CN101946982B - Use of natural plant material in cigarette - Google Patents
Use of natural plant material in cigarette Download PDFInfo
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- CN101946982B CN101946982B CN2010102702373A CN201010270237A CN101946982B CN 101946982 B CN101946982 B CN 101946982B CN 2010102702373 A CN2010102702373 A CN 2010102702373A CN 201010270237 A CN201010270237 A CN 201010270237A CN 101946982 B CN101946982 B CN 101946982B
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- cigarette
- queensland nut
- flower
- nut flower
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Abstract
The invention relates to a use of macadamia flower in preparing cigarette. Extractum is prepared from macadamia flower and then added to cigarette. The macadamia flower is subjected to the immersion treatment of hydrochloric acid, tannase, water and the like to obtain cigarette macadamia flower thin slice. A certain amount of macadamia flower extractum or thin slice is added to cigarette to obtain the cigarette product with the taste of macadamia flower, and the cigarette obtained has light and soft smoke and contains lower content of harmful substances than common commercially available cigarettes, thus the safety of the cigarette is enhanced.
Description
Technical field
The present invention relates to the cigarette industry technical field, the application of specifically a kind of natural plant material Queensland nut flower in cigarette.
Background technology
Queensland nut is the emerging fruit tree that southern china just grows up in recent years, is Proteaceae, Queensland nut platymiscium.Originate in the hylaeion hypotropicum of Queensland ,Australia and New South Wales, because its economic worth is high, whole world developed recently is very fast.Began plantation in 1858, so far the history in existing 150 years.China introduces a fine variety the seventies in 20th century and to plant experimentally Queensland nut, and in Guangdong, provinces and regions such as Guangxi, Yunnan, Hainan, Fujian, Zhejiang, Sichuan, Guizhou introduce a fine variety and plant experimentally, cultivated area reaches 5400hm
2, wherein, what cultivated area was maximum is Yunnan.Queensland nut is nutritious, oil content about 70%, and protein 9% contains 8 seed amino acids of needed by human, also is rich in minerals and vitamins B
1, B
2At present more to the research of Queensland nut, but to the research of Queensland nut flower with use lessly, do not see the comprehensive utilization of Queensland nut flower in cigarette.
Summary of the invention
The purpose of this invention is to provide application and the application process of a kind of Queensland nut flower in cigarette preparation, it is fragrant to make cigarette contain Queensland nut flower article.
The present invention is the fragrance material that from Queensland nut is spent, extracts, and extract mixes with pipe tobacco by a certain percentage, makes Queensland nut flower local flavor cigarette.Make cigarette that tangible Queensland nut flowery odour arranged, flue gas is simple and elegant soft.Queensland nut has been spent except that blade and stem, taken by weighing 10g and put into distilling and extracting device simultaneously, utilized the 20mL dichloromethane extraction, at 60 ℃ of following water-bath heating, distillation extraction 2h simultaneously.Extract adds an amount of dry anhydrous sodium sulfate, and placement is spent the night, 45 ℃ with normal pressure under be concentrated into 1mL, carry out GC-MS and analyze.Queensland nut medicinal extract GC-MS total ion chromatogram: like Fig. 1; Analysis result such as table 1 detect 55 kinds of materials altogether.
Table 1
The application process of Queensland nut flower of the present invention is following:
Method 1. has spent Queensland nut except that blade and stem; Insert in the quick solvent extraction appearance of ASE300, as extracting solvent, extracting temperature is 100～120 ℃ with mass percentage concentration 50%～90% ethanol; Extraction time is 5min～30min; Extraction pressure is 7MPa～14MPa, circulates 3 times, and extract concentrates and obtains the Queensland nut flower concrete; Add absolute ethyl alcohol to dissolving fully with the Queensland nut flower concrete, the amount with 13 μ L/g on pipe tobacco is sprayed.
Method 2. is soaked with hydrochloric acid or tannase or water the Queensland nut flower to it, refilter the back and process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo.
During with the salt soak: the concentration of hydrochloric acid is 0.01mol/L～0.1mol/L, and the solid-liquid mass ratio is 1: 1～1: 8; In temperature is under 50 ℃～100 ℃, and soak time is 30min～60min;
When soaking with tannase: the tannase mass percentage concentration is 0.1%～1%, and soaking temperature is 20 ℃～50 ℃, and soak time is 60min～150min; The solid-liquid mass ratio is 1: 1～1: 8.
When being soaked in water: the solid-liquid mass ratio is 1: 1～1: 8, and water temperature is 50 ℃～100 ℃, soak time 30min～60min.
The Queensland nut flower thin slice that said method is processed adds in the cigarette according to 1%～30% of every pipe tobacco gross weight, produces finished cigarettes.
The present invention and present compared with techniques have following outstanding beneficial effect:
1, when keeping the cigarette smoking characteristic, add natural plant perfume and extracted composition, protected consumer's health.
2, the cigarette effect of smokeing panel test is good, the cigarette aesthetic quality is influenced less, has increased Queensland nut fragrance of a flower gas in the cigarette.
3, this cigarette has increased the distinctive Queensland nut flowery odour of cigarette, will have good social benefit and economic benefit.
The present invention can keep the comfortableness of the fragrant and smoking cigarette of enough cigarette when effectively having guaranteed former cigarette style, and the cigarette style of peculiar Queensland nut fragrance of a flower gas is provided.For reducing the tar and the harmful substance of cigarette; Use the Queensland nut flower concrete in the cigarette; Because the tar of this medicinal extract burning can not increasing cigarette and new harmful substance produce, therefore, reasonable reducing tar and reducing harm and the technical barrier that keeps the cigarette smoking style of having solved of this technology.Its flue gas is simple and elegant soft, compares with common commercial cigarettes, and this cigarette has lower harmful substance contents, has improved the security of cigarette greatly.
Description of drawings
Fig. 1 is a Queensland nut medicinal extract GC-MS total ion chromatogram.
The specific embodiment
Below in conjunction with specific embodiment, the present invention is detailed further.But they are not to qualification of the present invention.
Embodiment 1:
Queensland nut has been spent except that blade and stem; Utilize the quick solvent extraction appearance of ASE300, as extracting solvent, extracting temperature is 100～120 ℃ with mass percentage concentration 70% ethanol; Extraction time is 10min; Extraction pressure is 10.34MPa, circulates 3 times, and extract concentrates and obtains the Queensland nut flower concrete.Take by weighing 0.05,0.10,0.15,0.20g Queensland nut flower concrete, add the 10mL absolute ethyl alcohol respectively, dissolving fully, the amount with 13 μ L/g on pipe tobacco is sprayed.Flue gas analysis and organoleptic analysis result are: fragrant the increasing of addition cigarette when 0.10mg/ props up, and flue gas concentration and sweet sense have raising, and flue gas matter is medium, and assorted gas is light slightly, and pleasant impression is more comfortable; Addition fragrance when 0.15mg/ props up is elegant, the flue gas hamony is good, nonirritant, and aftertaste is sweeter, and pleasant impression is totally comfortable; Addition hamony when 0.20mg/ props up is owed slightly, and mouthfeel has discomfort slightly.
Embodiment 2:
The Queensland nut flower is dried, and with the hydrochloric acid solution immersion of 0.05mol/L, the solid-liquid mass ratio is 1: 4; Temperature is 80 ℃, and soak time is 40min, after filtering; Process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo; Queensland nut flower thin slice is added in the cigarette, and addition is 10% of a pipe tobacco gross weight, produces finished cigarettes.
Embodiment 3:
The Queensland nut flower is dried, soak with 0.07mol/L hydrochloric acid, the solid-liquid mass ratio is 1: 6; Temperature is 100 ℃, and soak time is 30min, after filtering; Process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo; Queensland nut flower thin slice is added in the cigarette, and addition is 20% of a pipe tobacco gross weight, produces finished cigarettes.
Embodiment 4:
The Queensland nut flower is dried, soak with 0.1mol/L hydrochloric acid, the solid-liquid mass ratio is 1: 8; Temperature is 50 ℃, and soak time is 60min, after filtering; Process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo; Queensland nut flower thin slice is added in the cigarette, and addition is 30% of a pipe tobacco gross weight, produces finished cigarettes.
Embodiment 5:
The Queensland nut flower is dried, and using concentration is that 0.3% tannase soaks (enzymolysis), and the solid-liquid mass ratio is 1: 8; Temperature is 35 ℃, soaks 120min, after filtering; Process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo; Queensland nut flower thin slice is added in the cigarette, and addition is 15% of a pipe tobacco gross weight, produces finished cigarettes.
Embodiment 6:
The Queensland nut flower is dried, and using concentration is that 0.8% tannase is handled: the solid-liquid mass ratio is 1: 4, and temperature is 50 ℃; Enzymolysis is 60min; After filtering, process Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo, Queensland nut flower thin slice is added in the cigarette; Addition is 5% of a pipe tobacco gross weight, produces finished cigarettes.
Embodiment 7:
The Queensland nut flower is dried, be soaked in water, the solid-liquid mass ratio is 1: 1 (or 1: 5; Or 1: 8 all can), water temperature be 70 ℃ (or 50 ℃, or 100 ℃ all can); Soak time 30min～60min after filtering, processes Queensland nut flower thin slice by the technological process of producing reconstituted tobacoo; Queensland nut flower thin slice is added in the cigarette, and addition is 1% of a pipe tobacco gross weight, produces finished cigarettes.
Produce the technological process of reconstituted tobacoo: with the Queensland nut flower dry, pulverizing and water is configured to slurries (mass concentration 1～5%); With pulp liquor (with the mass concentration 1～5% of water) according to 5: 1～1: 1 mixed; Stirring to pulp; Paper pulp fiber is dispersed in the water, laminates and dry.The method of producing reconstituted tobacoo belongs to prior art, can find in the documents and materials.
Claims (4)
1. the application of Queensland nut flower in cigarette preparation; It is characterized in that: the Queensland nut flower is soaked it with hydrochloric acid or tannase or water; Process Queensland nut flower thin slice after the filtration, add in the cigarette, produce finished cigarettes according to 1%～30% of every pipe tobacco gross weight.
2. the application of Queensland nut flower according to claim 1 in cigarette preparation, when it is characterized in that the Queensland nut flower soaks it with hydrochloric acid, the concentration of hydrochloric acid is 0.01mol/L～0.1mol/L, the solid-liquid mass ratio is 1: 1～1: 8; Soaking temperature is 50 ℃～100 ℃, and soak time is 30min～60min.
3. the application of Queensland nut flower according to claim 1 in cigarette preparation; When it is characterized in that the Queensland nut flower soaks it with tannase; The tannase mass percentage concentration is 0.1%～1%; Soaking temperature is 20 ℃～50 ℃, and soak time is 60min～150min, and the solid-liquid mass ratio is 1: 1～1: 8.
4. the application of Queensland nut flower according to claim 1 in cigarette preparation, when it is characterized in that Queensland nut flower water soaks it, the solid-liquid mass ratio is 1: 1～1: 8, water temperature is 50 ℃～100 ℃, soaks to be time 30min～60min.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010102702373A CN101946982B (en) | 2010-09-02 | 2010-09-02 | Use of natural plant material in cigarette |
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|---|---|---|---|
| CN2010102702373A CN101946982B (en) | 2010-09-02 | 2010-09-02 | Use of natural plant material in cigarette |
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| CN101946982A CN101946982A (en) | 2011-01-19 |
| CN101946982B true CN101946982B (en) | 2012-08-15 |
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| CN2010102702373A Active CN101946982B (en) | 2010-09-02 | 2010-09-02 | Use of natural plant material in cigarette |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102488316B (en) * | 2011-12-08 | 2014-06-11 | 上海烟草集团有限责任公司 | Tobacco additive for improving sensory quality of tobacco sheet and preparation method as well as application thereof |
| CN102643719A (en) * | 2012-05-09 | 2012-08-22 | 云南烟草科学研究院 | Macadimia nut flower extract and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101624556A (en) * | 2009-07-30 | 2010-01-13 | 无锡嘉华香精香料有限公司 | Tobacco essence with style and features of safflower Hongda tobacco leaves |
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- 2010-09-02 CN CN2010102702373A patent/CN101946982B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101624556A (en) * | 2009-07-30 | 2010-01-13 | 无锡嘉华香精香料有限公司 | Tobacco essence with style and features of safflower Hongda tobacco leaves |
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| CN101946982A (en) | 2011-01-19 |
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