CN101865819A - Test method of textile printing fastness - Google Patents
Test method of textile printing fastness Download PDFInfo
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- CN101865819A CN101865819A CN200910049290A CN200910049290A CN101865819A CN 101865819 A CN101865819 A CN 101865819A CN 200910049290 A CN200910049290 A CN 200910049290A CN 200910049290 A CN200910049290 A CN 200910049290A CN 101865819 A CN101865819 A CN 101865819A
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Abstract
The invention discloses a test method of textile printing fastness. The test method comprises the following steps of: carrying out a speedy washing test to draw a conclusion of receiving or not; carrying out a practical family washing test to draw a conclusion of receiving or not; and carrying out a stretching test if the two tests draw the conclusions of receiving; and drawing a final conclusion of receiving or not. The test method of textile printing fastness is simple, practical and suitable for various printing textiles and provides national and international manufacturers and suppliers with an assessment criterion for evaluating the qualities of printing textiles.
Description
Technical field
The present invention relates to textile field, relate in particular to a kind of method of testing of textile printing fastness.
Background technology
Lack the fastness situation of change after unified testing standard is checked the PRINTED FABRIC washing at present on the world, the home market, and the various printing fastness testing standards that external buyer formulates such as NIKE, NEXT, DECATHLON, TARGET etc., used instrument is various, used test condition differs, and the mode of evaluation is also different.Therefore, domestic a large amount of manufacturer and supplier press for the printing fastness that such standard is tested textile, thereby the quality quality of examination stamp textile product whether.
Summary of the invention
The method of testing that the purpose of this invention is to provide a kind of textile printing fastness is in order to solve the defective that does not have unified standard to evaluate the printing textile printing fastness in the market.
For achieving the above object, the invention provides a kind of method of testing of textile printing fastness, described method of testing is: quicken washing test, conclusion is for accepting or not accepting; Actual home washings test, conclusion is for accepting or not accepting; If above-mentioned two test results all are to accept, then carry out extension test, final conclusion is for accepting or not accepting.
Wherein, described acceleration washing test is: sample and standard wash agent solution and steel ball are put into jar together, wash at the rotary water bath device; Washed samples; Dry sample; With gray scale evaluation sample change color, with self staining of standard rating staining with gray scale evaluation sample, the surface physics of range estimation evaluation sample changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results with the standard rating variable color.Described actual home washings test is: with sample and washing powder, accompany washing to put into home-use washing machine washing; Dry sample; With gray scale evaluation sample change color, with self staining of standard rating staining with gray scale evaluation sample, the surface physics of range estimation evaluation sample changes, and provides conclusion for accepting or not accepting according to above-mentioned these three evaluation results with the standard rating variable color.Described extension test is: will speed up sample after washing and the actual home washings several that stretches respectively; The variation of range estimation evaluation specimen surface decalcomania according to the evaluation result of two samples, provides final conclusion for accepting or not accepting.
Particularly, described acceleration washing test may further comprise the steps: along the textile broadwise cut two (150 ± 5mm) * (40 ± 5mm) sample, the color of described two samples is identical with stamp, its long limit is the textile weft direction, one as test specimens, and another piece is sample as a comparison; The standard wash agent of dissolving 4.0 ± 0.1g in three grades of water of 1000 ± 5ml is configured to the wash solution that concentration is 4g/L; The rotary water bath device of GB/T12490-2007 standard is warming up to 40 ± 2 ℃, with the jar that the described wash solution of 150 ± 1ml, 10 diameters stainless shot that is 6.0 ± 0.5mm and described test specimens are put into the GB/T12490-2007 standard, described jar is put into described rotary water bath device; Start running 150 ± 10 minutes; Take out described test specimens, it is dry to clean the back; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, self staining with GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results.
Further, described standard wash agent is AATCC 1993 WOB standard wash agent or agent of ECE standard wash or the agent of IEC standard wash that does not contain fluorescer.
Further, the start running cleans twice after quickening the described test specimens of washing in three grades of water of 100ml, and each one minute, and in circulating water, wash to clean.
Described actual home washings test may further comprise the steps: get two samples that color is identical with stamp, one as test specimens, and another piece is sample as a comparison; Accompany washing to put into the tumbling-box washing machine of GB/T8629-2001 standard GB/T 8629-2001 standard wash agent and the 2 ± 0.1kg of test specimens, 21 ± 2g, be set at the 5A washing procedure, 5 circulations of washing under 40 ± 3 ℃ water temperature; Perhaps, accompany washing to put into the agitator type washing machine of GB/T8629-2001 standard GB/T 8629-2001 standard wash agent and the 2 ± 0.1kg of test specimens, 66 ± 2g, be set at the 6B washing procedure, under 40 ± 3 ℃ water temperature with 5 circulations of mode standard washing; Then, take out described test specimens and dry; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, self staining with GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results.
In the actual home washings test,, then get its part sample as a comparison, but must guarantee that test specimens is identical with stamp with contrast sample color if having only a sample; If sample is too little, then must provide two samples.
Further, described standard wash agent is AATCC 1993 WOB standard wash agent or agent of ECE standard wash or the agent of IEC standard wash that does not contain fluorescer, wherein AATCC 1993 WOB standard wash agent are used for agitator type washing machine, and the agent of ECE standard wash or the agent of IEC standard wash that do not contain fluorescer are used for drum-type and two kinds of washing machines of stirring-type.
Further, described drying steps is to dry by the fire under 60-80 ℃ temperature 90 ± 10 minutes, or baking gets final product to dry.
Described extension test may further comprise the steps: tensile sample, the elastic extension of judgement sample; If the elastic extension of sample is less than 30%, with the sample after the described actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, carry out following operation respectively: the test specimens two ends are folding along its length, and respectively step on a seam, make two the seam between the distance be 100 ± 5mm, in the seam of two test specimens, insert metal bar, in addition on the weight of seam stuck-at-kg, the pull-up metal bar is mentioned weight and is continued 10 ± 1 seconds, repeats 5 times; If the elastic extension of sample is more than or equal to 30%, then with the sample after the described actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, carry out following operation respectively: the two ends of test specimens are separately fixed on the stretching fixture, making the middle not length of fixed part is 100 ± 5mm, with test specimens not fixed part be stretched to 130mm, repeat 5 times; At last, the variation of the decalcomania on two test specimens surfaces of range estimation evaluation according to the evaluation result of two test specimens, provides final conclusion for accepting or not accepting.
Further, the elastic extension of judging sample may further comprise the steps: cut (150 ± 5mm) * (40 ± 5mm) sample along the textile broadwise, its long limit is the textile weft direction, with the folding along its length seam of also respectively stepping in the two ends of sample, make two the seam between the distance be 100 ± 5mm, a seam is inserted metal bar, in addition on the weight of seam stuck-at-kg, the pull-up metal bar is mentioned weight, measure whether length reaches 130mm between two seams, if do not reach 130mm, then the elastic extension of sample is less than 30%; If meet or exceed 130mm, then the elastic extension of sample is more than or equal to 30%.
The method of testing of textile printing fastness provided by the invention, simple, be applicable to all kinds of printing textiles, the appraisal standards of an evaluation printing textile quality quality are provided for production firm both domestic and external and supplier.
Description of drawings
For can clearer understanding purpose of the present invention, characteristics and advantage, below with reference to accompanying drawing preferred embodiment of the present invention is described in detail, wherein:
Fig. 1 is the extension test first embodiment synoptic diagram among the present invention;
Fig. 2 is the extension test second embodiment synoptic diagram among the present invention.
Embodiment
Embodiment 1
Specimen: the knitting sample of the light blue tail band adularescent of flat pin decalcomania
1. acceleration washing test:
Cut the sample of two 150mm * 40mm along the sample broadwise, the color of two samples is identical with stamp, and its long limit is the sample weft direction, and one as test specimens, and another piece is sample as a comparison; Dissolving 4g does not contain the ECE standard wash agent (without phosphorus) of fluorescer in three grades of water of 1000ml, is configured to the wash solution that concentration is 4g/L; The rotary water bath device of GB/T12490-2007 standard is warming up to 40 ℃, with the jar that the above-mentioned wash solution of 150ml, 10 diameters stainless shot that is 6.0 ± 0.5mm and above-mentioned test specimens are put into the GB/T12490-2007 standard, described jar is put into described rotary water bath device; Start running 150 minutes; Washing is taken out described test specimens after finishing, and cleans twice respectively in three grades of water of 100ml, each one minute; Flushing is squeezed with hand and to be removed the excessive moisture of test specimens to clean in circulating water then, tiles in being no more than 60 ℃ air and dries; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, with self staining of GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes.
Change color:
Light blue bottom is 4-5 level (less than the 3-4 level for not accepting)
The white stamp is 4 grades (less than 3-4 levels for not accepting)
Self staining is 4-5 level (less than 4 grades for not accepting)
Surface physics changes:
There is slight frostwork phenomenon (there is tangible physical change on the surface for not accepting) on the test specimens surface
Conclusion is for accepting.
2. actual home washings test:
Get two samples that color is identical with stamp, one as test specimens, and another piece is sample as a comparison; Accompany washing to put into the tumbling-box washing machine of GB/T8629-2001 standard in test specimens and 21g family expenses ECE standard washing powder (without phosphorus) and 2kg, according to the wash conditions washing of table 1.
Table 1 wash conditions
| Wash temperature | ??40℃ |
| Washing procedure | ??5A |
| Washing times | 5 circulations |
After the washing, test specimens is taken out, baking is 90 minutes under 70 ℃ temperature, make its drying, then with the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, with self staining of GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes.
Change color:
Light blue bottom is 4-5 level (less than the 3-4 level for not accepting)
The white stamp is 4 grades (less than 3-4 levels for not accepting)
Self staining is 4-5 level (less than 4 grades for not accepting)
Surface physics changes:
There is slight frostwork phenomenon (there is tangible physical change on the surface for not accepting) on the test specimens surface
Conclusion is for accepting.
3. extension test:
Cut the sample of 150mm * 40mm in sample upper edge broadwise, with the folding along its length seam 11 of also respectively stepping in sample two ends, make between two seams apart from being 100mm, insert a metal bar 3 in the seam, insert another root metal bar 21 that connects on the 1kg weight 2 in the seam in addition, as shown in Figure 1.Upwards lift metal bar 3 to mention weight 2, the length of measuring test specimens 10 is stretched to 143mm, and promptly the elastic extension of sample is greater than 30%.
With the sample after the actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, carry out following operation respectively: the two ends of test specimens 10 are separately fixed on first fixture 41 and second fixture 42 of tensilometer 4, making the middle not length of fixed part is 100mm, as shown in Figure 2.By the handle on operation and the moving member 43 that second fixture 42 links to each other with in the middle of the test specimens 10 not fixed parts be stretched to 130mm, and then operation moving member 43 make test specimens 10 centres not fixed parts be returned to 100mm, repeat 5 times; The variation of the decalcomania on two test specimens surfaces of range estimation evaluation.
In addition, also can adopt this area stretcher commonly used that sample is carried out extension test, also can reach identical purpose.
Surface physics changes:
Two test specimens all do not return to original shape;
The printed surface of two test specimens all has tangible slight crack (test specimens does not return to original shape or visual slight crack arranged just for not accepting)
Conclusion is not for accepting.
Specimen: the lightpink tail band has the woven sample of the satin weave of peony decalcomania
1. acceleration washing test:
Cut the sample of two 155mm * 45mm along the sample broadwise, the color of two samples is identical with stamp, and its long limit is the sample weft direction, and one as test specimens, and another piece is sample as a comparison; The AATCC1993WOB standard wash agent of dissolving 4.1g is configured to the wash solution that concentration is 4g/L in three grades of water of 1005ml; The rotary water bath device of GB/T12490-2007 standard is warming up to 42 ℃, with the jar that the above-mentioned wash solution of 151ml, 10 diameters stainless shot that is 6.0 ± 0.5mm and above-mentioned test specimens are put into the GB/T12490-2007 standard, described jar is put into described rotary water bath device; Start running 160 minutes; Washing is taken out described test specimens after finishing, and cleans twice respectively in three grades of water of 100ml, each one minute; Flushing is squeezed with hand and to be removed the excessive moisture of test specimens to clean in circulating water then, tiles in being no more than 60 ℃ air and dries; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, with self staining of GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes.
Change color:
Lightpink bottom is 4-5 level (less than the 3-4 level for not accepting)
The peony stamp is 3-4 level (less than the 3-4 level for not accepting)
Self staining is 4-5 level (less than 4 grades for not accepting)
Surface physics changes:
There is slight frostwork phenomenon (there is tangible physical change on the surface for not accepting) on the test specimens surface
Conclusion is for accepting.
2. actual home washings test:
Get two samples that color is identical with stamp, one as test specimens, and another piece is sample as a comparison; Accompany washing to put into the agitator type washing machine of GB/T8629-2001 standard in test specimens and 66g family expenses AATCC 1993WOB standard washing powder and 2.1kg, according to the wash conditions washing of table 2.
Table 2 wash conditions
| Wash temperature | ??43℃ |
| Washing procedure | ??6B |
| Washing times | 5 circulations |
After the washing, test specimens is taken out, oven dry is 100 minutes under 60-80 ℃ of temperature, then with the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, with self staining of GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes.
Change color:
Lightpink bottom is 4-5 level (less than the 3-4 level for not accepting)
The peony stamp is 3-4 level (less than the 3-4 level for not accepting)
Self staining is 4-5 level (less than 4 grades for not accepting)
Surface physics changes:
There is slight frostwork phenomenon (there is tangible physical change on the surface for not accepting) on the test specimens surface
Conclusion is for accepting.
3. extension test:
Cut the sample of 150mm * 40mm in sample upper edge broadwise, with the folding along its length seam of also respectively stepping in sample two ends, make between two seams distance insert a metal bar in the seam for 100mm, insert another root metal bar that connects on the 1kg weight in the seam in addition.Upwards lift metal bar to mention weight, the length of measuring test specimens is stretched to 121mm, and promptly the elastic extension of test specimens is less than 30%.
With the sample after the described actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, the method operation that stretches according to above-mentioned weight respectively, upwards lift metal bar to mention weight and to continue 10 seconds, put down weight and make test specimens be returned to original length, repeat 5 times; The variation of the decalcomania on two test specimens surfaces of range estimation evaluation.
Surface physics changes:
Two test specimens all can return to original shape;
The printed surface of two test specimens does not all have tangible slight crack (test specimens does not return to original shape or visual slight crack arranged just for not accepting)
Conclusion is for accepting.
In sum, the method for testing of textile printing fastness provided by the invention, simple, be applicable to all kinds of printing textiles, the appraisal standards of an evaluation printing textile quality quality are provided for production firm both domestic and external and supplier.
Claims (11)
1. the method for testing of a textile printing fastness is characterized in that, described method of testing comprises:
Quicken washing test: sample and standard wash agent solution and steel ball are put into jar together, wash at the rotary water bath device; Washed samples; Dry sample; With gray scale evaluation sample change color, with self staining of standard rating staining with gray scale evaluation sample, the surface physics of range estimation evaluation sample changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results with the standard rating variable color;
Actual home washings test: with sample and washing powder, accompany washing to put into home-use washing machine washing; Dry sample; With gray scale evaluation sample change color, with self staining of standard rating staining with gray scale evaluation sample, the surface physics of range estimation evaluation sample changes, and provides conclusion for accepting or not accepting according to above-mentioned these three evaluation results with the standard rating variable color;
If the conclusion of described acceleration washing test and actual home washings test all is to accept, then carry out extension test: will speed up sample after washing and the actual home washings several that stretches respectively; The variation of range estimation evaluation specimen surface decalcomania according to the evaluation result of two samples, provides final conclusion for accepting or not accepting.
2. the method for testing of textile printing fastness according to claim 1, it is characterized in that, described acceleration washing test may further comprise the steps: cut two (150 ± 5mm) * (samples of 40 ± 5mm) along the textile broadwise, the color of described two samples is identical with stamp, its long limit is the textile weft direction, one as test specimens, and another piece is sample as a comparison; The standard wash agent of dissolving 4.0 ± 0.1g in three grades of water of 1000 ± 5ml is configured to the wash solution that concentration is 4g/L; The rotary water bath device of GB/T12490-2007 standard is warming up to 40 ± 2 ℃, with the jar that the described wash solution of 150 ± 1ml, 10 diameters stainless shot that is 6.0 ± 0.5mm and described test specimens are put into the GB/T12490-2007 standard, described jar is put into described rotary water bath device; Start running 150 ± 10 minutes; Take out described test specimens, it is dry to clean the back; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, self staining with GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results.
3. the method for testing of textile printing fastness according to claim 2, it is characterized in that: described standard wash agent is AATCC 1993 WOB standard wash agent or agent of ECE standard wash or the agent of IEC standard wash that does not contain fluorescer.
4. the method for testing of textile printing fastness according to claim 2 is characterized in that: the start running cleans twice after quickening the described test specimens of washing in three grades of water of 100ml, each one minute, and in circulating water flushing to clean.
5. the method for testing of textile printing fastness according to claim 1 is characterized in that, described actual home washings test may further comprise the steps: get two samples that color is identical with stamp, one as test specimens, and another piece is sample as a comparison; Accompany washing to put into the tumbling-box washing machine of GB/T8629-2001 standard GB/T 8629-2001 standard wash agent and the 2 ± 0.1kg of test specimens, 21 ± 2g, be set at the 5A washing procedure, 5 circulations of washing under 40 ± 3 ℃ water temperature; Take out described test specimens and dry; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, self staining with GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results.
6. the method for testing of textile printing fastness according to claim 5 is characterized in that: described standard wash agent is not for containing the agent of ECE standard wash or the agent of IEC standard wash of fluorescer.
7. the method for testing of textile printing fastness according to claim 1 is characterized in that, described actual home washings test may further comprise the steps: get two samples that color is identical with stamp, one as test specimens, and another piece is sample as a comparison; Accompany washing to put into the agitator type washing machine of GB/T8629-2001 standard GB/T 8629-2001 standard wash agent and the 2 ± 0.1kg of test specimens, 66 ± 2g, be set at the 6B washing procedure, under 40 ± 3 ℃ water temperature, wash 5 circulations with mode standard; Take out described test specimens and dry; With the change color of GB250-2008 evaluation variable color with gray scale contrast contrast sample evaluation test specimens, self staining with GB251-2008 grey scale for assessing staining of colour evaluation test specimens, the surface physics of range estimation evaluation test specimens changes, and provides conclusion for accepting or not accepting according to above-mentioned three evaluation results.
8. the method for testing of textile printing fastness according to claim 7, it is characterized in that: described standard wash agent is AATCC 1993WOB standard wash agent or ECE standard wash agent that does not contain fluorescer or the agent of IEC standard wash.
9. according to the method for testing of claim 5 or 7 described textile printing fastness, it is characterized in that: described drying steps is to dry under 60-80 ℃ temperature, up to drying.
10. the method for testing of textile printing fastness according to claim 1 is characterized in that, described extension test may further comprise the steps: tensile sample, the elastic extension of judgement sample; If the elastic extension of sample is less than 30%, with the sample after the described actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, carry out following operation respectively: the test specimens two ends are folding along its length, and respectively step on a seam, make two the seam between the distance be 100 ± 5mm, in the seam of two test specimens, insert metal bar, in addition on the weight of seam stuck-at-kg, the pull-up metal bar is mentioned weight and is continued 10 ± 1 seconds, repeats 5 times; If the elastic extension of sample is more than or equal to 30%, then with the sample after the described actual home washings along broadwise cut (150 ± 5mm) * (40 ± 5mm) as test specimens, sample after the described acceleration washing is as another test specimens, carry out following operation respectively: the two ends of test specimens are separately fixed on the stretching fixture, making the middle not length of fixed part is 100 ± 5mm, with test specimens not fixed part be stretched to 130mm, repeat 5 times; At last, the variation of the decalcomania on two test specimens surfaces of range estimation evaluation according to the evaluation result of two test specimens, provides final conclusion for accepting or not accepting.
11. the method for testing of textile printing fastness according to claim 10, it is characterized in that, the elastic extension of judging sample may further comprise the steps: cut (150 ± 5mm) * (40 ± 5mm) sample along the textile broadwise, its long limit is the textile weft direction, with the folding along its length seam of also respectively stepping in the two ends of sample, make two the seam between the distance be 100 ± 5mm, a seam is inserted metal bar, in addition on the weight of seam stuck-at-kg, the pull-up metal bar is mentioned weight, measure whether length reaches 130mm between two seams, if do not reach 130mm, then the elastic extension of sample is less than 30%; If meet or exceed 130mm, then the elastic extension of sample is more than or equal to 30%.
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