brightened and moisture required by skin can be replenished, pores can be shrinked, grease secretion is balanced, and the effects of whitening and brightening the skin colour can be achieved.
Description
Technical field
The present invention relates to a kind of astringent, be specifically related to a kind of microemulsion astringent that adds the pearl hydrolysate liposome parcel.
Background technology
Margarita is used to improve looks has had history in several thousand; The trace element that it contains and each seed amino acid, for skin provides the guarantee of nourishing and whitening, and the main composition-calcium carbonate of Margarita powder and trace element are demulsifiers; Destroy the emulsification system of cosmetics; Reduce the stability of product, make that nutritional labeling adds in the cosmetics in the Margarita to receive, how add the nutritional labeling in the Margarita in the cosmetics and can better be absorbed purpose and the direction that has become present research than limitations.
Chinese patent " CN1795874A " discloses a kind of method for preparing pearl hydrolysate liposome; It is that Margarita hydrolyzed solution is dissolved in the phosphate buffer; Transfer pH value to neutral; Slowly join then in the bottle of processing by the soybean lecithin dry film, obtain pearl hydrolysate liposome through vibration, ultrasonic Treatment.The pearl hydrolysate liposome that is prepared by this method can reduce the conductivity of hydrolyzed solution; Minimizing can protect the effective ingredient of Margarita not destroyed by other components to the destruction of cosmetics series effectively, and several amino acids and trace element in the Margarita hydrolyzed solution fat can better be absorbed by the body; Promote the activity of the superoxide dismutase (SOD) in the human skin; Suppress melanic formation, keep skin pale, reach the beautifying whitening double effects.
The astringent shortcoming is that the effective ingredient that adds is restricted in the market, and moistening effect not contain a small amount of greasy astringent good, in astringent, adding pearl hydrolysate liposome is the difficult problem that present cosmetic industry needs to be resolved hurrily.
Summary of the invention
A kind of microemulsion astringent that adds the pearl hydrolysate liposome parcel that the objective of the invention is to be directed against the deficiency of prior art and provide; Be a kind ofly both can keep the skin wet for skin; Regulate skin ph value; And on skin, form one deck moisture film, can let again nutritional labeling in the Margarita hydrolyzed solution is more effective to be absorbed by skin, reach the effect of whitening, put forward the bright colour of skin.
The beauty treatment principle that the present invention adopts: according to the principle of similar compatibility, oils and fats is absorbed by the body than water more easily, in astringent, adds certain oils and fats and emulsifying agent, is made into microemulsion; Margarita hydrolyzed solution is wrapped up with the soybean lecithin film; Add to then in the microemulsion astringent that contains oils and fats and surfactant; Impel the nutritional labeling in the Margarita better to be absorbed by skin; Add the raw material of effects such as having pore refining, soften cuticle and whiten again, really reach acid-base scale of skin, promotion skin water oil balance, the effect of whitening and moisturizing regulated.
The technical scheme that the present invention adopted is:
A kind of microemulsion astringent that adds the pearl hydrolysate liposome parcel; Be to form microemulsion and process, wherein be respectively: xanthan gum 0.03～0.1%, butanediol 5～15%, methyl hydroxybenzoate 0.05～0.15%, glycerol 5～15%, pearl hydrolysate liposome 5～10%, allantoin 0.05～0.15%, C20-22 phosphate ester/C20-22 aliphatic alcohol 0.4～0.8%, 1-methyl hydantoin-2-acid imide 0.5～1.5%, trimethyl glycine 1～5%, triethanolamine 0.05～0.15%, carbonic acid dibutyl ester 1～5%, polydimethylsiloxane 1～3%, phenoxyethanol 0.4～0.8%, caprylyl glycine 1.0～2.0%, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers 0.5～1.5%, polyquaternary ammonium salt-510.5～2%, essence 0.02～0.05%, deionized water 37.8～78.5% according to each components contents of weight percent meter by xanthan gum, butanediol, methyl hydroxybenzoate, glycerol, pearl hydrolysate liposome, allantoin, C20-22 phosphate ester/C20-22 aliphatic alcohol, 1-methyl hydantoin-2-acid imide, trimethyl glycine, triethanolamine, carbonic acid dibutyl ester, polydimethylsiloxane, phenoxyethanol, caprylyl glycine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers, polyquaternary ammonium salt-51, essence and deionized water high speed homogenization after mixing.
A kind of method for preparing of above-mentioned microemulsion astringent, its concrete steps are following:
1, press formula ratio and xanthan gum, butanediol are mixed stir subsequent usely, the caprylyl glycine is subsequent use with the deionized water dissolving of an amount of sterilization, and 1-methyl hydantoin-2-acid imide is subsequent use with the deionized water dissolving of an amount of sterilization.
2, pressing formula ratio adds glycerol, residue deionized water, C20-22 phosphate ester/C20-22 aliphatic alcohol, methyl hydroxybenzoate, allantoin, trimethyl glycine, triethanolamine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers in the emulsifying pot; And the mixed liquor of xanthan gum and butanediol is added the emulsifying pot add and pine for to 75～85 ℃, be heated to 75～85 ℃ in carbonic acid dibutyl ester and the polydimethylsiloxane adding oil cauldron.
3, add phenoxyethanol before the emulsifying; High speed homogenization 5～8 minutes; Be cooled to 50～60 ℃ and add dissolved caprylyl glycine solution and 1-methyl hydantoin-2-imide solution; Add pearl hydrolysate liposome, polyquaternary ammonium salt-51, essence after temperature is reduced to 40～45 ℃, temperature is reduced to the room temperature discharging and is got finished product.
For understanding the result of use of this product, with the form of questionnaire survey this product has been carried out investigation on probation widely in China, men and women's property trier 100 people in all parts of the country are included in this investigation altogether in; Male 12 people wherein; Women 88 people, the oldest 41 years old, minimum 18 years old; About 24 years old mean age, regain 94 parts of effective questionnaires altogether.
94 triers use 4 week of the disposable facial film back of interpolation pearl hydrolysate liposome following to the result of each item index improvement degree self evaluation:
Moistening effect has 17% and 75% trier to have moderate to improve and obviously improve respectively;
The moisturizing effect has 30.1% and 68% trier to have moderate to improve and obviously improve respectively;
Putting forward bright colour of skin effect has 53.8% and 40.5% trier to have moderate to improve and obviously improve respectively;
The Sage Extract effect has 42.8% and 48.5% trier to have moderate to improve and obviously improve respectively;
Can find out from the result of trier's self assessment, this product to the preserving moisture of skin, moisturizing, put forward the bright colour of skin and all there is improvement in various degree the Sage Extract aspect.
Show according to survey result: the microemulsion cosmetic glassware for drinking water of this interpolation pearl hydrolysate liposome parcel has maintenance effect preferably.
Technology of the present invention is simple; Effectively utilize effective ingredient and active substance in the Margarita, plurality of active ingredients is organically combined, not only can desalinate melanin, put forward the bright colour of skin; Replenish the required moisture of skin; And can pore refining, Bergamot Mint Extract reaches the effect of whitening, put forward the bright colour of skin.
The specific embodiment
With non-limiting examples the present invention is further specified below.
Embodiment one,
Xanthan gum 0.05kg; Butanediol 5kg; Methyl hydroxybenzoate 0.10kg; Glycerol 8kg; Pearl hydrolysate liposome 5kg; Allantoin 0.1kg; C20-22 phosphate ester/C20-22 aliphatic alcohol 0.5kg; 1-methyl hydantoin-2-acid imide 0.5kg; Trimethyl glycine 2kg; Triethanolamine 0.10kg; Carbonic acid dibutyl ester 2kg; Polydimethylsiloxane 2kg; Phenoxyethanol 0.5kg; Caprylyl glycine 1.0kg; Hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers 0.5kg; Polyquaternary ammonium salt-510.5kg; Essence 0.03kg; Deionized water 72.12kg.
1, xanthan gum, butanediol are mixed stir subsequent usely, the caprylyl glycine is subsequent use with the deionized water dissolving of an amount of sterilization, and 1-methyl hydantoin-2-acid imide is subsequent use with the deionized water dissolving of an amount of sterilization.
2, glycerol, residue deionized water, C20-22 phosphate ester/C20-22 aliphatic alcohol, methyl hydroxybenzoate, allantoin, trimethyl glycine, triethanolamine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers are added in the emulsifying pot; And the mixed liquor of xanthan gum and butanediol is added the emulsifying pot add and pine for to 75 ℃, be heated to 75 ℃ in carbonic acid dibutyl ester and the polydimethylsiloxane adding oil cauldron.
3, add phenoxyethanol before the emulsifying, high speed homogenization 5 minutes is cooled to 50 ℃ and adds dissolved caprylyl glycine solution and 1-methyl hydantoin-2-imide solution, adds pearl hydrolysate liposome, polyquaternary ammonium salt-51, essence after temperature is reduced to 40 ℃.Temperature is reduced to the room temperature discharging and is got finished product.
Embodiment two,
Xanthan gum 1.0kg; Butanediol 150kg; Methyl hydroxybenzoate 1.5kg; Glycerol 150kg; Pearl hydrolysate liposome 100kg; Allantoin 1.5kg; C20-22 phosphate ester/C20-22 aliphatic alcohol 8.0kg; 1-methyl hydantoin-2-acid imide 15kg; Trimethyl glycine 50kg; Triethanolamine 1.5kg; Carbonic acid dibutyl ester 50kg; Polydimethylsiloxane 30kg; Phenoxyethanol 8kg; Caprylyl glycine 20kg; Hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers 15kg; Polyquaternary ammonium salt-51 20kg; Essence 0.5kg; Deionized water 378kg.
1, xanthan gum, butanediol are mixed stir subsequent usely, the caprylyl glycine is subsequent use with the deionized water dissolving of an amount of sterilization, and 1-methyl hydantoin-2-acid imide is subsequent use with the deionized water dissolving of an amount of sterilization.
2, glycerol, residue deionized water, C20-22 phosphate ester/C20-22 aliphatic alcohol, methyl hydroxybenzoate, allantoin, trimethyl glycine, triethanolamine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers are added in the emulsifying pot; And the mixed liquor of xanthan gum and butanediol is added the emulsifying pot add and pine for to 85 ℃, be heated to 85 ℃ in carbonic acid dibutyl ester and the polydimethylsiloxane adding oil cauldron.
3, add phenoxyethanol before the emulsifying, high speed homogenization 8 minutes is cooled to 55 ℃ and adds dissolved caprylyl glycine solution and 1-methyl hydantoin-2-imide solution, adds pearl hydrolysate liposome, polyquaternary ammonium salt-51, essence after temperature is reduced to 45 ℃.Temperature is reduced to the room temperature discharging and is got finished product.
Claims (2)
1. one kind is added the microemulsion astringent that pearl hydrolysate liposome wraps up; It is characterized in that forming microemulsion and processing, wherein be respectively: xanthan gum 0.03～0.1%, butanediol 5～15%, methyl hydroxybenzoate 0.05～0.15%, glycerol 5～15%, pearl hydrolysate liposome 5～10%, allantoin 0.05～0.15%, C20-22 phosphate ester/C20-22 aliphatic alcohol 0.4～0.8%, 1-methyl hydantoin-2-acid imide 0.5～1.5%, trimethyl glycine 1～5%, triethanolamine 0.05～0.15%, carbonic acid dibutyl ester 1～5%, polydimethylsiloxane 1～3%, phenoxyethanol 0.4～0.8%, caprylyl glycine 1.0～2.0%, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers 0.5～1.5%, polyquaternary ammonium salt-51 0.5～2%, essence 0.02～0.05%, deionized water 37.8～78.5% according to each components contents of weight percent meter by xanthan gum, butanediol, methyl hydroxybenzoate, glycerol, pearl hydrolysate liposome, allantoin, C20-22 phosphate ester/C20-22 aliphatic alcohol, 1-methyl hydantoin-2-acid imide, trimethyl glycine, triethanolamine, carbonic acid dibutyl ester, polydimethylsiloxane, phenoxyethanol, caprylyl glycine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers, polyquaternary ammonium salt-51, essence and deionized water high speed homogenization after mixing.
2. the method for preparing of the described microemulsion astringent of claim 1 is characterized in that, its concrete steps are following:
1), press formula ratio and xanthan gum, butanediol are mixed stir subsequent usely, the caprylyl glycine is subsequent use with the deionized water dissolving of an amount of sterilization, 1-methyl hydantoin-2-acid imide is subsequent use with the deionized water dissolving of an amount of sterilization;
2), pressing formula ratio adds glycerol, residue deionized water, C20-22 phosphate ester/C20-22 aliphatic alcohol, methyl hydroxybenzoate, allantoin, trimethyl glycine, triethanolamine, hydroxy ethyl methacrylate/sodium acryloyldimethyl taurate copolymers in the emulsifying pot; And be heated to 75～85 ℃ in the mixed liquor adding emulsifying pot with xanthan gum and butanediol, be heated to 75～85 ℃ in carbonic acid dibutyl ester and the polydimethylsiloxane adding oil cauldron;
3), add phenoxyethanol before the emulsifying; High speed homogenization 5～8 minutes; Be cooled to 50～60 ℃ and add dissolved caprylyl glycine solution and 1-methyl hydantoin-2-imide solution; Add pearl hydrolysate liposome, polyquaternary ammonium salt-51, essence after temperature is reduced to 40～45 ℃, temperature is reduced to the room temperature discharging and is got finished product.
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| CN106983714A (en) * | 2017-05-05 | 2017-07-28 | 海南京润珍珠生物技术股份有限公司 | Naked adornment eye essence dew of pearl and preparation method thereof |
| WO2018145827A1 (en) * | 2017-02-08 | 2018-08-16 | Unilever Plc | Xanthan structured high polyol liquid cleansers |
| US12023395B2 (en) | 2017-02-08 | 2024-07-02 | Conopco, Inc. | Xanthan structured high polyol liquid cleansers |
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| WO2018145827A1 (en) * | 2017-02-08 | 2018-08-16 | Unilever Plc | Xanthan structured high polyol liquid cleansers |
| US12023395B2 (en) | 2017-02-08 | 2024-07-02 | Conopco, Inc. | Xanthan structured high polyol liquid cleansers |
| CN106983714A (en) * | 2017-05-05 | 2017-07-28 | 海南京润珍珠生物技术股份有限公司 | Naked adornment eye essence dew of pearl and preparation method thereof |
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Denomination of invention: Micro emulsion toning lotion added with pearl hydrolysate liposome Effective date of registration: 20160518 Granted publication date: 20120704 Pledgee: Haikou rural commercial bank Limited by Share Ltd Pledgor: Hainan Jingrun Zhenzhu Biological Technology Co., Ltd. Registration number: 2016460000001 |
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Date of cancellation: 20200831 Granted publication date: 20120704 Pledgee: Haikou rural commercial bank Limited by Share Ltd. Pledgor: HAINAN JINGRUN PEARL BIOTECHNOLOGY Co.,Ltd. Registration number: 2016460000001 |