CN105133389A - Color fastness standard fabric for blue series in textile and application of color fastness standard fabric - Google Patents
Color fastness standard fabric for blue series in textile and application of color fastness standard fabric Download PDFInfo
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- CN105133389A CN105133389A CN201510596841.8A CN201510596841A CN105133389A CN 105133389 A CN105133389 A CN 105133389A CN 201510596841 A CN201510596841 A CN 201510596841A CN 105133389 A CN105133389 A CN 105133389A
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- 239000004744 fabric Substances 0.000 title claims abstract description 135
- 239000004753 textile Substances 0.000 title claims abstract description 52
- 238000004043 dyeing Methods 0.000 claims abstract description 61
- 229920000742 Cotton Polymers 0.000 claims abstract description 25
- 238000002360 preparation method Methods 0.000 claims abstract description 19
- 210000003296 saliva Anatomy 0.000 claims abstract description 17
- 239000000975 dye Substances 0.000 claims description 56
- 238000000034 method Methods 0.000 claims description 46
- 230000008569 process Effects 0.000 claims description 34
- 238000005406 washing Methods 0.000 claims description 29
- 238000012360 testing method Methods 0.000 claims description 19
- 239000000463 material Substances 0.000 claims description 17
- 239000011248 coating agent Substances 0.000 claims description 13
- 238000000576 coating method Methods 0.000 claims description 13
- 238000002203 pretreatment Methods 0.000 claims description 11
- 238000005554 pickling Methods 0.000 claims description 10
- 239000000985 reactive dye Substances 0.000 claims description 10
- 239000004902 Softening Agent Substances 0.000 claims description 9
- 239000007788 liquid Substances 0.000 claims description 8
- 238000010606 normalization Methods 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 7
- 241001062009 Indigofera Species 0.000 claims description 6
- 238000009835 boiling Methods 0.000 claims description 5
- 235000011194 food seasoning agent Nutrition 0.000 claims description 5
- 238000005517 mercerization Methods 0.000 claims description 5
- 239000000049 pigment Substances 0.000 claims description 5
- 229920001296 polysiloxane Polymers 0.000 claims description 5
- 238000005096 rolling process Methods 0.000 claims description 3
- 238000007781 pre-processing Methods 0.000 abstract description 7
- 238000001514 detection method Methods 0.000 abstract description 6
- 238000005516 engineering process Methods 0.000 abstract description 4
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- 239000000523 sample Substances 0.000 description 25
- 235000011121 sodium hydroxide Nutrition 0.000 description 16
- 238000010186 staining Methods 0.000 description 13
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 12
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 8
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 8
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- 230000008020 evaporation Effects 0.000 description 4
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- 238000009992 mercerising Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000000344 soap Substances 0.000 description 4
- 235000017550 sodium carbonate Nutrition 0.000 description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 description 4
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Abstract
The invention relates to color fastness standard fabric for blue series in textile and further relates to an application of the standard fabric in textile color fastness detection and rating. The standard fabric adopts cotton plain cloth as grey cloth and is prepared by adopting the following specific preparation method comprising steps of pre-processing and dyeing; according to the standard fabric, color fastness to rubbing relates to eight color fastness grades, color fastness to perspiration relates to four color fastness grades, and color fastness to saliva relates to four color fastness grades. The original grey card rating is converted into standard fabric comparison rating, the rating is more visual, subjective influence of a detection worker is reduced, and the accuracy rate of the detection is increased; through improvement of the technology of the standard fabric, the preparation process of the standard fabric is controllable, the color accuracy is high, and the application prospect is wide.
Description
Technical field
The invention belongs to textile inspection technical field, be specifically related to textile color stability blue series standard fabric and application thereof.
Background technology
Textile and garment enterprise occupies critical role in the economic development of China, in order to improve the core competitiveness of enterprise, needs the high-quality, the high added value that ensure fabric clothing.Textile color stability is one of important indicator evaluating properties of textile, the important Interventions Requested relating to consumer's health of human body, safety and sanitation, to this, standard GB/T 18401 has done Compulsory Feature, and therefore COLOR FASTNESS controls and seem in finished product inspection to be even more important in the quality of production of textiles.
Textile color stability mainly refers to the resistance of color to various effect in processing and use procedure on textiles, show the intensity that on fabric, auxiliary or goods, fiber is combined with dyestuff, the mensuration of COLOR FASTNESS carries out evaluating according to the variable color of sample and the staining of adjacent fabric.Textile color stability is divided into five ranks, nine grades (wherein crucial grade has 2/3,3,3/4,4 grade), the staining degree in staining COLOR FASTNESS paper examines process of the test in standard cotton cloth.In standard cotton cloth, staining is more shallow, and COLOR FASTNESS higher grade, then the COLOR FASTNESS of textiles is better; Otherwise COLOR FASTNESS is poorer.The detection of textile color stability, affect by very many-sided factor, comprise the oneself state etc. of reviewer to the selection of the technical merit of the process of sample, grading personnel, grading environmental condition, the evaluation analysis of process, the order of grading and reviewer, these all have very large relation with the experience of reviewer.
Current color fastness grading method comprises ocular estimate and instrumental method, because instrumental assessment can be subject to the restriction such as sample shape, configuration of surface, does not therefore extensively promote; The grading of traditional COLOR FASTNESS continues to use ocular estimate always.The statement that textiles rub resistance standard is graded to ocular estimate, without specific requirement, is all compare with reference to corresponding ash card.Inspector, by the range estimation to the change of sample color and luster, converts the sample variation of colour to gray scale difference, then compares with standard ash card, after comprehensive analysis, draw evaluation result.In this course, color conversion grey is graded by testing staff, because intuitive is too poor, there is certain mistaken ideas and risk, especially for the inspector just starting to learn.Cultivate a ripe testing staff, need the long period, grading person, when grading, also will avoid tired grading, and these objective and subjective factors are easy to the judgement just affecting inspector, cause evaluation result to produce very big error.So set up the standard fabric of a set of scientific, visual each grade of COLOR FASTNESS color series, to crack this puzzlement industry difficult problem for many years, improve the quality of China's textile inspection standard, strengthen the right of speech that China formulates standard, have realistic meaning energetically.
Development textile color stability standard sample has versatile: the COLOR FASTNESS grade that 1, can judge the textiles of similar colour system more intuitively, and be not only confined to grade to the sample of all colours with ash card, the difficulty of testing staff in ranking process can be reduced like this, handled easily, improves accuracy; 2, as the authentic specimen of digitlization rating system, can be the foundation of the quick ranking method of COLOR FASTNESS, lay a solid foundation.3, can be used as checkout procedure Quality Control standard specimen or examination standard specimen, in every fastness test process, use the COLOR FASTNESS standard sample of the similar colour system of known grades as Quality Control sample simultaneously, the standard sample of known grades and the grade of the actual standard sample detected is evaluated after off-test, whether consistent, thus judge the normalization of testing process, the accuracy of testing result.4, help factory better to carry out production process quality monitoring, ensure that the product dyeing of batch production is more even, reduce aberration.
Dyeing document relevant at present and production technology are all inquire into how to contaminate better by every COLOR FASTNESS of textiles usually, for research or the blank of the standard fabric of development different brackets.And want the color standard stained clot-h just obtaining certain grade, comparatively strict control must be carried out to dyeing.
Summary of the invention
For the defect that prior art exists, the technical problem that the present invention solves be to provide can visual inspection blue series textile color stability, improve the standard fabric of Detection accuracy, its preparation process is controlled, standard fabric precision is high, provide simultaneously its textile color stability detect in application.
The technical scheme that the present invention solves the employing of its technical problem is:
A kind of textile color stability blue series standard fabric, it is with cotton plain for grey cloth, and adopt following preparation method to obtain, concrete preparation method comprises:
Step (1) pre-treatment: grey cloth carries out boiling drift, singing and mercerization finish;
Step (2) dyes: adopt active blue dyestuff to carry out the dyeing of variable concentrations.
Concrete, described cotton plain is density is 14*14/60*60, and brute force is 673N*687N, and grammes per square metre is 232g/m
2;
Concrete, described in boil drift through first time mangle, first time decatize, first time washing, second time mangle, second time decatize, second time washing, to dry, described first time mangle select caustic soda 50g/L, refining agent 888g/L, chelated dispersants 5103g/L; Described first time, decatize was 100 DEG C of decatize 60min; Described first time washing selects 85 DEG C to wash 4 lattice; Described second time mangle selects hydrogen peroxide 6g/L, refining agent 883g/L, chelated dispersants 5g/L, stabilizing agent 10g/L; Described second time decatize is 100 DEG C of decatize 60min; Described second time washing selects 85 DEG C to wash 4 lattice.
Concrete, described in singe and respectively the obverse and reverse of cotton plain carried out, speed of a motor vehicle 75m/min, burner is high 2 centimetres, adopt gasoline vaporizer to make fuel evaporation and and air be mixed into the combustion material of singing.
Concrete, described mercerising adopts caustic soda 210g/L-220g/L to carry out mangle, then washes, and 80 DEG C-90 DEG C washing 6 lattice, then dry.
Further, step carries out sanding process after (1), then carries out step (2) dyeing; The described sanding speed of a motor vehicle is 22m/min, pressure 1.2Kg, tension force 21Kg.
Further, step carries out Final finishing after (2), and described Final finishing is soft treatment, is specially softening agent and carries out mangle, then oven dry, anti-shrinking, and described soft treatment selects hydrophilic silicone softening agent, preferred softener CGF.
Further, described step (2) dyeing for continous mode dyeing, comprise roll material, oven dry, fixation, decatize, washing are soaped, pickling, mistake padding machine and oven dry processing step; The blue S-G of REACTIVE DYES selected by the described material that rolls, control liquid carrying rate 65%, infrared baking is to containing tide 5%, fixation selects salt, soda ash and caustic soda to process, described decatize adopts 100 DEG C of decatize 60s, washing is soaped and is selected soap lye ZS990.5g/L, and it is 6.5-7.5 that described pickling selects acetic acid to control sample cloth pH.
Further, described step (2) dyeing select pigment dyeing technique, select coating indigo plant to carry out rolling material, after carry out hot-air seasoning, cropping; Described coating indigo plant selects the blue FFG of coating, as the blue FFG of coating that Hua Da coating Co., Ltd produces, controls liquid carrying rate 65%; Described hot-air seasoning is to containing tide 5%.
The present invention provides the described application of textile color stability blue series standard fabric in colour fastness to rubbing detects and grades simultaneously, and standard fabric is concrete preparation method comprise: pre-treatment, dyeing, Final finishing; When described dyeing adopts continous mode to dye, preparation comprises sanding process, dyestuff selects 1.5 successively, 8,20,30,40,80g/L concentration, make dyeing described in 1-6 standard fabric when adopting pigment dyeing technique, dyestuff select 6 and 15g/L concentration make 7 and No. 8 standard fabric; Described 1-8 standard fabric respectively corresponding resistance to dry friction COLOR FASTNESS 4-5,4,3-4,3,2-3,2,1-2,1 grade, respectively corresponding moisture-proof colorfastness to rubbing 4,3,2,1-2,1-2,1,1,1 grade, carry out sample comparison grading and the examination of testing process normalization.
The present invention provides the described application of textile color stability blue series standard fabric in colour fastness to perspiration detects and grades simultaneously, the concrete preparation method of standard fabric is: pre-treatment, continous mode dyeing and Final finishing, wherein during continous mode dyeing dyestuff select 18 successively, 30,40,60g/L concentration, make standard fabric, be corresponding in turn to colour fastness to perspiration 4,3-4,3,2-3 grade carry out sample comparison grading and testing process normalization examination.
The present invention provides the described application of textile color stability blue series standard fabric in resistance to saliva COLOR FASTNESS detects and grades simultaneously, the concrete preparation method of standard fabric is: pre-treatment, continous mode dyeing and Final finishing, wherein during continous mode dyeing dyestuff select 20 successively, 35,40,65g/L concentration, make standard fabric, be corresponding in turn to resistance to saliva COLOR FASTNESS 4,3-4,3,2-3 grade, carry out sample comparison grading and testing process normalization examination.
Beneficial effect of the present invention is:
(1) the present invention selects cotton plain as grey cloth, and surfacing, ABRASION RESISTANCE is good, and easy dyeing is even.
(2) existing sanding technology is used for the touch comfort level improving fabric, the present invention utilizes sanding treatment process, reach beyond thought effect, the increase that fabric face amasss on the one hand causes the dyestuff being adsorbed on fabric face during dyeing to increase, and forms more loose colour; The villus fiber of fabric face is elongated on the other hand, and add the resistance of friction when rub resistance is tested, so more easily make the dyestuff on DYED FABRICS surface be transferred on standard calico, double action causes the decline of the COLOR FASTNESS of sanded cloth.
(3) along with dye strength increases, COLOR FASTNESS grade decreases, the present invention obtains the standard items of different brackets by the concentration controlling dyestuff, the color of standard fabric is subject to the impact of technological parameter, its interact relation is very complicated, the present invention determines required processing step, the parameter adopted of each standard fabric accurately, especially carries out quantitatively to dye strength, the comparison standard items when COLOR FASTNESS standard fabric obtaining different brackets is identified as COLOR FASTNESS.
(4) uniformity of textile dyeing obviously can be improved through soft Final finishing, especially uneven phenomenon can be improved, this may be due in soft last handling process, and the dye well dyeing assistant being adsorbed on fabric face once distributes under hygrometric state state again, makes dyeing become more even.
(5) in addition, after soft treatment, fabric color fastness all increases than the result without soft treatment.This is because one side energy removal part in soft treatment process sticks in the loose colour of fabric face, softener has certain lubrication on the other hand, the smoothness of fabric can be improved, fabric face coefficient of friction can be reduced when friction test, thus minimizing some dyes comes off, and makes colour fastness to rubbing to improve.
The grading of original ash card is converted into the standard fabric comparison grading that the present invention obtains by the present invention, detects more directly perceived, is subject to tester's subjective impact and reduces, improve Detection accuracy; The present invention also can be applicable to the examination of various COLOR FASTNESS testing process normalization.The technique of this standard fabric is through improving, and its preparation process is controlled, color accuracy is high, and application prospect is extensive.
Detailed description of the invention
For enabling above-mentioned purpose of the present invention, feature and advantage become apparent more, below in conjunction with the detailed description of the invention in the embodiment of the present invention, technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
embodiment 1 textiles colour fastness to rubbing blue series standard fabric and application thereof
Embodiment 1 textiles colour fastness to rubbing blue series standard fabric, chooses 1-8 sample cloth, and it for grey cloth, adopts following concrete preparation method to obtain with cotton plain:
Step (1) pre-treatment: grey cloth carries out boiling drift, singing and mercerization finish;
Described cotton plain is density is 14*14/60*60, and brute force is 673N*687N, and grammes per square metre is 232g/m
2, specifically select the textile plain that Nantong Rui Rui contains;
Described boil drift through first time mangle, first time decatize, first time washing, second time mangle, second time decatize, second time washing, to dry, described first time mangle select caustic soda 50g/L, refining agent 888g/L, chelated dispersants 5103g/L; Described first time, decatize was 100 DEG C of decatize 60min; Described first time washing selects 85 DEG C to wash 4 lattice; Described second time mangle selects hydrogen peroxide 6g/L, refining agent 883g/L, chelated dispersants 5g/L, stabilizing agent 10g/L; Described second time decatize is 100 DEG C of decatize 60min; Described second time washing selects 85 DEG C to wash 4 lattice;
Described singing is carried out the obverse and reverse of cotton plain respectively, speed of a motor vehicle 75m/min, and burner is high 2 centimetres, adopt gasoline vaporizer make fuel evaporation and and air be mixed into the combustion material of singing;
Described mercerising adopts caustic soda 210g/L-220g/L to carry out mangle, then 80 DEG C-90 DEG C washing 6 lattice, post-drying;
The pre-processing device that pre-processing device selects Xinchang, Zhejiang Province dyeing machine Co., Ltd to produce.
Step (2) sanding, 1-6 sample cloth carries out sanding process, and the described sanding speed of a motor vehicle is 22m/min, pressure 1.2Kg, tension force 21Kg, and described roughing process selects Zhangjiagang to build the LAM018-180 type roughing-up machine of industry dyeing machine; 7-8 sample cloth is without sanding process.
Step (3) dyes: adopt active blue dyestuff to carry out the dyeing of variable concentrations.
No. 1-6, sample cloth adopts continous mode dyeing, comprise roll material, oven dry, fixation, decatize, washing are soaped, pickling, mistake padding machine and oven dry processing step; The blue S-G of REACTIVE DYES selected by the described material that rolls, the lot number specifically selecting Hentsman company to produce is the reactive blue S-G dyestuff of 0029722100, control liquid carrying rate 65%, dye strength is followed successively by 1.5,8,20,30,40,80g/L, infrared baking is to containing tide 5%, and fixation selects salt, soda ash and caustic soda to process, and described decatize adopts 100 DEG C of decatize 60s, washing is soaped and is selected soap lye ZS990.5g/L, and it is 6.5-7.5 that described pickling selects acetic acid to control sample cloth pH;
No. 7-8, sample cloth adopt pigment dyeing technique, select coating indigo plant to carry out rolling material, after carry out hot-air seasoning, cropping; Described coating indigo plant selects the blue FFG of coating, as the blue FFG of coating that Hua Da coating Co., Ltd produces, controls liquid carrying rate 65%; Described hot-air seasoning is to containing tide 5%; Coating concentration selects 6 and 15g/L successively.
Step (4) Final finishing: described Final finishing is soft treatment, be specially softening agent and carry out mangle, then oven dry, anti-shrinking, described soft treatment selects hydrophilic silicone softening agent, preferred softener CGF, as the softener CGF that Hua Da helps dye chemical plant to produce.
Through above process, obtain 1-8 standard fabric, the dry of stained clot-h is measured respectively with reference to GB/T3920-2008 " textile color stability test colour fastness to rubbing ", wet friction, and evaluate the dry friction of friction cloth and the staining progression of wet friction COLOR FASTNESS with " GB/T251-2008 textile color stability test evaluation staining gray scale ", described 1-8 standard fabric is corresponding resistance to dry friction COLOR FASTNESS 4-5 respectively, 4, 3-4, 3, 2-3, 2, 1-2, 1 grade, corresponding moisture-proof colorfastness to rubbing 4 respectively, 3, 2, 1-2, 1-2, 1, 1, 1 grade, appraiser can carry out sample identify according to this standard fabric.
embodiment 2 textiles colour fastness to perspiration blue series standard fabric and application thereof
Embodiment 2 textiles colour fastness to perspiration blue series standard fabric, chooses 1-4 sample cloth, and it for grey cloth, adopts following concrete preparation method to obtain with cotton plain:
Step (1) pre-treatment: grey cloth carries out boiling drift, singing and mercerization finish;
Described cotton plain is density is 14*14/60*60, and brute force is 673N*687N, and grammes per square metre is 232g/m
2, specifically select the textile plain that Nantong Rui Rui contains;
Described boil drift through first time mangle, first time decatize, first time washing, second time mangle, second time decatize, second time washing, to dry, described first time mangle select caustic soda 50g/L, refining agent 888g/L, chelated dispersants 5103g/L; Described first time, decatize was 100 DEG C of decatize 60min; Described first time washing selects 85 DEG C to wash 4 lattice; Described second time mangle selects hydrogen peroxide 6g/L, refining agent 883g/L, chelated dispersants 5g/L, stabilizing agent 10g/L; Described second time decatize is 100 DEG C of decatize 60min; Described second time washing selects 85 DEG C to wash 4 lattice;
Described singing is carried out the obverse and reverse of cotton plain respectively, speed of a motor vehicle 75m/min, and burner is high 2 centimetres, adopt gasoline vaporizer make fuel evaporation and and air be mixed into the combustion material of singing;
Described mercerising adopts caustic soda 210g/L-220g/L to carry out mangle, and then 80 DEG C-90 DEG C washing 6 lattice, then dry;
The pre-processing device that pre-processing device selects Xinchang, Zhejiang Province dyeing machine Co., Ltd to produce.
Step (2) dyes: adopt active blue dyestuff to carry out the dyeing of variable concentrations;
No. 1-4, sample cloth adopts continous mode dyeing, comprise roll material, oven dry, fixation, decatize, washing are soaped, pickling, mistake padding machine and oven dry processing step; The blue S-G of REACTIVE DYES selected by the described material that rolls, the lot number specifically selecting Hentsman company to produce is the reactive blue S-G dyestuff of 0029722100, liquid carrying rate 65%, dye strength is followed successively by 18,30,40,60g/L, infrared baking is to containing tide 5%, and fixation selects salt, soda ash and caustic soda to process, and described decatize adopts 100 DEG C of decatize 60s, washing is soaped and is selected soap lye ZS990.5g/L, and it is 6.5-7.5 that described pickling selects acetic acid to control sample cloth pH.
Step (3) Final finishing: described Final finishing is soft treatment, be specially softening agent and carry out mangle, then oven dry, anti-shrinking, described soft treatment selects hydrophilic silicone softening agent, preferred softener CGF, as the softener CGF that Hua Da helps dye chemical plant to produce.
Through above process, obtain 1-4 standard fabric, the colour fastness to perspiration of stained clot-h is measured with reference to GB/T3922-2013 " textile color stability test colour fastness to perspiration ", and the cotton staining progression of colour fastness to perspiration is evaluated with " GB/T251-2008 textile color stability test evaluation staining gray scale ", 1-4 standard fabric be corresponding in turn to colour fastness to perspiration 4,3-4,3,2-3 grade, appraiser can carry out sample identify according to this standard fabric, specifically comprises the cotton staining COLOR FASTNESS of resistance to sweat stain and the cotton staining COLOR FASTNESS of sweat proof acid.
embodiment 3 saliva of textile COLOR FASTNESS blue series standard fabric and application thereof
Embodiment 3 saliva of textile COLOR FASTNESS blue series standard fabric, chooses 1-4 sample cloth, and it for grey cloth, adopts following concrete preparation method to obtain with cotton plain:
Step (1) pre-treatment: grey cloth carries out boiling drift, singing and mercerization finish;
Described cotton plain is density is 14*14/60*60, and brute force is 673N*687N, and grammes per square metre is 232g/m
2, specifically select the textile plain that Nantong Rui Rui contains;
Described boil drift through first time mangle, first time decatize, first time washing, second time mangle, second time decatize, second time washing, to dry, described first time mangle select caustic soda 50g/L, refining agent 888g/L, chelated dispersants 5103g/L; Described first time, decatize was 100 DEG C of decatize 60min; Described first time washing selects 85 DEG C to wash 4 lattice; Described second time mangle selects hydrogen peroxide 6g/L, refining agent 883g/L, chelated dispersants 5g/L, stabilizing agent 10g/L; Described second time decatize is 100 DEG C of decatize 60min; Described second time washing selects 85 DEG C to wash 4 lattice.
Described singing is carried out the obverse and reverse of cotton plain respectively, speed of a motor vehicle 75m/min, burner height 2cm, adopt gasoline vaporizer make fuel evaporation and and air be mixed into the combustion material of singing.
Described mercerising adopts caustic soda 210g/L-220g/L to carry out mangle, and then 80 DEG C-90 DEG C washing 6 lattice, dry;
The pre-processing device that pre-processing device selects Xinchang, Zhejiang Province dyeing machine Co., Ltd to produce.
Step (2) dyes: adopt active blue dyestuff to carry out the dyeing of variable concentrations;
No. 1-4, sample cloth adopts continous mode dyeing, comprise roll material, oven dry, fixation, decatize, washing are soaped, pickling, mistake padding machine and oven dry processing step; The blue S-G of REACTIVE DYES selected by the described material that rolls, the lot number specifically selecting Hentsman company to produce is the reactive blue S-G dyestuff of 0029722100, liquid carrying rate 65%, dye strength is followed successively by 20,35,40,65g/L, infrared baking is to containing tide 5%, and fixation selects salt, soda ash and caustic soda to process, and described decatize adopts 100 DEG C of decatize 60s, washing is soaped and is selected soap lye ZS990.5g/L, and it is 6.5-7.5 that described pickling selects acetic acid to control sample cloth pH.
Step (3) Final finishing: described Final finishing is soft treatment, be specially softening agent and carry out mangle, then oven dry, anti-shrinking, described soft treatment selects hydrophilic silicone softening agent, preferred softener CGF, as the softener CGF that Hua Da helps dye chemical plant to produce.
Through above process, obtain 1-4 standard fabric, the resistance to saliva COLOR FASTNESS of stained clot-h is measured with reference to GB/T18886-2002 " textile color stability tests resistance to saliva COLOR FASTNESS ", and the cotton staining progression of resistance to saliva COLOR FASTNESS is evaluated with " GB/T251-2008 textile color stability test evaluation staining gray scale ", 1-4 mark be corresponding in turn to resistance to saliva COLOR FASTNESS 4,3-4,3,2-3 grade, appraiser can carry out sample identify according to this standard fabric.
experimental example 1 dyes base cloth sanding preliminary treatment to the impact of colour fastness to rubbing
Select the blue S-G of REACTIVE DYES, dye liquor concentration is that 20g/L carries out dyeing and soft Final finishing to sanding and the cotton plain of non-sanding, get six representative positions of stained clot-h and carry out resistance to dry, wet friction COLOR FASTNESS test, investigate sanding preliminary treatment and the difference without the pretreated stained clot-h colour fastness to rubbing of sanding respectively, manually grade under standard sources, the results are shown in Table 1.
Known by table 1, be starkly lower than without the pretreated result of sanding through the pretreated resistance to dry wet friction COLOR FASTNESS of sanding.The staining mechanism of textiles colour fastness to rubbing, mainly makes the dyestuff of the non-set of fabric face directly be transferred to standard calico causes under the effect of friction mechanism power.So fabric is after sanding process, the increase that fabric face amasss on the one hand causes the dyestuff being adsorbed on fabric face during dyeing to increase, and forms more loose colour; The villus fiber of fabric face is elongated on the other hand, and add the resistance of friction when rub resistance is tested, so more easily make the dyestuff on DYED FABRICS surface be transferred on standard calico, double action causes the decline of the colour fastness to rubbing of sanded cloth.So can consider to use sanded cloth for the standard fabric dyeing lower grade colour fastness to rubbing.
experimental example 2 dye strength is on the impact of stained clot-h colour fastness to rubbing
Select the blue S-G of REACTIVE DYES, dyestuff dye liquor concentration is respectively 5g/L, 10g/L, 20g/L, 40g/L, 60g/L carry out dyeing and soft post processing to the cotton plain of sanding, and the center position getting stained clot-h carries out colour fastness to perspiration test, investigate the impact of different dye liquor concentration on colour fastness to perspiration, the results are shown in Table 2.
Dye strength is larger on the impact of Fabrics Dyed with Reactive Dyes COLOR FASTNESS.The dye strength colour fastness to perspiration of 5g/L is 5 grades, along with the continuous increase of dye strength, when not changing other techniques of dyeing, the colour fastness to perspiration of fabric can constantly reduce, when dye strength reaches 60g/L, the colour fastness to perspiration of fabric is only 2-3 level.This is because dye strength used is higher, the probability forming loose colour in fabric face accumulation is larger, thus reduces the COLOR FASTNESS of DYED FABRICS.
By testing discovery above, the standard items of the COLOR FASTNESS dyeing different brackets can be controlled by the concentration changing dyestuff.
the soft Final finishing of experimental example 3 is on the impact of stained clot-h colour fastness to rubbing
Select the blue S-G of REACTIVE DYES, dye liquor concentration is that 40g/L dyes to cotton plain, dyeing later half cloth specimen does not do soft Final finishing, second half cloth specimen carries out soft Final finishing, two kinds of cloth specimens are got six representative positions respectively and does the experiment of resistance to saliva COLOR FASTNESS, investigate the difference without soft Final finishing and the resistance to saliva COLOR FASTNESS of stained clot-h through soft Final finishing, manually grade under standard sources, the results are shown in Table 3.
Known by table 3, uneven without each position of soft treatment fabric resistance to saliva COLOR FASTNESS, after soft treatment, the resistance to saliva COLOR FASTNESS of fabric six positions are even, are 3 grades.The uniformity obviously can improving textile dyeing through soft Final finishing is described, this may be due in soft last handling process, and the dye well dyeing assistant being adsorbed on fabric face once distributes under hygrometric state state again, makes dyeing become more even.
In addition, after soft treatment, fabric saliva COLOR FASTNESS increases than the result without soft treatment.This is because energy removal part sticks in the loose colour of fabric face in soft treatment process, resistance to saliva COLOR FASTNESS can be improved.
To sum up can obtain:
(1) be starkly lower than without the pretreated COLOR FASTNESS of sanding through the pretreated resistance to dry wet friction COLOR FASTNESS of sanding, so use sanded cloth as base cloth in the process of development COLOR FASTNESS standard fabric, its dyeing relatively easily controls, and more easily obtains the especially low-grade colour fastness to rubbing standard fabric of different brackets.
(2) along with dye strength increases, festness ratings decreases.The rub resistance standard items of different brackets can be obtained by the concentration controlling dyestuff.
(3) the soft Final finishing of DYED FABRICS can improve the uniformity of REACTIVE DYES to cotton dyeing, and can improve the grade of COLOR FASTNESS to a certain extent.Uniformity and the stability of standard fabric can be improved by increasing soft Final finishing.
Claims (8)
1. a textile color stability blue series standard fabric, is characterized in that, it is with cotton plain for grey cloth, and adopt following preparation method to obtain, concrete preparation method comprises:
Step (1) pre-treatment: grey cloth carries out boiling drift, singing and mercerization finish;
Step (2) dyes: adopt active blue dyestuff or coating to carry out the dyeing of variable concentrations.
2. textile color stability blue series standard fabric according to claim 1, is characterized in that, step carries out sanding process after (1), then carries out step (2) dyeing.
3. textile color stability blue series standard fabric according to claim 1 and 2, is characterized in that, step carries out Final finishing after (2), and described Final finishing is soft treatment, and described soft treatment selects hydrophilic silicone softening agent.
4. textile color stability blue series standard fabric according to claim 3, it is characterized in that, described step (2) dyeing for continous mode dyeing, comprise roll material, oven dry, fixation, decatize, washing are soaped, pickling, mistake padding machine and oven dry processing step; The described material that rolls selects the blue S-G of REACTIVE DYES, liquid carrying rate 65%, and described decatize adopts 100 DEG C of decatize 60s, and it is 6.5-7.5 that described pickling controls sample cloth pH.
5. textile color stability blue series standard fabric according to claim 3, is characterized in that, described step (2) dyeing select pigment dyeing technique, select coating indigo plant to carry out rolling material, after carry out hot-air seasoning, cropping; Described coating indigo plant selects the blue FFG of coating, liquid carrying rate 65%.
6. the application of the textile color stability blue series standard fabric described in claim 4 or 5 in colour fastness to rubbing detects and grades, it is characterized in that, standard fabric is concrete preparation method comprise: pre-treatment, dyeing and Final finishing; When described dyeing adopts continous mode dyeing, preparation comprises sanding process, dyestuff selects 1.5 successively, 8,20,30,40,80g/L concentration, make 1-6 standard fabric; When described dyeing adopts pigment dyeing technique, dyestuff select 6 and 15g/L concentration make 7 and No. 8 standard fabric; Described 1-8 standard fabric respectively corresponding resistance to dry friction COLOR FASTNESS 4-5,4,3-4,3,2-3,2,1-2,1 grade, respectively corresponding moisture-proof colorfastness to rubbing 4,3,2,1-2,1-2,1,1,1 grade, carry out sample comparison grading and the examination of testing process normalization.
7. the application of textile color stability blue series standard fabric according to claim 4 in colour fastness to perspiration detects and grades, it is characterized in that, the concrete preparation method of standard fabric is: pre-treatment, continous mode dyeing and Final finishing, wherein during continous mode dyeing dyestuff select 18 successively, 30,40,60g/L concentration, make standard fabric, be corresponding in turn to colour fastness to perspiration 4,3-4,3,2-3 grade carry out sample comparison grading and testing process normalization examination.
8. the application of textile color stability blue series standard fabric according to claim 4 in resistance to saliva COLOR FASTNESS detects and grades, it is characterized in that, the concrete preparation method of standard fabric is: pre-treatment, continous mode dyeing and Final finishing, wherein during continous mode dyeing dyestuff select 20 successively, 35,40,65g/L concentration, make standard fabric, be corresponding in turn to resistance to saliva COLOR FASTNESS 4,3-4,3,2-3 grade, carry out sample comparison grading and testing process normalization examination.
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