CN104099207A - Ultrafiltration separation technology suitable for strengthening and tonifying wine - Google Patents
Ultrafiltration separation technology suitable for strengthening and tonifying wine Download PDFInfo
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- CN104099207A CN104099207A CN201310121834.3A CN201310121834A CN104099207A CN 104099207 A CN104099207 A CN 104099207A CN 201310121834 A CN201310121834 A CN 201310121834A CN 104099207 A CN104099207 A CN 104099207A
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- membrane filtration
- filtration equipment
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- membrane filter
- membrane
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Abstract
The invention discloses an ultrafiltration separation technology suitable for strengthening and tonifying wine, and the concrete steps of the technology are as follows: after extracting liquid solid-liquid separation and diatomite microfiltration, adding the extracting liquid into membrane filtration equipment, checking whether valves and switches are in the normal state, starting the membrane filtration equipment, setting the temperature to 40 DEG C to 45 DEG C, the transmembrane pressure as 0.6MPa-0.8MPa, and cut-off molecular core amount to-2, adding a solvent for diluting the top washing amount to be 3 times of the cyclic interception liquid of the membrane filtration equipment for three times of top washing, taking out the material liquid, removing filter residues in the membrane filtration equipment, washing the membrane filtration equipment with clear water, then adding a cleaning-agent-containing aqueous solution for washing the membrane filtration equipment, running the membrane filtration equipment for 30min at 50 DEG C, and washing the membrane filtration equipment with the clear water; the ultrafiltration separation technology can achieve the effect of clarifying and separation in the extraction separation of the strengthening and tonifying wine traditional Chinese medicine, and all the active ingredients in medicinal materials can be retained.
Description
Technical field
The present invention relates to a kind of Ultrafiltration Membrane that is applicable to strong power tonic wine.
Background technology
At present Chinese medicine refining, mainly with polarity difference between chemical composition (as solvent deposition or extraction, fractionation by adsorption etc.) for ultimate principle separation, remains in more deficiency.
Summary of the invention
In order to solve the deficiencies in the prior art, the present invention has developed a kind of Ultrafiltration Membrane that is applicable to strong power tonic wine, the concrete steps of this technology are: by after extracting solution solid-liquid separation and diatomite micro-filtration, add in membrane filter plant, check each valve, whether switch is in standard state, start membrane filter plant, temperature is made as 40 DEG C-45 DEG C, transmembrane pressure is made as 0.6MPa-0.8MPa, the molecule core rod amount of damming is made as-2, the solubilizing agent dilution top amount of washing is that 3 times of tops of membrane filter plant minimal circulation trapped fluid are washed three times, take out feed liquid, membrane filter plant is got rid of to filter residue, with clear water flushing membrane filter plant, again with adding the aqueous cleaning membrane filter plant that contains cleaning agents of membrane, make membrane filter plant move 30min in 50 DEG C, use again clear water cleaning membrane filtration equipment, described extracting solution has two kinds, and wherein one comprises: mulberry fruit, Radix Codonopsis, the Radix Astragali, Radix Glycyrrhizae, wolfberry fruit, Radix Angelicae Sinensis, ginseng palpus, the bark of eucommia, 50% ethanol, yellow wine extraction liquid, another kind comprises: Herba Epimedii, 50% ethanol extract.
The invention has the beneficial effects as follows: this isolation technique separates the effect that can reach clarified separation in strong power tonic wine traditional Chinese medicine extraction, retained effective constituent all in medicinal material, hold back tannin, macromole impurity etc., reach parting liquid stable, reduced production cost, environmental protection, has improved quality product.
Embodiment
The Ultrafiltration Membrane that is applicable to strong power tonic wine of the present invention, the concrete steps of this technology are: by after extracting solution solid-liquid separation and diatomite micro-filtration, add in membrane filter plant, check each valve, whether switch is in standard state, start membrane filter plant, temperature is made as 40 DEG C-45 DEG C, transmembrane pressure is made as 0.6MPa-0.8MPa, the molecule core rod amount of damming is made as-2, the solubilizing agent dilution top amount of washing is that 3 times of tops of membrane filter plant minimal circulation trapped fluid are washed three times, take out feed liquid, membrane filter plant is got rid of to filter residue, with clear water flushing membrane filter plant, again with adding the aqueous cleaning membrane filter plant that contains cleaning agents of membrane, make membrane filter plant move 30min in 50 DEG C, use again clear water cleaning membrane filtration equipment, described extracting solution has two kinds, and wherein one comprises: mulberry fruit, Radix Codonopsis, the Radix Astragali, Radix Glycyrrhizae, wolfberry fruit, Radix Angelicae Sinensis, ginseng palpus, the bark of eucommia, 50% ethanol, yellow wine extraction liquid, another kind comprises: Herba Epimedii, 50% ethanol extract.
This isolation technique separates the effect that can reach clarified separation in strong power tonic wine traditional Chinese medicine extraction, retained effective constituent all in medicinal material, holds back tannin, macromole impurity etc., reaches parting liquid stable, reduced production cost, and environmental protection, has improved quality product.
Claims (1)
1. be applicable to the Ultrafiltration Membrane of strong power tonic wine, it is characterized in that, the concrete steps of this technology are: by after extracting solution solid-liquid separation and diatomite micro-filtration, add in membrane filter plant, check each valve, whether switch is in standard state, start membrane filter plant, temperature is made as 40 DEG C-45 DEG C, transmembrane pressure is made as 0.6MPa-0.8MPa, the molecule core rod amount of damming is made as-2, the solubilizing agent dilution top amount of washing is that 3 times of tops of membrane filter plant minimal circulation trapped fluid are washed three times, take out feed liquid, membrane filter plant is got rid of to filter residue, with clear water flushing membrane filter plant, again with adding the aqueous cleaning membrane filter plant that contains cleaning agents of membrane, make membrane filter plant move 30min in 50 DEG C, use again clear water cleaning membrane filtration equipment, described extracting solution has two kinds, and wherein one comprises: mulberry fruit, Radix Codonopsis, the Radix Astragali, Radix Glycyrrhizae, wolfberry fruit, Radix Angelicae Sinensis, ginseng palpus, the bark of eucommia, 50% ethanol, yellow wine extraction liquid, another kind comprises: Herba Epimedii, 50% ethanol extract.
Priority Applications (1)
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CN201310121834.3A CN104099207A (en) | 2013-04-10 | 2013-04-10 | Ultrafiltration separation technology suitable for strengthening and tonifying wine |
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CN201310121834.3A CN104099207A (en) | 2013-04-10 | 2013-04-10 | Ultrafiltration separation technology suitable for strengthening and tonifying wine |
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Citations (5)
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---|---|---|---|---|
CN1751676A (en) * | 2004-09-22 | 2006-03-29 | 天津天士力制药股份有限公司 | Diaphragm ultrafiltration method for refining traditional Chinese medicine |
CN1884469A (en) * | 2006-06-01 | 2006-12-27 | 谢海腾 | Process for promoting yellow wine non-biostability using fractional ultrafiltration |
CN101829501A (en) * | 2010-04-21 | 2010-09-15 | 周滨江 | Combined membrane filtering method for Chinese traditional medicine extraction, separation and concentration |
CN102174360B (en) * | 2011-02-15 | 2012-06-06 | 杨军 | Process for preparing largehead atractylodes rhizome tonic spirit |
CN102021106B (en) * | 2009-09-18 | 2012-11-21 | 劲牌有限公司 | Traditional Chinese medicine health wine and production technology thereof |
-
2013
- 2013-04-10 CN CN201310121834.3A patent/CN104099207A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1751676A (en) * | 2004-09-22 | 2006-03-29 | 天津天士力制药股份有限公司 | Diaphragm ultrafiltration method for refining traditional Chinese medicine |
CN1884469A (en) * | 2006-06-01 | 2006-12-27 | 谢海腾 | Process for promoting yellow wine non-biostability using fractional ultrafiltration |
CN102021106B (en) * | 2009-09-18 | 2012-11-21 | 劲牌有限公司 | Traditional Chinese medicine health wine and production technology thereof |
CN101829501A (en) * | 2010-04-21 | 2010-09-15 | 周滨江 | Combined membrane filtering method for Chinese traditional medicine extraction, separation and concentration |
CN102174360B (en) * | 2011-02-15 | 2012-06-06 | 杨军 | Process for preparing largehead atractylodes rhizome tonic spirit |
Non-Patent Citations (4)
Title |
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中国质量新闻网: "国家质检总局通报果露酒产品质量监督抽查结果", 《HTTP://WWW.CQN.COM.CN/NEWS/XFPD/CCGG/GJCC/2009/300059.HTML》, 3 March 2010 (2010-03-03), pages 36 * |
赵国锋等: "超滤分离技术在中药保健酒工艺中应用研究", 《第三届全国膜分离技术在食品工业中应用研讨会论文集》 * |
邢卫红: "陶瓷膜成套装备与工程应用技术的研究", 《中国博士学位论文全文数据库工程科技1辑》, no. 1, 15 March 2004 (2004-03-15), pages 015 - 10 * |
陈余: "膜分离技术在中药提取分离中的应用", 《化学工程与装备》, no. 2, 28 February 2013 (2013-02-28), pages 126 - 128 * |
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Application publication date: 20141015 |