CN102042978B - 快速判定大黄等级的比色卡及其制备方法 - Google Patents
快速判定大黄等级的比色卡及其制备方法 Download PDFInfo
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样 品 | 产地 | 规格 | 等 级 | 芦荟大黄 素(mg/g) | 大黄酸 (mg/g) | 大黄素 (mg/g) | 大黄酚 (mg/g) | 大黄素甲 醚(mg/g) | 含量总和 (mg/g) |
D1 | 甘肃 礼县 | 出口八 成吉 | 一 等 | 4.41 | 14.58 | 2.91 | 6.99 | 1.71 | 30.60 |
D2 | 甘肃 礼县 | 出口八 成小吉 | 二 等 | 3.94 | 8.46 | 3.35 | 9.93 | 6.04 | 31.73 |
D3 | 甘肃 礼县 | 出口七 成片 | 二 等 | 4.11 | 21.08 | 3.58 | 6.10 | 3.62 | 38.50 |
D4 | 甘肃 礼县 | 蛋吉 | 二 等 | 4.32 | 14.11 | 4.34 | 8.91 | 5.63 | 37.30 |
D5 | 甘肃 礼县 | 苏吉 | 三 等 | 1.80 | 5.33 | 1.71 | 3.81 | 2.06 | 14.71 |
D6 | 甘肃 礼县 | 出口统 货 | 一 等 | 4.57 | 13.14 | 3.40 | 13.47 | 5.54 | 40.13 |
D7 | 甘肃 礼县 | 统水根 | 二 等 | 4.54 | 14.72 | 3.34 | 13.32 | 5.45 | 41.37 |
D8 | 云南 大理 | 大黄片 吉 | 二 等 | 3.07 | 12.15 | 4.81 | 7.18 | 3.94 | 31.15 |
D9 | 云南 大理 | 马蹄大 黄 | 三 等 | 3.19 | 6.93 | 3.48 | 5.16 | 3.44 | 22.20 |
D10 | 云南 大理 | 水根 | 三 等 | 3.98 | 10.79 | 1.98 | 3.77 | 2.33 | 22.84 |
D11 | 甘肃 | 原大黄 统货 | 三 等 | 3.50 | 10.66 | 4.68 | 9.61 | 4.59 | 33.03 |
D12 | 青海 | 原大黄 统货 | 一 等 | 4.36 | 29.84 | 2.35 | 5.10 | 1.98 | 43.64 |
D13 | 青海 西宁 | 原大黄 统货 | 二 等 | 6.57 | 2.63 | 3.39 | 15.80 | 7.64 | 36.04 |
D14 | 重庆 奉节 | 马蹄黄 | 三 等 | 3.41 | 3.82 | 1.27 | 7.00 | 3.51 | 19.00 |
D15 | 青海 西宁 | 统货 | 一 等 | 6.32 | 2.63 | 4.65 | 18.43 | 9.76 | 41.79 |
D16 | 甘肃 | 饮片 | 三 等 | 2.15 | 8.37 | 2.05 | 6.70 | 1.58 | 20.85 |
D17 | 山西 | 原大黄 统货 | 二 等 | 3.18 | 1.39 | 2.26 | 15.81 | 7.11 | 29.76 |
D18 | 甘肃 | 野生水 根黄 | 三 等 | 1.69 | 5.21 | 1.68 | 5.58 | 1.44 | 15.61 |
D19 | 藏江 达 | 野生去 皮统货 | 一 等 | 5.55 | 33.48 | 2.97 | 8.55 | 2.52 | 53.07 |
D20 | 石柒 | 野生统 货 | 一 等 | 3.01 | 30.65 | 1.66 | 4.78 | 1.12 | 41.23 |
D21 | 川西 塞达 | 野生统 货 | 一 等 | 2.94 | 32.37 | 1.99 | 4.51 | 1.27 | 43.09 |
D22 | 西藏 昌都 | 家种统 货 | 一 等 | 5.63 | 11.63 | 5.01 | 11.15 | 6.12 | 39.53 |
D23 | 甘肃 | 家种统 货 | 二 等 | 3.11 | 3.04 | 2.01 | 12.77 | 5.75 | 26.66 |
D24 | 西藏 | 家种统 货 | 二 等 | 3.48 | 9.65 | 2.48 | 8.68 | 3.36 | 27.65 |
D25 | 北川 | 野生统 货 | 二 等 | 5.71 | 9.30 | 2.27 | 11.52 | 4.91 | 33.71 |
D26 | 凉山 州得 卑 | 野生统 货 | 二 等 | 4.92 | 20.12 | 2.54 | 5.19 | 4.13 | 36.89 |
D27 | 贵州 | 野生统 货 | 三 等 | 2.55 | 13.45 | 2.55 | 3.36 | 2.02 | 23.94 |
D28 | 四川 | 野生统 | 一 | 4.40 | 20.45 | 5.38 | 7.39 | 1.13 | 38.75 |
雅安 | 货 | 等 | |||||||
D29 | 西藏 昌都 | 饮片 | 二 等 | 3.53 | 15.02 | 2.09 | 4.19 | 1.55 | 26.37 |
D30 | 甘肃 | 饮片 | 三 等 | 2.39 | 1.71 | 2.10 | 11.45 | 6.48 | 24.12 |
D31 | 青海 | 饮片 | 一 等 | 4.00 | 31.62 | 2.24 | 5.32 | 1.96 | 45.14 |
D32 | 四川 | 饮片 | 二 等 | 4.03 | 12.61 | 3.03 | 8.48 | 5.04 | 33.20 |
D33 | 甘肃 | 饮片 | 三 等 | 1.66 | 1.01 | 1.86 | 11.90 | 6.72 | 23.14 |
D34 | 青海 | 饮片 | 三 等 | 1.92 | 4.56 | 1.66 | 6.26 | 1.81 | 16.20 |
表面 颜色 | 粉末 颜色 | 粉末显色 后颜色 | 断面 颜色 | 断面显色后颜色 | ||
一等 | R | 104~176 | 120~195 | 128~203 | 104~165 | 65~165 |
G | 82~141 | 86~148 | 58~163 | 78~164 | 34~80 | |
B | 22~49 | 18~38 | 26~55 | 31~135 | 226~47 | |
二等 | R | 93~159 | 111~175 | 173~233 | 124~165 | 107~157 |
G | 65~160 | 88~135 | 74~159 | 110~154 | 42~67 | |
B | 26~56 | 20~33 | 31~46 | 42~116 | 31~44 | |
三等 | R | 80~127 | 103~150 | 180~233 | 108~202 | 64~198 |
G | 70~95 | 76~113 | 83~170 | 100~181 | 42~79 | |
B | 28~53 | 17~36 | 41~87 | 42~112 | 31~43 |
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CN102879394B (zh) * | 2012-10-08 | 2015-01-21 | 成都中医药大学 | 一种正品大黄种子的快速检测方法 |
CN106353469B (zh) * | 2015-07-14 | 2018-12-14 | 中国人民解放军第三〇二医院 | 一种中药品质的综合评价方法 |
CN106611428A (zh) * | 2015-10-21 | 2017-05-03 | 中国人民解放军第三〇二医院 | 一种快速判断北五味子的质量等级的判别卡及其制备方法和应用 |
CN107144531A (zh) * | 2017-04-19 | 2017-09-08 | 黄建国 | 一种基于颜色数据分析的物质含量检测方法、系统及装置 |
CN109682798A (zh) * | 2018-12-07 | 2019-04-26 | 亳州学院 | 一种用于中药饮片的智能显色鉴别装置及鉴别方法 |
CN113933293A (zh) * | 2021-11-08 | 2022-01-14 | 中国联合网络通信集团有限公司 | 浓度检测方法及装置 |
CN114199786B (zh) * | 2021-11-19 | 2023-10-03 | 湖北中医药大学 | 一种盐炙杜仲质量控制方法 |
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CN102042984A (zh) * | 2009-10-19 | 2011-05-04 | 中国人民解放军第三〇二医院 | 药材等级评价方法及系统 |
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CN101799329A (zh) * | 2010-03-04 | 2010-08-11 | 江西中医学院 | 一种检测中药饮片外观色泽的方法 |
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