CN101890119A - Medicament for treating cardiovascular and cerebrovascular diseases and preparation method thereof - Google Patents
Medicament for treating cardiovascular and cerebrovascular diseases and preparation method thereof Download PDFInfo
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- CN101890119A CN101890119A CN 201010158833 CN201010158833A CN101890119A CN 101890119 A CN101890119 A CN 101890119A CN 201010158833 CN201010158833 CN 201010158833 CN 201010158833 A CN201010158833 A CN 201010158833A CN 101890119 A CN101890119 A CN 101890119A
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Abstract
The invention discloses a coronary artery healing capsule and a preparation method thereof. According to the formula, the coronary artery healing capsule comprises the following components in percentage by weight: 1 to 5 percent of panax pseudoginseng, 40 to 45 percent of red paeony root, 20 to 30 percent of finger citron, 20 to 30 percent of oriental waterplantain rhizome, and 2 to 7 percent of licorice. The preparation method of the coronary artery healing capsule comprises the following steps of: (1) cleaning and slicing the red paeony root, the oriental waterplantain rhizome and the licorice; (2) cleaning, crushing and sterilizing the panax pseudoginseng; (3) crushing and sterilizing the licorice; (4) decocting the read paeony root and the oriental waterplantain rhizome with water, filtering and concentrating decoction, cooling concentrated solution to the room temperature, depositing the concentrated solution in alcohol, standing the mixture to take supernatant fluid, and concentrating the supernatant fluid again to obtain a clear paste; (5) coarsely crushing the finger citron, adding ethanol into the finger citron and refluxing the finger citron twice, and recovering the ethanol to obtain a clear paste; and (6) mixing and stirring the two clear pastes uniformly, adding the panax pseudoginseng and the licorice powder into the mixture, stirring the mixture uniformly, performing vacuum drying on the mixture to obtain dry paste powder, mixing starch and the dry paste powder uniformly, adding 80 percent ethanol into the mixture, preparing a soft material, and performing granulation, drying, granule straightening, total mixing and capsule filling.
Description
Technical field
The present invention relates to a kind of Chinese patent medicine arteria coronaria recovering capsule and preparation method thereof, belong to the Chinese patent medicine preparing technical field.
Background technology
Raising along with people's living standard, cardiovascular patient is more and more, especially old people, cardiovascular and cerebrovascular disease is very general, usually the method that adopts, except that strengthening physical exercise, being careful in one's diet, rely on medicine to treat, and Drug therapy adopts the Western medicine of chemosynthesis mostly, the medicine of chemosynthesis can be controlled some disease, but also have very big side effect simultaneously, human body is caused damage.
Chinese medicine is the valuable cultural heritage of China, and the Chinese medicine side effect of curing the disease is little, and particularly the old people for the cardiovascular patient more is fit to take.The arteria coronaria recovering capsule is a kind of Chinese patent medicine that is used for the cardiovascular patient of this enterprise research and development, and it through being processed into, has blood circulation promoting and blood stasis dispelling by Radix Notoginseng, Radix Paeoniae Rubra, Fructus Citri Sarcodactylis, Rhizoma Alismatis, Radix Glycyrrhizae, starch, and regulating QI to relieve pain has the expansion coronary vasodilator, the effect of blood flow increasing.Be used for the uncomfortable in chest and angina pectoris of coronary heart disease, hypercholesterolemia and hypertriglyceridemia are also had certain curative effect.
Summary of the invention
The purpose of this invention is to provide a kind of treatment cardiovascular and cerebrovascular disease Chinese patent medicine---arteria coronaria recovering capsule, and the preparation method of arteria coronaria recovering capsule is provided.
Technical scheme of the present invention is, arteria coronaria recovering capsule of the present invention is processed into by Radix Notoginseng, Radix Paeoniae Rubra, Fructus Citri Sarcodactylis, Rhizoma Alismatis, Radix Glycyrrhizae, starch process, the composition of their preparations is: Radix Notoginseng accounts for 1%～5% of formula proportion, Radix Paeoniae Rubra accounts for 40%～45% of formula proportion, Fructus Citri Sarcodactylis accounts for 20%～30% of formula proportion, Rhizoma Alismatis accounts for 20%～30% of formula proportion, and Radix Glycyrrhizae accounts for 2%～7% of formula proportion, and starch accounts for 1%～3% of formula proportion.
Preparation technology's flow process of arteria coronaria recovering capsule of the present invention as shown in drawings.
The preparation method of arteria coronaria recovering capsule of the present invention is:
(1) sheet, drying are made, run through, cut to the Radix Paeoniae Rubra after the weighing, Rhizoma Alismatis, Radix Glycyrrhizae respectively only;
(2) Radix Notoginseng after the weighing is made only, pulverize after drying, sterilize, standby;
(3) dried Radix Glycyrrhizae is pulverized, sterilization, standby;
(4) dried Radix Paeoniae Rubra, Rhizoma Alismatis are decocted with water 2 times, decocting liquid filters the back and concentrates, and concentrated solution is cooled to room temperature, and precipitate with ethanol is got supernatant after leaving standstill, and reconcentration obtains clear paste;
(5) with the Fructus Citri Sarcodactylis coarse crushing after the weighing, add alcohol reflux 2 times, reclaim ethanol, obtain clear paste;
(6) above-mentioned two kinds of clear paste are mixed stir evenly, stir evenly after adding Radix Notoginseng, Radix Glycyrrhizae powder, it is carried out drying under reduced pressure, pulverize after obtaining dried cream, dried cream powder is standby;
(7) with the starch sieving for standby after the weighing;
(8) particle manufacture: with starch, dried cream powder mixing, add 80% ethanol, the system soft material is granulated, drying, and granulate, total mixing, capsule is filled.
The baking temperature of Radix Paeoniae Rubra, Rhizoma Alismatis, Radix Glycyrrhizae: must not be above 80 ℃; Drying time: 4～8 hours, meet the clean quality of medicinal material standard of this kind with the medical material water content and be as the criterion.
The sterilization time of Radix Notoginseng, Radix Glycyrrhizae is 30 minutes; 121 ℃ of sterilising temps, 30 minutes drying times, steam pressure is controlled at 0.3～0.6Mpa.
Radix Paeoniae Rubra, Rhizoma Alismatis decoct twice, each 1 hour; Medical material need soak the regular hour before decocting, and soak time is 30 minutes; Each decoction amount of water is about 6 times of medical material amount; Decoct and adopt steam, Steam Pressure Control of Circulated is in 0.33Mpa, and steam pressure should be to keep the little degree of being that boils of medicinal liquid.
The decoction liquor filtrate of Radix Paeoniae Rubra, Rhizoma Alismatis is concentrated into relative density to 1.06 (65～75 ℃) precipitate with ethanol again when above, and decoction liquor filtrate is concentrated in concentration tank carries out, and adopts the Steam Heating evaporating liquid, and steam pressure is controlled at 0.03～0.1Mpa; In the concentration tank jar negative pressure value be controlled at-0.06～-0.09Mpa.
It is consistent with the weight of thick paste to add amount of alcohol when Radix Paeoniae Rubra, Rhizoma Alismatis concentrated solution precipitate with ethanol; Leave standstill the 24 hours sedimentary time that makes.
Fructus Citri Sarcodactylis is refluxed and adopts 90% ethanol with solvent, and consumption is 5 times of medical material amount; Backflow adds thermal recovery steam, and vapour pressure is controlled at 0.05～0.1Mpa, and steam pressure should be to keep the little degree of being that boils of medicinal liquid; Can adopt during backflow No. 1 or No. 2 multi-function extractors reflux; The reflux, extract, secondary, each 2 hours.
The concentration of alcohol that reclaims is lower than at 20% o'clock and promptly stops to reclaim ethanol, transfers enriching stage to; Steam pressure when reclaiming ethanol is controlled at 0.02～0.1Mpa, and steam pressure should turn down as far as possible when reclaiming ethanol, can guarantee that normally reclaiming ethanol gets final product; In the concentration tank jar negative pressure value be controlled at-0.06～-0.09Mpa.
Radix Paeoniae Rubra, Rhizoma Alismatis precipitate with ethanol supernatant and Fructus Citri Sarcodactylis backflow reclaim ethanol respectively, receive cream when being concentrated into relative density and being 1.30 (65～75 ℃).
Drying under reduced pressure carries out at drying baker, the drying baker vacuum degree control-0.06～-0.09Mpa; Steam pressure is controlled at 0.1-0.15Mpa; Baking temperature is controlled at below 75 ℃, and practical situation (dry thing water content) was decided when drying time should be according to drying; Dry thing water content: answer≤5.0%.
During granulation, dry thing fine powder and starch premixing time are 5～10 minutes; Wetting agent is 80% ethanol; Soft material soft moderate (that holds is agglomerating, and that touches promptly looses), color even; The granulation sieve mesh is 18 or 20 orders; 55～60 ℃ of outlet temperatures during particle drying; Granule water content :≤5.0%.
The present invention's beneficial effect compared with the prior art is, the active ingredient of forming each Chinese crude drug component of this medicine fully can be gathered by this method, guarantee the curative effect of each Chinese crude drug, arteria coronaria recovering capsule by this method preparation has blood circulation promoting and blood stasis dispelling, regulating QI to relieve pain, the expansion coronary vasodilator is arranged, the effect of blood flow increasing.Uncomfortable in chest and the angina pectoris treatment that can be used for coronary heart disease also has certain curative effect to high gallbladder hypercholesterolemia and hypertriglyceridemia.
Description of drawings
Accompanying drawing is preparation technology's flow chart of arteria coronaria recovering capsule of the present invention.
The specific embodiment
The embodiment of the invention is pressed process chart shown in the accompanying drawing and is implemented.
Embodiment 1:
Present embodiment is prepared raw material by following prescription: Radix Notoginseng 4kg, and Radix Paeoniae Rubra 96kg, Fructus Citri Sarcodactylis 65kg, Rhizoma Alismatis 65kg, Radix Glycyrrhizae 6kg, starch 4kg makes 100,000 of arteria coronaria recovering capsules, every 2.4g.Be prepared according to the following steps:
(1) sheet, drying are made, run through, cut to the Radix Paeoniae Rubra after the weighing, Rhizoma Alismatis, Radix Glycyrrhizae respectively only;
After medical material Radix Paeoniae Rubra, Rhizoma Alismatis, the Radix Glycyrrhizae of need cutting run through respectively, cut sheet, cutting thickness: Radix Paeoniae Rubra: be the similar round section, diameter 0.5～3cm, thick 0.3～0.5cm; Rhizoma Alismatis: thick 0.2～0.4cm; Radix Glycyrrhizae: thick 0.2～0.4cm;
Medical material carries out drying at heated-air circulation oven, and baking temperature must not be above 80 ℃; Drying time: 4～8 hours, meet the clean quality of medicinal material standard of this kind with the medical material water content and be as the criterion.
(2) Radix Notoginseng after the weighing is made only, pulverize after drying, sterilize, standby;
Radix Notoginseng is made after drying only, pulverizes on pulverizer, and 30 minutes drying times, steam pressure is controlled at 0.3～0.6Mpa; Sterilization time 30 minutes; 121 ℃ of sterilising temps.
(3) dried Radix Glycyrrhizae is pulverized, sterilization, standby, sterilization process is identical with the Radix Notoginseng sterilization process;
(4) dried Radix Paeoniae Rubra, Rhizoma Alismatis are decocted with water, decocting liquid filters the back and concentrates, and concentrated solution is cooled to room temperature, and precipitate with ethanol is got supernatant after leaving standstill, and reconcentration obtains clear paste;
Radix Paeoniae Rubra, Rhizoma Alismatis decoct twice, each 1 hour; Medical material need soak the regular hour before decocting, and soak time is 30 minutes; Each decoction amount of water is about 6 times of medical material amount; Decoct and adopt steam, Steam Pressure Control of Circulated is in 0.33Mpa, and steam pressure should be to keep the little degree of being that boils of medicinal liquid.
Decoction liquor filtrate is concentrated into relative density to 1.06 (65～75 ℃) precipitate with ethanol again when above, and decoction liquor filtrate is concentrated in concentration tank carries out, and adopts the Steam Heating evaporating liquid, and steam pressure is controlled at 0.03～0.1Mpa; In the concentration tank jar negative pressure value be controlled at-0.06～-0.09Mpa.
It is consistent with the weight of thick paste to add amount of alcohol when Radix Paeoniae Rubra, Rhizoma Alismatis concentrated solution precipitate with ethanol; Leave standstill the 24 hours sedimentary time that makes.
(5) with the Fructus Citri Sarcodactylis coarse crushing after the weighing, add alcohol reflux 2 times, reclaim ethanol, obtain clear paste;
Fructus Citri Sarcodactylis is refluxed and adopts 90% ethanol with solvent, and consumption is 5 times of medical material amount; Backflow adds thermal recovery steam, and vapour pressure is controlled at 0.05～0.1Mpa, and steam pressure should be to keep the little degree of being that boils of medicinal liquid; Can adopt during backflow No. 1 or No. 2 multi-function extractors reflux; The reflux, extract, secondary, each 2 hours.
(6) above-mentioned two kinds of clear paste are mixed stir evenly, stir evenly after adding Radix Notoginseng, Radix Glycyrrhizae powder, it is carried out drying under reduced pressure, pulverize after obtaining dried cream, dried cream powder is standby;
After Radix Paeoniae Rubra, Rhizoma Alismatis precipitate with ethanol supernatant and Fructus Citri Sarcodactylis backflow reclaim ethanol respectively, receive cream when continuing to be concentrated into relative density and being 1.30 (65～75 ℃).
Drying under reduced pressure carries out at drying baker, the drying baker vacuum degree control-0.06～-0.09Mpa; Steam pressure is controlled at 0.1-0.15Mpa; Baking temperature is controlled at below 75 ℃, and practical situation (dry thing water content) was decided when drying time should be according to drying; Dry thing water content: answer≤5.0%.
(7) with the starch sieving for standby after the weighing;
(8) particle manufacture: with starch, dried cream powder mixing, add 80% ethanol, the system soft material is granulated, drying, and granulate, total mixing, capsule is filled.
During granulation, dry thing fine powder and starch premixing time are 5～10 minutes; Wetting agent is 80% ethanol; Soft material soft moderate (that holds is agglomerating, and that touches promptly looses), color even; The granulation sieve mesh is 18 or 20 orders; 55～60 ℃ of outlet temperatures during particle drying; Granule water content :≤5.0%.
Embodiment 2:
Present embodiment is prepared raw material by following prescription: Radix Notoginseng 6kg, and Radix Paeoniae Rubra 100kg, Fructus Citri Sarcodactylis 60kg, Rhizoma Alismatis 60kg, Radix Glycyrrhizae 10kg, starch 4kg makes 100,000 of arteria coronaria recovering capsules, every 2.4g.Same steps as by embodiment 1 is prepared.
Embodiment 3:
Present embodiment is prepared raw material by following prescription: Radix Notoginseng 12kg, and Radix Paeoniae Rubra 108kg, Fructus Citri Sarcodactylis 50kg, Rhizoma Alismatis 50kg, Radix Glycyrrhizae 16kg, starch 4kg makes 100,000 of arteria coronaria recovering capsules, every 2.4g.Same steps as by embodiment 1 is prepared.
Claims (10)
1. arteria coronaria recovering capsule and preparation method thereof is characterized in that, the prescription of described arteria coronaria recovering capsule consists of: Radix Notoginseng accounts for 1%～5% of formula proportion; Radix Paeoniae Rubra accounts for 40%～45% of formula proportion; Fructus Citri Sarcodactylis accounts for 20%～30% of formula proportion; Rhizoma Alismatis accounts for 20%～30% of formula proportion; Radix Glycyrrhizae accounts for 2%～7% of formula proportion;
The preparation method of described arteria coronaria recovering capsule may further comprise the steps:
(1) sheet, drying are made, run through, cut to the Radix Paeoniae Rubra after the weighing, Rhizoma Alismatis, Radix Glycyrrhizae respectively only;
(2) Radix Notoginseng after the weighing is made only, pulverize after drying, sterilize, standby;
(3) dried Radix Glycyrrhizae is pulverized, sterilization, standby;
(4) dried Radix Paeoniae Rubra, Rhizoma Alismatis are decocted with water 2 times, decocting liquid filters the back and concentrates, and concentrated solution is cooled to room temperature, and precipitate with ethanol is got supernatant after leaving standstill, and reconcentration obtains clear paste;
(5) with the Fructus Citri Sarcodactylis coarse crushing after the weighing, add alcohol reflux 2 times, reclaim ethanol, obtain clear paste;
(6) above-mentioned two kinds of clear paste are mixed stir evenly, stir evenly after adding Radix Notoginseng, Radix Glycyrrhizae powder, it is carried out drying under reduced pressure, pulverize after obtaining dried cream, dried cream powder is standby;
(7) with the starch sieving for standby after the weighing;
(8) particle manufacture: with starch, dried cream powder mixing, add 80% ethanol, the system soft material is granulated, drying, and granulate, total mixing, capsule is filled.
2. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, the baking temperature of described Radix Paeoniae Rubra, Rhizoma Alismatis, Radix Glycyrrhizae must not be above 80 ℃; Drying time: 4～8 hours.
3. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, the sterilization time of described Radix Notoginseng, Radix Glycyrrhizae is 30 minutes; 121 ℃ of sterilising temps, 30 minutes drying times, steam pressure is controlled at 0.3～0.6Mpa.
4. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, described Radix Paeoniae Rubra, Rhizoma Alismatis decoct twice, each 1 hour; Medical material need soak 30 minutes before decocting; Each decoction amount of water is 6 times of medical material amount; Decoct and adopt steam, Steam Pressure Control of Circulated is in 0.33Mpa.
5. arteria coronaria recovering capsule according to claim 1 and preparation method thereof, it is characterized in that, the decoction liquor filtrate of described Radix Paeoniae Rubra, Rhizoma Alismatis, be concentrated into relative density to 1.06 (65～75 ℃) precipitate with ethanol again when above, decoction liquor filtrate is concentrated in concentration tank and carries out, adopt the Steam Heating evaporating liquid, steam pressure is controlled at 0.03～0.1Mpa; In the concentration tank jar negative pressure value be controlled at-0.06～-0.09Mpa;
It is consistent with the weight of thick paste to add amount of alcohol when Radix Paeoniae Rubra, Rhizoma Alismatis concentrated solution precipitate with ethanol; Leave standstill and make sedimentary time 〉=72 hour.
6. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, described Fructus Citri Sarcodactylis is refluxed and adopts 90% ethanol with solvent, and consumption is 5 times of medical material amount; Backflow adds thermal recovery steam, and vapour pressure is controlled at 0.05～0.1Mpa; Can adopt multi-function extractor to reflux during backflow; The reflux, extract, secondary, each 2 hours.
7. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, the concentration of alcohol of described recovery is lower than at 20% o'clock and promptly stops to reclaim ethanol, transfers enriching stage to; Steam pressure when reclaiming ethanol is controlled at 0.02～0.1Mpa; In the concentration tank jar negative pressure value be controlled at-0.06～-0.09Mpa.
8. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, described Radix Paeoniae Rubra, Rhizoma Alismatis precipitate with ethanol supernatant and Fructus Citri Sarcodactylis backflow reclaim ethanol respectively, receives cream when being concentrated into relative density and being 1.30 (65～75 ℃).
9. arteria coronaria recovering capsule according to claim 1 and preparation method thereof is characterized in that, described drying under reduced pressure carries out at drying baker, the drying baker vacuum degree control-0.06～-0.09Mpa; Steam pressure is controlled at 0.1-0.15Mpa; Baking temperature is controlled at below 75 ℃, dry thing water content≤5.0%.
10. the preparation method of arteria coronaria recovering capsule according to claim 1 is characterized in that, during described granulation, dry thing fine powder and starch premixing time are 5～10 minutes; Wetting agent is 80% ethanol; The granulation sieve mesh is 18 or 20 orders; 55～60 ℃ of outlet temperatures during particle drying; Granule water content≤5.0%.
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| Application Number | Priority Date | Filing Date | Title |
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| CN 201010158833 CN101890119A (en) | 2010-04-28 | 2010-04-28 | Medicament for treating cardiovascular and cerebrovascular diseases and preparation method thereof |
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| CN 201010158833 CN101890119A (en) | 2010-04-28 | 2010-04-28 | Medicament for treating cardiovascular and cerebrovascular diseases and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103223047A (en) * | 2013-05-21 | 2013-07-31 | 卫斌 | Medicine for treating hyperlipemia and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101385814A (en) * | 2008-09-17 | 2009-03-18 | 李浪辉 | Medicine for treating the coronary heart disease and preparation method thereof |
| CN101496857A (en) * | 2008-01-28 | 2009-08-05 | 天科仁祥技术（北京）有限责任公司 | Blood-activating, stasis-resolving, qi-regulating and analgesic dropping pill and preparation method thereof |
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2010
- 2010-04-28 CN CN 201010158833 patent/CN101890119A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101496857A (en) * | 2008-01-28 | 2009-08-05 | 天科仁祥技术（北京）有限责任公司 | Blood-activating, stasis-resolving, qi-regulating and analgesic dropping pill and preparation method thereof |
| CN101385814A (en) * | 2008-09-17 | 2009-03-18 | 李浪辉 | Medicine for treating the coronary heart disease and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103223047A (en) * | 2013-05-21 | 2013-07-31 | 卫斌 | Medicine for treating hyperlipemia and preparation method thereof |
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Open date: 20101124 |