CN102021106B - Traditional Chinese medicine health wine and production technology thereof - Google Patents
Traditional Chinese medicine health wine and production technology thereof Download PDFInfo
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Abstract
The invention discloses a traditional Chinese medicine health wine and a production technology thereof. The traditional Chinese medicine health wine is prepared in the following steps: selecting ten traditional Chinese medicines of cinnamon, cistanche, Astragalus mongholicus, Chinese yam rhizome, medlar and the like; after processing, extracting single medicine of each medicine by taking ethanol as extraction solvent to obtain the extract of each medicine; respectively processing the extract of each medicine by a centrifugal machine, a microfiltration membrane, an ultrafiltration membrane and a nanofiltration membrane; after detecting the content of the effective ingredients, blending with a base wine quantificationally to cause the effective ingredients in each medicine to reach stipulated content; and then toning, blending flavour and ageing. In the invention, the traditional Chinese medicine health wine is quantificationally blended according to the effective ingredients in each medicine, so that product quality is easy to control, and prepared traditional Chinese medicine health wine has good clarity and stability. The active ingredients of the traditional Chinese medicines are easy to control. The invention is simple to operate, saves energy, lowers consumption, and provides a new thought for health wine production.
Description
(1) technical field: the present invention relates to a kind of Chinese medicine health-care wine and production technique thereof.
(2) background technology: health promoting wine is meant that with liquor, fermented wine or edible ethanol be the wine base, as being perfume, being flavor, present-color material, by what certain production technique processed human body is had the alcoholic drink of nourishing function with edible plant-animal, foodstuff additive.It is applicable to that specific crowd is edible, and the adjusting body function is arranged.Along with improving constantly of concept of health, the human consumer is increasing to the demand of health promoting wine.Gliding though present domestic wine industry is whole, but is a dark horse in health promoting wine market, just with annual 30% rate of increase high speed development; Following market potential is very big; By 2010, the health promoting wine market capacity will reach more than 13,000,000,000, be main with Chinese medicine health-care wine again wherein.
The working method of existing Chinese medicine health-care wine mainly is to mix back infiltration, seepage extraction to Chinese medicinal materials, does the filtration clarifying treatment after ageing for some time again.Though this working method technology is simple, because multiple medicinal material mixes extraction, some interaction between component, product stability is poor; Simultaneously because filter such as the diatomite filter selected for use can only be removed some tangible particulate contamination, and can not remove macromolecular substance invalid in the herbal extract.And invalid macromole of this type such as polysaccharide, protein, tannin are very unstable, not only influence mouthfeel, fragrance, color and luster, clarity, the stability of wine, and are to cause the muddy and sedimentary basic reason of wine body.In addition; Along with the difference of the quality of medicinal material own, existing method is difficult for quantitatively allocating according to active constituent content in each medicine, makes quality product wayward; Simultaneously; Later stage adopts diatomite filtration that total flavones in the wine is had very big crown_interception, and the sewage that cleaning zeyssatite produces is very serious, deals with very complicated.
(3) summary of the invention: the object of the invention just provides a kind of Chinese medicine health-care wine and production technique thereof; Chinese medicine health-care wine clarity and good stability that this technology is prepared; Active ingredient of Chinese herbs content is easy to control; Easy to operate, energy-saving and cost-reducing, for a new thinking is opened up in the production of Chinese medicine health-care wine.
A kind of Chinese medicine health-care wine of the present invention, process by following step:
1. select Chinese cassia tree for use, Herba Cistanches, the Radix Astragali, Rhizoma dioscoreae, matrimony vine, thizoma curculiginis, cloves, Radix Angelicae Sinensis, Herba Epimedii, ten kinds of Chinese medicines of fructus amomi, through concocting processing, for use;
2. above-mentioned every kind of medicinal material all with 20%～80% (v/v) ethanol of 6～8 times of medicinal material weight as extracting solvent, carry out single medicine respectively with thermal backflow or contrary jar of stream method of group and extract, the extracting solution of every kind of medicinal material;
3. the extracting solution with above-mentioned each medicinal material of gained separates with whizzer respectively, gets centrate;
4. each medicine centrate of above-mentioned gained is filtered with the microfiltration membrane system respectively, get the micro-filtrate of each medicine;
5. the micro-filtrate with above-mentioned each medicine of gained separates through the ultra-filtration membrane separation system, gets the ultrafiltrated of each medicine;
6. each medicine ultrafiltrated of above-mentioned gained is carried out nanofiltration through the nanofiltration membrane separation system and concentrates, each medicine hold back liquid concentrator;
7. after medicinal material being held back liquid concentrator and is detected active constituent content respectively; Be converted to the concentrated liquid measure that should add by containing medicinal material effective constituent amount in the health promoting wine wine body per ton; Add respectively in the basic wine, make that each medicinal material effective constituent reaches regulation content in the wine, and add an amount of toning, blending material;
8. above-mentioned allotment is good health promoting wine ageing 6～18 months is made clarifying treatment with ceramic membrane filter again, promptly gets.
Prepare the production technique of a kind of Chinese medicine health-care wine of the present invention, comprise the steps:
1. select Chinese cassia tree for use, Herba Cistanches, the Radix Astragali, Rhizoma dioscoreae, matrimony vine, thizoma curculiginis, cloves, Radix Angelicae Sinensis, Herba Epimedii, ten kinds of Chinese medicines of fructus amomi, through concocting processing, for use;
2. above-mentioned every kind of medicinal material all with 20%～80% (v/v) ethanol of 6～8 times of medicinal material weight as extracting solvent, carry out single medicine respectively with thermal backflow or group pipe adverse current method and extract, the extracting solution of every kind of medicinal material;
3. the extracting solution with above-mentioned each medicinal material of gained separates with whizzer respectively, gets centrate;
4. each medicine centrate of above-mentioned gained is filtered with the microfiltration membrane system respectively, get the micro-filtrate of each medicine;
5. the micro-filtrate with above-mentioned each medicine of gained separates through the ultra-filtration membrane separation system, gets the ultrafiltrated of each medicine;
6. each medicine ultrafiltrated of above-mentioned gained is carried out nanofiltration through the nanofiltration membrane separation system and concentrates, each medicine hold back liquid concentrator;
7. after medicinal material being held back liquid concentrator and is detected active constituent content respectively; Be converted into the concentrated liquid measure that should add by contained medicinal material effective constituent weight in the health promoting wine wine body per ton; Add respectively in the basic wine, make that each medicinal material effective constituent reaches regulation content in the wine, and add an amount of toning, blending material;
8. above-mentioned allotment is good health promoting wine ageing 6～18 months is made clarifying treatment with ceramic membrane filter again, promptly gets.
Used whizzer adopts Alfa Laval disc centrifuge, 1000～20000 rev/mins of rotating speeds, centrifugation time 20～30min.
Used microfiltration membrane pipe is the AL2O3 ceramic-film tube, and the film pore directly is 0.02um～1um, and working pressure is 0.05Mpa～0.5Mpa, and solution temperature is 25～75 degree.
Used ultra-filtration membrane is the polysulfones organic hybrid films, film pipe model 5000～100000 molecular weight, working pressure 0.5～2Mpa, 20～50 ℃ of solution temperatures.
Used nf membrane is the polysulfones organic hybrid films, film pipe model 200～500 molecular weight, and working pressure is 1～3Mpa, 20～50 ℃ of solution temperatures, 8～15 times of cycles of concentration.
Used basic wine is little song of 20%～38% (v/v) or yeast wine.
Contained medicinal material effective constituent and content are following in the said health promoting wine wine body per ton:
Chinese cassia tree is by cinnamic aldehyde 1g～50g;
Herba Cistanches is by echinacoside 5g～100g;
The Radix Astragali is by Cyclosiversioside F 5g～100g;
Rhizoma dioscoreae is by total saponins 5g～200g;
Matrimony vine is by LBP 5g～100g;
Thizoma curculiginis is by total saponins 5g～100g;
Cloves is by Syzygium aromaticum stem oil 1g～50g;
The root of kudzu vine is counted 5g～50g by puerarin;
Herba Epimedii is by icarin 10g～150g;
Fructus amomi is counted 10g～200g by volatile oil.
This technology realizes that single medicine of Production of Health Wine extracts, and quantitatively is added in the basic wine by content of effective, has improved the stability and the security of product greatly.Utilize advanced extraction and membrane separation process; Extract the effective constituent in the medicinal material to greatest extent; Remove the invalid components in the extracting solution; The effective ingredient of Chinese medicinal materials can intactly be retained in the wine liquid, keep the characteristics that the clarification of wine body is bright, be pleasant to the eye and taste simultaneously again, realize the energy-conserving and environment-protective effect.For Production of Healthy Wine has been opened up a novel process.
This technology compares with traditional technology, has following advantage:
1, traditional method uses seepage to extract, and extraction time is 18 to 20 days, and filtering, be formulated to ageing is 5 days.From the medicinal material extract to the ageing, need about 25 days.Process using thermal backflow of the present invention or group jar countercurrent extraction, 0.3 day extraction time; Membrane filtration 0.3 day is allocated 0.1 day, needs 0.6 to 1 day altogether, and production efficiency improves 17 to 24 times;
2, the traditional vacuum concentrating under reduced pressure needs steam heating; Vacuum pump and cooling water system; And concentrated electricity and the water of only needing of nanofiltration, like concentrated 16 times water, the spissated energy consumption cost of nanofiltration is about 33 yuan/ton; And 360 yuan/ton of vacuum decompression simmer down tos, so nanofiltration is concentrated in and concentrates cost than the concentrated advantage that has more of vacuum decompression.
3, the temperature of traditional vacuum concentrating under reduced pressure is at 75 ℃～80 ℃, and must under vacuum condition, concentrate, in the concentration process; Must be heated for a long time; And adopt the nanofiltration thickening temperature among the present invention at 27 ℃～30 ℃, and carrying out basically at normal temperatures, concentration process does not have phase transformation; Therefore and the traditional vacuum decompression of nanofiltration concentration ratio is concentrated in and keeps original material property aspect to have more advantage; Vacuum decompression concentrates the material rate of loss generally 2%～3% simultaneously; Possibly cause heat-sensitive substance and volatile substances to decompose owing to be heated for a long time; Thereby loss is higher; And nanofiltration to concentrate be to carry out at normal temperatures, the loss of material rate is generally 0.1%～0.2% in the concentration process, loss mainly is residual and lose by the film pipe;
4, single medicine extracts and replaces compound to extract, and realizes quantitatively adding effective constituent in the desired amount, has improved the stability of quality product.
5, thermal backflow or group pipe countercurrent extraction replace traditional infiltration or seepage to extract, and have improved extraction ratio of effective constituents in the medicinal material, shorten extraction time greatly, enhance productivity.
Replace conventional filter such as zeyssatite, microporous membrane fine filting machine with ceramic membrane, shortened filtration time; With macromole inert matters such as the protein in the ultra-filtration membrane removal extracting solution, polysaccharide, tannins, solve the wine body and often produce sedimentary problem.
The nanofiltration membrane separation system of this process using also is the concentration process that a low temperature does not have phase transformation when holding back target substance, has reduced concentration time, has reduced energy consumption;
The health promoting wine steady quality of this explained hereafter, nourishing function is remarkable, and the clarification of wine body is bright, and color, smell and taste are all good,
Replace diatomite filtration wine body with ceramic membrane, can reduce loss of active ingredients in the wine body, reduce the pollution of zeyssatite environment.
(4) embodiment:
Embodiment 1
1, Chinese cassia tree, Herba Cistanches, the Radix Astragali, Rhizoma dioscoreae, matrimony vine, thizoma curculiginis, the cloves of selecting for use processing treatment to cross; The root of kudzu vine, Herba Epimedii, ten kinds of medicinal materials of fructus amomi; 50%～60% ethanol with 6～8 times of medicinal material weight extracts three times with group jar reflux type respectively, and the time is respectively 1.5h, 1h, 0.5h; Get each medicament extracting solution;
2, each medicament extracting solution is carried out high speed centrifugation 20～30min with the Alfa Laval disc centrifuge respectively, rotating speed is 1000～10000 commentaries on classics/min, collects supernatant, and the solution after centrifugal asks for a clarification transparent;
3, be the micro-filtration alumina-ceramic membrane filtration of 0.02um～1um with each medicine supernatant through the aperture, working pressure is 0.05Mpa～0.5Mpa, and temperature is 25～75 ℃, removes pectin, particulate, flocks and most of mikrobe, gets micro-filtrate;
4, be that 5000～100000 ultrafiltration PS membrane filters through molecular weight cut-off respectively with each medicine micro-filtrate of gained, working pressure 0.5～2Mpa, 20～50 ℃ of temperature are removed soluble large molecule impurity such as polysaccharide, phlegmatic temperament, protein, the ultrafiltrated of each medicine;
5, with each medicine ultrafiltrated of gained through molecular weight be 200～500 nanofiltration polysulfones organic hybrid films concentration respectively, working pressure is 1～3Mpa, 20～50 ℃ of temperature, 8～15 times of cycles of concentration, each medicine held back liquid concentrator;
6, utilize near infrared online monitoring and other test set, each medicine held back liquid concentrator carry out monitoring and detection, detect each medicine respectively and hold back active constituent content corresponding in the liquid concentrator, reach following scope and can get into the allotment operation:
Radix Astragali liquid concentrator Astragaloside content: 100～200mg/L;
Herba Epimedii liquid concentrator icarin content: 500～1500mg/L;
Rhizoma dioscoreae liquid concentrator total saponin content: 1000～3000mg/L;
Thizoma curculiginis liquid concentrator total saponin content: 1000～4500mg/L;
Chinese cassia tree liquid concentrator cinnamic aldehyde content: 1000～3750mg/L;
Herba Cistanches echinacoside content: 500～1500mg/L;
Matrimony vine liquid concentrator LBP content: 1500～4500mg/L;
Cloves liquid concentrator Syzygium aromaticum stem oil content: 1000～5000mg/L;
Root of kudzu vine liquid concentrator puerarin content: 1000～6000mg/L;
Fructus amomi liquid concentrator volatile oil content: 1500～7500mg/L;
7, allotment operation: according to the amount of contained medicinal material effective constituent in the health promoting wine wine body per ton, be converted into corresponding each medicinal material and concentrate liquid measure, quantitatively join in little song of 20%～38% (v/v) or the yeast wine, make that each medicinal material effective constituent reaches regulation content in the wine; And add an amount of toning, blending material.
Calculate required concentrated liquid measure according to 1 ton of health promoting wine wine body:
The Radix Astragali concentrates liquid measure: 50.00～500.00L
Herba Epimedii concentrates liquid measure: 20.00～100.00L
Rhizoma dioscoreae concentrates liquid measure: 5.00～66.67L
Thizoma curculiginis concentrates liquid measure: 5.00～22.22L
Chinese cassia tree concentrates liquid measure: 1.00～13.33L
Herba Cistanches concentrates liquid measure: 10.00～66.67L
Matrimony vine concentrates liquid measure: 3.33～22.22L
Cloves concentrates liquid measure: 1.00～10.00L
The root of kudzu vine concentrates liquid measure: 5.00～8.33L
Fructus amomi concentrates liquid measure: 6.67～26.67L
8, health promoting wine ageing that above-mentioned allotment is good is 6～18 months, uses film pore footpath to do clarifying treatment as the ceramic membrane of 0.02um～1um again, gets product, and detects the packing warehouse-in.
Employed 50%～60% ethanol (v/v) is food grade among the present invention;
Each medicine is held back in the liquid concentrator corresponding active constituent content and is detected all by 2005 editions that " corresponding method is carried out in one one of the Chinese pharmacopoeia.
Claims (8)
1. Chinese medicine health-care wine, process by following step:
1. select Chinese cassia tree for use, Herba Cistanches, the Radix Astragali, Rhizoma dioscoreae, matrimony vine, thizoma curculiginis, cloves, Radix Angelicae Sinensis, Herba Epimedii, ten kinds of Chinese medicines of fructus amomi, through concocting processing, for use;
2. above-mentioned every kind of medicinal material all with 20%～80% (v/v) ethanol of 6～8 times of medicinal material weight as extracting solvent, carry out single medicine respectively with a thermal backflow or a group jar adverse current method and extract, the extracting solution of every kind of medicinal material;
3. the extracting solution with above-mentioned each medicinal material of gained separates with whizzer respectively, gets centrate;
4. each medicine centrate of above-mentioned gained is filtered with the microfiltration membrane system respectively, get the micro-filtrate of each medicine;
5. the micro-filtrate with above-mentioned each medicine of gained separates through the ultra-filtration membrane separation system, gets the ultrafiltrated of each medicine;
6. each medicine ultrafiltrated of above-mentioned gained is carried out nanofiltration through the nanofiltration membrane separation system and concentrates, each medicine hold back liquid concentrator;
7. after medicinal material being held back liquid concentrator and is detected active constituent content respectively; Be converted to the concentrated liquid measure that should add by containing the medicinal material active constituent content in the health promoting wine wine body per ton; Add respectively in the basic wine, make that each medicinal material effective constituent reaches regulation content in the wine, and add an amount of toning, blending material;
8. above-mentioned allotment is good health promoting wine ageing 6～18 months is made clarifying treatment with ceramic membrane filter again, promptly gets;
Contained medicinal material effective constituent and content are following in the said health promoting wine wine body per ton:
Chinese cassia tree is by cinnamic aldehyde 1g～50g;
Herba Cistanches is by echinacoside 5g～100g;
The Radix Astragali is by Cyclosiversioside F 5g～100g;
Rhizoma dioscoreae is by total saponins 5g～200g;
Matrimony vine is by LBP 5g～100g;
Thizoma curculiginis is by total saponins 5g～100g;
Cloves is by Syzygium aromaticum stem oil 1g～50g;
The root of kudzu vine is counted 5g～50g by puerarin;
Herba Epimedii is by icarin 10g～150g;
Fructus amomi is counted 10g～200g by volatile oil.
2. the production technique of a kind of Chinese medicine health-care wine according to claim 1 is characterized in that comprising the steps:
1. select Chinese cassia tree for use, Herba Cistanches, the Radix Astragali, Rhizoma dioscoreae, matrimony vine, thizoma curculiginis, cloves, Radix Angelicae Sinensis, Herba Epimedii, ten kinds of Chinese medicines of fructus amomi, through concocting processing, for use;
2. above-mentioned every kind of medicinal material all with 20%～80% (v/v) ethanol of 6～8 times of medicinal material weight as extracting solvent, carry out single medicine with the thermal backflow method and extract, extracting solution that must every kind of medicinal material;
3. the extracting solution with above-mentioned each medicinal material of gained separates with whizzer respectively, gets centrate;
4. each medicine centrate of above-mentioned gained is filtered with the microfiltration membrane system respectively, get the micro-filtrate of each medicine;
5. the micro-filtrate with above-mentioned each medicine of gained separates through the ultra-filtration membrane separation system, gets the ultrafiltrated of each medicine;
6. each medicine ultrafiltrated of above-mentioned gained is carried out nanofiltration through the nanofiltration membrane separation system and concentrates, each medicine hold back liquid concentrator;
7. after medicinal material being held back liquid concentrator and is detected active constituent content respectively; Be converted into the concentrated liquid measure that should add by contained medicinal material active constituent content in the health promoting wine wine body per ton; Add respectively in the basic wine, make that each medicinal material effective constituent reaches regulation content in the wine, and add an amount of toning, blending material;
8. above-mentioned allotment is good health promoting wine ageing 6～18 months is made clarifying treatment with ceramic membrane filter again, promptly gets.
3. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: used whizzer adopts Alfa Laval disc centrifuge, 1000～20000 rev/mins of rotating speeds, centrifugation time 20～30min.
4. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: used microfiltration membrane pipe is Al
2O
3Ceramic-film tube, film pore directly are 0.02 μ m～1 μ m, and working pressure is 0.05MPa～0.5MPa, and solution temperature is 25～75 degree.
5. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: used ultra-filtration membrane is the polysulfones organic hybrid films, film pipe model 5000～100000 molecular weight, working pressure 0.5～2MPa, 20～50 ℃ of solution temperatures.
6. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: used nf membrane is the polysulfones organic hybrid films, film pipe model 200～500 molecular weight, and working pressure is 1～3MPa, 20～50 ℃ of solution temperatures; 8～15 times of cycles of concentration.
7. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: used basic wine is little song of 20%～38% (v/v) or yeast wine.
8. the production technique of a kind of Chinese medicine health-care wine according to claim 2 is characterized in that: contained medicinal material effective constituent and content are following in the said health promoting wine wine body per ton:
Chinese cassia tree is by cinnamic aldehyde 1g～50g;
Herba Cistanches is by echinacoside 5g～100g;
The Radix Astragali is by Cyclosiversioside F 5g～100g;
Rhizoma dioscoreae is by total saponins 5g～200g;
Matrimony vine is by LBP 5g～100g;
Thizoma curculiginis is by total saponins 5g～100g;
Cloves is by Syzygium aromaticum stem oil 1g～50g;
The root of kudzu vine is counted 5g～50g by puerarin;
Herba Epimedii is by icarin 10g～150g;
Fructus amomi is counted 10g～200g by volatile oil.
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Inventor after: Yang Yuejun Inventor after: Wu Shaoxun Inventor after: Zhao Guofeng Inventor after: Liu Yuancai Inventor after: Yu Dayan Inventor after: Chen Zhiyuan Inventor after: Liu Shenghua Inventor after: Zhang Haoran Inventor after: Liu Shilong Inventor before: Yang Yuejun Inventor before: Zhao Guofeng Inventor before: Liu Yuancai Inventor before: Yu Dayan Inventor before: Chen Zhiyuan Inventor before: Liu Shenghua Inventor before: Zhang Haoran Inventor before: Liu Shilong |