CN101848904B - 生产ε-己内酯的方法 - Google Patents

生产ε-己内酯的方法 Download PDF

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Publication number
CN101848904B
CN101848904B CN200880114782.4A CN200880114782A CN101848904B CN 101848904 B CN101848904 B CN 101848904B CN 200880114782 A CN200880114782 A CN 200880114782A CN 101848904 B CN101848904 B CN 101848904B
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CN
China
Prior art keywords
caprolactone
mixture
cyclisation
preparation purity
carried out
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN200880114782.4A
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English (en)
Chinese (zh)
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CN101848904A (zh
Inventor
R·平科斯
G-D·特贝恩
T·克鲁格
T·西尔希
T·C·斯彭格曼
S·贝如恩
J·T·安德烈斯
T·嘉西洛夫斯基
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BASF SE
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BASF SE
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Publication of CN101848904B publication Critical patent/CN101848904B/zh
Expired - Fee Related legal-status Critical Current
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D313/00—Heterocyclic compounds containing rings of more than six members having one oxygen atom as the only ring hetero atom
    • C07D313/02—Seven-membered rings
    • C07D313/04—Seven-membered rings not condensed with other rings

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrane Compounds (AREA)
CN200880114782.4A 2007-11-05 2008-10-28 生产ε-己内酯的方法 Expired - Fee Related CN101848904B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US98542407P 2007-11-05 2007-11-05
US60/985,424 2007-11-05
PCT/EP2008/064608 WO2009059913A1 (de) 2007-11-05 2008-10-28 VERFAHREN ZUR HERSTELLUNG ε-CAPROLACTON

Publications (2)

Publication Number Publication Date
CN101848904A CN101848904A (zh) 2010-09-29
CN101848904B true CN101848904B (zh) 2013-05-01

Family

ID=40303445

Family Applications (1)

Application Number Title Priority Date Filing Date
CN200880114782.4A Expired - Fee Related CN101848904B (zh) 2007-11-05 2008-10-28 生产ε-己内酯的方法

Country Status (7)

Country Link
US (1) US8247580B2 (enExample)
EP (1) EP2217587B1 (enExample)
JP (1) JP5453289B2 (enExample)
KR (1) KR20100088691A (enExample)
CN (1) CN101848904B (enExample)
CA (1) CA2703828A1 (enExample)
WO (1) WO2009059913A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8466299B2 (en) * 2008-12-05 2013-06-18 Basf Se Process for preparing delta-valerolactone in the gas phase
WO2010066674A2 (de) 2008-12-09 2010-06-17 Basf Se Verfahren zur herstellung von polymethylolen
US8575401B2 (en) 2008-12-09 2013-11-05 Basf Se Method for purifying crude polymethylols
US20120101009A1 (en) * 2008-12-18 2012-04-26 Invista North America S.A.R.L. Cyclohexane oxidation process byproduct stream derivatives and methods for using the same
EP2385933B1 (de) 2009-01-12 2014-06-25 Basf Se Verfahren zur herstellung von polymethylolen
EP2384344B1 (en) * 2009-01-30 2019-10-16 INVISTA Textiles (U.K.) Limited Aromatic polyesterpolyols, isocyanuratemodified polyurethane foams, and methods of making them
CA2755698A1 (en) 2009-04-07 2010-10-14 Basf Se Method for producing 1,6-hexanediol and caprolactone
JP5586686B2 (ja) 2009-04-07 2014-09-10 ビーエーエスエフ ソシエタス・ヨーロピア １，６−ヘキサンジオールの製造方法
EP2614056B1 (de) * 2010-09-08 2014-07-23 Basf Se Verfahren zur herstellung von epsilon-caprolacton und 1,6-hexandiol
US11208394B2 (en) 2018-09-17 2021-12-28 Regents Of The University Of Minnesota Chemical process to manufacture branched-caprolactone
CN111995612A (zh) * 2020-08-24 2020-11-27 青岛科技大学 一种己内酯的合成方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1140184A (en) * 1967-06-13 1969-01-15 Chisso Corp Process for manufacturing e-caprolactone
WO1997031883A1 (de) * 1996-03-01 1997-09-04 Basf Aktiengesellschaft Verfahren zur herstellung von 1,6-hexandiol und caprolacton
DE10100552A1 (de) * 2001-01-09 2002-07-11 Basf Ag Verfahren und Vorrichtung zur destillativen Aufarbeitung von 1,6-Hexandiol, 1,5-Pentandiol ung Caprolacton
DE10308489A1 (de) * 2003-02-26 2004-09-09 Basf Ag Verfahren zur Herstellung von Cyclopentanon und Caprolacton aus Dicarbonsäure-Lösung

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB140184A (en) * 1919-02-22 1920-03-25 Thomas Stanislaus Fildes Improvements in or relating to hot water cylinders
DE3823213A1 (de) 1988-07-08 1990-01-11 Basf Ag Verfahren zur herstellung von caprolacton
DE19744400A1 (de) * 1997-10-08 1999-04-15 Bayer Ag Verfahren zur Herstellung von Triazolinthion-Derivaten
DE19750532A1 (de) * 1997-11-14 1999-05-20 Basf Ag Verfahren zur Herstellung von 1,6-Hexandiol und 6-Hydroxycapronsäure bzw. deren Estern

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1140184A (en) * 1967-06-13 1969-01-15 Chisso Corp Process for manufacturing e-caprolactone
WO1997031883A1 (de) * 1996-03-01 1997-09-04 Basf Aktiengesellschaft Verfahren zur herstellung von 1,6-hexandiol und caprolacton
DE10100552A1 (de) * 2001-01-09 2002-07-11 Basf Ag Verfahren und Vorrichtung zur destillativen Aufarbeitung von 1,6-Hexandiol, 1,5-Pentandiol ung Caprolacton
DE10308489A1 (de) * 2003-02-26 2004-09-09 Basf Ag Verfahren zur Herstellung von Cyclopentanon und Caprolacton aus Dicarbonsäure-Lösung

Also Published As

Publication number Publication date
JP2011503021A (ja) 2011-01-27
CN101848904A (zh) 2010-09-29
EP2217587B1 (de) 2015-09-23
WO2009059913A1 (de) 2009-05-14
CA2703828A1 (en) 2009-05-14
KR20100088691A (ko) 2010-08-10
US8247580B2 (en) 2012-08-21
US20100240913A1 (en) 2010-09-23
EP2217587A1 (de) 2010-08-18
JP5453289B2 (ja) 2014-03-26

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SE01 Entry into force of request for substantive examination
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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130501

Termination date: 20171028