CN102031075A - Environmentally-friendly energy-saving cigarette adhesive and production method thereof - Google Patents
Environmentally-friendly energy-saving cigarette adhesive and production method thereof Download PDFInfo
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- CN102031075A CN102031075A CN2009100950450A CN200910095045A CN102031075A CN 102031075 A CN102031075 A CN 102031075A CN 2009100950450 A CN2009100950450 A CN 2009100950450A CN 200910095045 A CN200910095045 A CN 200910095045A CN 102031075 A CN102031075 A CN 102031075A
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Abstract
The invention discloses an environmentally-friendly energy-saving cigarette adhesive, which comprises 20 to 33 percent of base material, 65 to 78 percent of water-soluble vinyl acetate elastomer (VAE) series raw materials for preparing the cigarette adhesive according to the adhesive kind needed by the cigarette adhesive and the base material, and 0.001 to 0.008 percent of antifoaming agent, 0.007 to 0.02 percent of plasticizer and 0.005 to 0.05 percent of edible ethanol in an adhesive-making process, wherein the base material is prepared by the following steps of: adding high-purity polyvinyl chloride (PVC) and deionized water according to a ratio of the water to the PVC of 4:1 into a reaction kettle, and raising the temperature to 95 DEG C for dissolving; and adding 25 to 60 weight percent of selected VAE emulsion based on the prepared product, and sealing the reaction kettle to prepare the base material. The cigarette adhesive is prepared by dripping the antifoaming agent, the plasticizer, the edible ethanol and solution of sodium carbonate and sealing the reaction kettle. Therefore, the liquidity, adhesiveness, cohesion, freezing resistance and corrosion resistance of the adhesive are improved.
Description
Technical field
The invention belongs to a kind of environmental protection and energy saving cigarette glue and production method thereof.
Background technology
Cigarette glue is the tackiness agent that uses in the production of cigarettes, and along with the development of cigarette machine technology, cigarette machine speed brings up to 8000 by 6000 of original per minutes---16000 cigarette speed.The cigarette glue that the original synthesis process technology is produced is difficult to adapt to the bonding requirement of high-speed cigarette machine to cigarette, and the production time is long, power consumption is high.Along with the raising of environmental requirement, also more and more stricter to the requirement of the harmful substance contents in the glue.Need to use the cigarette glue that does not contain oxious components such as benzene, lead, arsenic.Thereby, have the new demand that cigarette glue product energy-conservation in high speed cohesiveness, environmental protection and the production has become cigarette industry.
Summary of the invention
Purpose of the present invention discloses exactly and a kind ofly can adapt to high speed cigarette bonding, environmental protection, energy-conservation and simple environmental protection and energy saving cigarette glue of technology and production method thereof.
The environmental protection and energy saving cigarette glue, comprise base-material, be deployed into defoamer, softening agent, the edible ethanol of using in the water-soluble VAE series raw material of cigarette glue and the adhesive-preparing technology by required glue kind of cigarette glue and base-material, the base-material that comprises 20-33% in the constituent, VAE 65-78%, defoamer: 0.001-0.008%, softening agent: 0.007-0.02%, edible ethanol: 0.005-0.05%.Wherein base-material is by high purity PVC and deionized water, and by water: PVC=4: 1 goes into reactor, dissolves under temperature rise to the 95 ℃ condition, again by the 25-60% of formulated product weight, adds selected VAE emulsion, sealed reactor and makes.According to the overlapping glue in the cigarette working procedure, connecing mouth glue, center line glue, capsule packing glue, barrel packing colloidality can requirement, the amount of getting is sealed in the cigarette glue that makes above-mentioned application target requirement in the reactor in proportion.Improved glue flowability, binding property, hold viscosity, frost resistance and antiseptic property.
The production method of environmental protection and energy saving cigarette glue:
Method one, the production method of environmental protection and energy saving cigarette glue, comprise that base-material is made and the preparation of glue kind, the base-material blending process is to select Sweet natural gas synthetic high purity PVC and deionized water, by water: PVC=4: 1 goes into reactor, through soaking, the still skin adds the steam rising temperature for dissolving, dissolve under temperature rise to the 95 ℃ condition, in still, press the speed that per minute 10-50 rises, by the gelatigenous kind of giving birth to, 25-60% by formulated product weight, add selected VAE emulsion, and the speed titration 0.001-0.008% defoamer that rises with per minute 0.1-1, the 0.007-0.02% softening agent, the 0.005-0.05% edible ethanol, sealed reactor, extract residual monomer ethanol, ethene is cooled to normal temperature, and strainer filtering and detection obtain base-material.
Press the solids content of the cigarette glue of required kind, viscosity, the pH value requirement, select the water-soluble VAE705 of nontoxic compliance with environmental protection requirements, VAE707, the VAE-I type, the VAE-II type, 149, in 8265 raw materials two to three kinds, with above-mentioned synthetic base-material, by the technical requirements of required glue kind, in gross weight, get base-material 20-33%, VAE65-78%, add again by product weight, edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5%, these auxiliary material total amounts are not more than 2%, transfer pH value 4-6, with conventional dispensing mode, be deployed into the cigarette glue of various performance requriementss by the kind technical requirements of required glue.
Press such scheme, get base-material be no less than 25% with any 2 to 3 kinds that are not more than in 73% the VAE series raw material, adding is not more than 2% edible ethanol, defoamer, softening agent, yellow soda ash, transfers pH value 4-6 can be mixed with the cigarette glue that is fit to various performance requriementss.
Method 2, be the PVC lysate of 10-30% with solids content, with in water-soluble VAE705, VAE707, VAE-I type, VAE-II type, 149, the raw materials such as 8265 two to three kinds, press restatement with PVC lysate 10-23%, VAE75-88%, add again by product weight, edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5%, these auxiliary material total amounts are not more than 2%, transfer pH value 4-6, directly be deployed into the cigarette glue of various performance requriementss by the kind technical requirements of required glue.
This Technology has changed original synthesis technique, cancelled and used vinyl acetate between to for plastic to add the reaction process of raw materials such as ammonium persulphate and OP-10 in the former technology, reduced objectionable impurities, all used nontoxic PVC and VAE series emulsion, calculated to prepare 1000 kilograms of cigarette glues, old explained hereafter needs 12 hours, novel process only needs 5 hours, makes that technology is simple, constant product quality, and it is bonding to adapt to high speed, save energy consumptions such as water, electricity, gas, bonding, environmental protection, energy-saving effect are remarkable.
Embodiment
1, the environmental protection and energy saving cigarette glue is selected Sweet natural gas synthetic high purity polyethylene alcohol (PVC) for use, use earlier deionized water, and by water: PVC=4: 1 goes into reactor soaks and is no less than 4 hours, in still skin adding steam rising temperature for dissolving gradually.Temperature rises to dissolves after 1 hour under 95 ℃ of conditions, press the speed that per minute 10-50 rises, the VAE emulsion that in still, slowly adds formulated product weight 25-60%, cancel the amount of infusion 0.001-0.008%, softening agent 0.007-0.02%, edible ethanol 0.5-5% by weight proportion, the flow titration that rises with per minute 0.1-1 adds in the still; Sealed reactor extracts residual ethanol, vinyl monomer 1 hour, is cooled to 20-28 ℃, filters with the 160-200 mesh filter screen, detects viscosity, solids content is standby as base-material.
2, press dry powder weight, the technical requirementss such as viscosity 80-6500mpa.s, pH value 4-6 of the solid content solids content 25-55% of required cigarette glue, by 100 kilograms of glue of preparation, get 73 kilograms of water-soluble VAE705, VAE707, VAE-I type, VAE-II type, 149, any two to three kinds of raw materials in the raw materials such as 8265 and 25 kilograms of step 1 synthetic base-materials of nontoxic compliance with environmental protection requirements, add 2 kilograms of defoamer, softening agent, edible ethanol and yellow soda ash sums.By 100 kilograms of glue amounts, wherein edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5% transfer pH value 4-6.Be mixed with high tack, high workability by the overlapping glue that uses in the cigarette process, the technological standard and the performance requriements that connect mouth glue, center line glue, packing glue, the machine speed that adapts to high speed cigarette is that 8000-16000 props up/cigarette glue of minute mentioned kind that bonding is good.
The same technology, the parts by weights meter, according to VAE: base-material, get 75 kilograms respectively: 23 kilograms, 70 kilograms: 28 kilograms, 71 kilograms: 27 kilograms, 68 kilograms: 30 kilograms, 65 kilograms: 33 kilograms, press overall control again at 2 kilograms, add edible ethanol defoamer, softening agent, yellow soda ash.Transfer pH value 4-6, be deployed into the cigarette glue of various performance requriementss by the kind technical requirements of required glue.
3, with solids content be the PVC lysate of 10-30%, with in water-soluble VAE705, VAE 707, VAE-I type, VAE-II type, 149, the raw materials such as 8265 two to three kinds, by 100 kilograms of glue of preparation, get 15 kilograms of PVC lysates, 83 kilograms of VAE, add again by product weight, edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5%, these auxiliary material total amounts are not more than 2 kilograms, transfer pH value 4-6, directly the kind technical requirements by required glue is deployed into cigarette glue.
With above-mentioned identical technology, to prepare 100 kilograms, according to PVC: VAE, get the PVC and the VAE of 12: 86,18: 70,20: 78,11: 87,23: 75 kilogram numbers respectively, adding edible ethanol, defoamer, softening agent, yellow soda ash are made auxiliary material, total amount is not more than 2 kilograms, transfers pH value 4-6, is deployed into desired cigarette glue.
Claims (5)
1. environmental protection and energy saving cigarette glue, it is characterized in that comprising base-material, be deployed into defoamer, softening agent, the edible ethanol of using in the water-soluble VAE series raw material of cigarette glue and the adhesive-preparing technology by required glue kind of cigarette glue and base-material, the base-material that comprises 20-33% in the constituent, VAE 65-78%, defoamer: 0.001-0.008%, softening agent: 0.007-0.02%, edible ethanol: 0.005-0.05%.Wherein base-material is by high purity PVC and deionized water, and by water: PVC=4: 1 goes into reactor, dissolves under temperature rise to the 95 ℃ condition, again by the 25-60% of formulated product weight, adds selected VAE emulsion, sealed reactor and makes.
2. the production method of environmental protection and energy saving cigarette glue, comprise that base-material is made and the preparation of glue kind, it is characterized in that: the base-material blending process is to select Sweet natural gas synthetic high purity PVC and deionized water, by water: PVC=4: 1 goes into reactor, through soaking, the still skin adds the steam rising temperature for dissolving, dissolve under temperature rise to the 95 ℃ condition, in still, press the speed that per minute 10-50 rises, by the gelatigenous kind of giving birth to, 25-60% by formulated product weight, add selected VAE emulsion, and the speed titration 0.001-0.008% defoamer that rises with per minute 0.1-1, the 0.007-0.02% softening agent, the 0.005-0.05% edible ethanol, sealed reactor, extract residual monomer ethanol, ethene is cooled to normal temperature, and strainer filtering and detection obtain base-material.
3. the production method of environmental protection and energy saving cigarette glue according to claim 2, it is characterized in that solids content by the cigarette glue of required kind, viscosity, the pH value requirement, select the water-soluble VAE705 of nontoxic compliance with environmental protection requirements, VAE707, the VAE-I type, the VAE-II type, 149, in 8265 raw materials two to three kinds, with above-mentioned synthetic base-material, by the technical requirements of required glue kind, in gross weight, get base-material 20-33%, VAE65-78%, add again by product weight, edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5%, these auxiliary material total amounts are not more than 2%, transfer pH value 4-6,, be deployed into the cigarette glue of various performance requriementss by the kind technical requirements of required glue with conventional dispensing mode.
4. according to the production method of claim 2 or 3 described environmental protection and energy saving cigarette glues, it is characterized in that percentage meter by weight, get base-material be not more than 33% with any 2 to 3 kinds that are not more than in 78% the VAE series raw material, add total amount and be not more than 2% edible ethanol, defoamer, softening agent, yellow soda ash, transfer pH value 4-6, can be mixed with the cigarette glue that is fit to various performance requriementss.
5. the production method of environmental protection and energy saving cigarette glue according to claim 2, it is characterized in that with solids content being the PVC lysate of 10-30%, with water-soluble VAE705, VAE 707, the VAE-I type, the VAE-II type, 149, in 8265 raw materials such as grade two to three kinds, press restatement, get PVC lysate 10-23%, VAE 75-88%, add again by product weight, edible ethanol 0.005-0.05%, defoamer 0.001-0.008%, softening agent 0.007-0.02%, yellow soda ash 0.5-1.5%, these auxiliary material total amounts are not more than 2%, transfer pH value 4-6, directly be deployed into the cigarette glue of various performance requriementss by the kind technical requirements of required glue.
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| CN 200910095045 CN102031075B (en) | 2009-09-27 | 2009-09-27 | Environmentally-friendly energy-saving cigarette adhesive and production method thereof |
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| CN 200910095045 CN102031075B (en) | 2009-09-27 | 2009-09-27 | Environmentally-friendly energy-saving cigarette adhesive and production method thereof |
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Cited By (10)
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| CN102965056A (en) * | 2012-10-31 | 2013-03-13 | 刘斐 | Water-based adhesive and preparation method thereof |
| CN103059777A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Frost-resisting environment-friendly lap adhesive used for high-speed cigarette making machine and preparation method thereof |
| CN103059779A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Environment-friendly type lap joint port glue used for high speed cigarette making machine and preparation method thereof |
| CN103059778A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Cigarette environment-friendly high-speed packaging glue and preparation method thereof |
| CN103059774A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Waterproof environment-friendly cigarette plug molding glue and preparing method thereof |
| CN103773273A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive based on esterified gelatinized starch and non-gelatinized starch |
| CN108893084A (en) * | 2018-06-21 | 2018-11-27 | 江苏光辉粘合科技有限公司 | 399B low softening point hot melt adhesive |
| CN108913060A (en) * | 2018-06-21 | 2018-11-30 | 江苏光辉粘合科技有限公司 | Ramuscule is sprayed glue |
| CN109294488A (en) * | 2018-09-19 | 2019-02-01 | 湖北恒远化工有限公司 | A kind of cigarette radium-shine packs glue and preparation method thereof with water base |
| CN113416507A (en) * | 2021-07-14 | 2021-09-21 | 湖北恒阳科技发展有限公司 | Ultrahigh-speed nozzle connecting glue and preparation method thereof |
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| CN105567133B (en) * | 2016-01-13 | 2018-10-30 | 华威粘结材料（上海）股份有限公司 | A kind of ultrahigh speed cigarette connects mouth glue and preparation method thereof |
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| CN1033332C (en) * | 1992-07-29 | 1996-11-20 | 李有才 | Preparation method for cigarette glue |
| CN1159472A (en) * | 1996-12-20 | 1997-09-17 | 田素军 | Special glue for lamination of aluminium foil |
| US6568399B1 (en) * | 1999-04-26 | 2003-05-27 | National Starch And Chemical Investment Holding Corporation | Low application temperature hot melt adhesive for cigarette preparation |
| CN1163533C (en) * | 2000-12-27 | 2004-08-25 | 中国科学院长春应用化学研究所 | Process for preparing high-ethylene ethylene vinylacetate latex |
| CN1635042A (en) * | 2003-12-30 | 2005-07-06 | 陈晓光 | Process of preparing adhesive for building materials |
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| CN103773273A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive based on esterified gelatinized starch and non-gelatinized starch |
| CN103773273B (en) * | 2012-10-20 | 2016-02-24 | 中国烟草总公司郑州烟草研究院 | A kind of based on esterification class-pasted starch and the amyloid starchiness cigarette glue of non-gelatinization |
| CN102965056A (en) * | 2012-10-31 | 2013-03-13 | 刘斐 | Water-based adhesive and preparation method thereof |
| CN102965056B (en) * | 2012-10-31 | 2014-12-03 | 刘斐 | Water-based adhesive and preparation method thereof |
| CN103059777A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Frost-resisting environment-friendly lap adhesive used for high-speed cigarette making machine and preparation method thereof |
| CN103059779A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Environment-friendly type lap joint port glue used for high speed cigarette making machine and preparation method thereof |
| CN103059778A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Cigarette environment-friendly high-speed packaging glue and preparation method thereof |
| CN103059774A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Waterproof environment-friendly cigarette plug molding glue and preparing method thereof |
| CN108893084A (en) * | 2018-06-21 | 2018-11-27 | 江苏光辉粘合科技有限公司 | 399B low softening point hot melt adhesive |
| CN108913060A (en) * | 2018-06-21 | 2018-11-30 | 江苏光辉粘合科技有限公司 | Ramuscule is sprayed glue |
| CN109294488A (en) * | 2018-09-19 | 2019-02-01 | 湖北恒远化工有限公司 | A kind of cigarette radium-shine packs glue and preparation method thereof with water base |
| CN113416507A (en) * | 2021-07-14 | 2021-09-21 | 湖北恒阳科技发展有限公司 | Ultrahigh-speed nozzle connecting glue and preparation method thereof |
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