CN101945823B - 大晶体分子筛及其制备 - Google Patents

大晶体分子筛及其制备 Download PDF

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Publication number
CN101945823B
CN101945823B CN2009801059086A CN200980105908A CN101945823B CN 101945823 B CN101945823 B CN 101945823B CN 2009801059086 A CN2009801059086 A CN 2009801059086A CN 200980105908 A CN200980105908 A CN 200980105908A CN 101945823 B CN101945823 B CN 101945823B
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CN
China
Prior art keywords
molecular sieve
reaction mixture
source
molar ratio
amorphous material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2009801059086A
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English (en)
Chinese (zh)
Other versions
CN101945823A (zh
Inventor
W·J·鲁斯
C·L·肯尼迪
T·约克
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ExxonMobil Chemical Patents Inc
Original Assignee
ExxonMobil Chemical Patents Inc
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Publication date
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Publication of CN101945823A publication Critical patent/CN101945823A/zh
Application granted granted Critical
Publication of CN101945823B publication Critical patent/CN101945823B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/36—Pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11
    • C01B39/38—Type ZSM-5
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Materials Engineering (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
CN2009801059086A 2008-02-22 2009-01-19 大晶体分子筛及其制备 Expired - Fee Related CN101945823B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US3070608P 2008-02-22 2008-02-22
US61/030,706 2008-02-22
EP08158024 2008-06-11
EP08158024.3 2008-06-11
PCT/EP2009/000388 WO2009103394A2 (en) 2008-02-22 2009-01-19 Large crystal molecular sieves and their manufacture

Publications (2)

Publication Number Publication Date
CN101945823A CN101945823A (zh) 2011-01-12
CN101945823B true CN101945823B (zh) 2013-07-03

Family

ID=40091847

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2009801059086A Expired - Fee Related CN101945823B (zh) 2008-02-22 2009-01-19 大晶体分子筛及其制备

Country Status (7)

Country Link
US (1) US9296619B2 (enExample)
EP (1) EP2262732B1 (enExample)
JP (1) JP5717447B2 (enExample)
CN (1) CN101945823B (enExample)
SG (1) SG188173A1 (enExample)
WO (1) WO2009103394A2 (enExample)
ZA (1) ZA201005377B (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101952200A (zh) * 2008-02-22 2011-01-19 埃克森美孚化学专利公司 高金属含量分子筛及其制备
KR101858310B1 (ko) 2011-12-01 2018-05-15 엑손모빌 리서치 앤드 엔지니어링 컴퍼니 고활성의 큰 결정 zsm-5의 합성
EP2920112A4 (en) * 2012-11-13 2016-12-07 Basf Se PREPARATION AND USE OF A ZEOLITE MATERIAL IN A PROCESS FOR CONVERTING OXYGENATES IN OLEFINE

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4375458A (en) * 1977-08-17 1983-03-01 Mobil Oil Corporation Synthesis of large crystallite zeolites
CN1732127A (zh) * 2002-12-30 2006-02-08 Sk株式会社 在没有有机模板下采用可变温度制备zsm－5的方法
CN101112996A (zh) * 2007-07-09 2008-01-30 南京工业大学 一种快速合成NaY分子筛的方法

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ193928A (en) * 1979-06-11 1982-09-07 Mobil Oil Corp Preparation of large crystal zeolite zsm-5
ZA807515B (en) * 1979-12-07 1982-07-28 British Petroleum Co Ocess for the productrion of crystalline aluminosilicates and their use as catalyst supports
JPS5954620A (ja) * 1982-09-20 1984-03-29 Toyo Soda Mfg Co Ltd ゼオライトを製造する方法
DK164097C (da) * 1982-09-20 1992-10-05 Tosoh Corp Fremgangsmaade til fremstilling af zeoliter
NZ215434A (en) * 1985-04-08 1988-11-29 Mobil Oil Corp Method of producing a zeolite
US4908342A (en) * 1985-09-04 1990-03-13 Mobil Oil Corporation ZSM-5 zeolites having uniformly large crystals
JP2564581B2 (ja) * 1987-12-28 1996-12-18 水澤化学工業株式会社 高シリカ含有量ゼオライトの製法
JP3537908B2 (ja) * 1995-03-23 2004-06-14 三井造船株式会社 Ｙ型ゼオライト膜製造法及び液体混合物分離膜
JP4065560B2 (ja) * 1995-06-06 2008-03-26 モービル オイル コーポレーション 大きな結晶のｚｓｍ−５の製造方法
ZA979264B (en) * 1996-10-17 1998-12-29 Exxon Chemical Patents Inc Synthesis of large crystal zeolites
US6180550B1 (en) * 1998-12-22 2001-01-30 Mobile Oil Corporation Small crystal ZSM-5, its synthesis and use
EP1587756A4 (en) * 2002-12-30 2011-07-06 Sk Energy Co Ltd PROCESS FOR THE PREPARATION OF ZSM-5 BY VARIABLE TEMPERATURE WITHOUT ORGANIC STENCIL MATERIAL
CN101952200A (zh) * 2008-02-22 2011-01-19 埃克森美孚化学专利公司 高金属含量分子筛及其制备

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4375458A (en) * 1977-08-17 1983-03-01 Mobil Oil Corporation Synthesis of large crystallite zeolites
CN1732127A (zh) * 2002-12-30 2006-02-08 Sk株式会社 在没有有机模板下采用可变温度制备zsm－5的方法
CN101112996A (zh) * 2007-07-09 2008-01-30 南京工业大学 一种快速合成NaY分子筛的方法

Also Published As

Publication number Publication date
WO2009103394A2 (en) 2009-08-27
EP2262732B1 (en) 2017-05-24
JP2011523393A (ja) 2011-08-11
US9296619B2 (en) 2016-03-29
EP2262732A2 (en) 2010-12-22
ZA201005377B (en) 2011-04-28
SG188173A1 (en) 2013-03-28
WO2009103394A3 (en) 2010-04-22
JP5717447B2 (ja) 2015-05-13
US20110207983A1 (en) 2011-08-25
CN101945823A (zh) 2011-01-12

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130703

Termination date: 20210119

CF01 Termination of patent right due to non-payment of annual fee