CN101845338A - High-efficiency oil-saving agent, preparation method and application thereof - Google Patents
High-efficiency oil-saving agent, preparation method and application thereof Download PDFInfo
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- CN101845338A CN101845338A CN 201010177993 CN201010177993A CN101845338A CN 101845338 A CN101845338 A CN 101845338A CN 201010177993 CN201010177993 CN 201010177993 CN 201010177993 A CN201010177993 A CN 201010177993A CN 101845338 A CN101845338 A CN 101845338A
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Abstract
The invention discloses a high-efficiency oil-saving agent, a preparation method and the application thereof. The high-efficiency oil-saving agent comprises 0.05-2.0% of fluorenone compound, 0.05-2.0% of nitrotoluene, 80-99.5% of camphor, 0.3-12% of borneol and balance low-grade fatty alcohol. The preparation method of the high-efficiency oil-saving agent comprises the steps of: completely dissolving the fluorenone compound and the nitrotoluene into the low-grade fatty alcohol, then fully mixing the camphor and the borneol, and obtaining the high-efficiency oil-saving agent. When being added into fuel oil, the high-efficiency oil-saving agent has the oil-saving rate reaching up to 30%. As metal salt is not used as an active agent in the high-efficiency oil-saving agent, residues are not left after the fuel oil is fully burnt, and the service life of an engine can be prolonged; the high-efficiency oil-saving agent is solid additive, thus being convenient for transportation and storage, easily dissolved into the fuel oil and low in adding proportion, and not changing the physical property of the fuel oil; and furthermore, the high-efficiency oil-saving agent is safe and can improve the antiknock property. The invention has simple preparation method and low cost, and is wide in application prospect.
Description
Technical field
The invention belongs to petrochemical industry, particularly a kind of high-efficiency oil-saving agent and preparation method thereof and application.
Background technology
The world today is along with the develop rapidly of transportation, and is more and more higher with the demand of oil to transport facility.Yet the non-renewable and present reserves of oil of petroleum resources is day by day exhausted, and the sharp increase of automobile pollution and turnout, and transport facility was becoming tight with oil day.How effectively to improve the efficiencies of combustion in oil engine such as gasoline, diesel oil, save fuel oil, become one of hot spot technology of competitively studying countries in the world.In fuel oil, add oil-saving agent, simple and effective, receive common people's concern, both at home and abroad to the existing relevant research work of oil-saving additive, mainly comprise following several: (1) adds metal-salt as activeconstituents in fuel oil, is a current important class oil-saving agent, is activeconstituents as U.S. Pat 4195190 with ferrous sulfate and picric acid, be dissolved in lower alcohol, the toluene, form liquid oil-saving agent; Application number is 97103812.0, denomination of invention for the national inventing patent application of " gasoline comburant " discloses a kind of with the ferrocene be activeconstituents oil-saving agent; But, can form residue after the metal-salt burning, cause that mechanical friction increases and the infringement engine, and this class oil-saving agent is generally liquid state, product should not transport, carry; (2) with the natural plant extracts be activeconstituents, save fuel oil, application number is 93101691.6, denomination of invention is the oil-saving agent of activeconstituents for the national inventing patent application of " new type gasoline, combustion promoter for diesel oil synthesis method " discloses a kind of with Radix Ginseng or ginseng roots leach liquor, rate of economizing gasoline is about 10%, yet this method popularization is poor, addition height, and preparation process complexity; (3) by adding organism such as alkanes or alcohols, change the octane value of fuel oil, improve the anti-knocking property and the combustionproperty of fuel oil, but rate of economizing gasoline is generally not high, about 10%.
Summary of the invention
Primary and foremost purpose of the present invention is to overcome the shortcoming of oil-saving agent that prior art provides with not enough, a kind of high-efficiency oil-saving agent is provided, this oil-saving agent is few based on camphor, addition, can be dissolved in fuel oil fast, and rate of economizing gasoline can be up to 30%, and residue is not stayed in metal-containing salt, burning.
Another object of the present invention is to provide the preparation method of described high-efficiency oil-saving agent.
A further object of the present invention is to provide the application of described high-efficiency oil-saving agent.
Purpose of the present invention is achieved through the following technical solutions: a kind of high-efficiency oil-saving agent is grouped into by following one-tenth by mass percentage:
Camphor 80～99.5%
Borneol 0.3～12%
Nitrotoluene 0.05～2.0%
Fluorenone compounds 0.05～2.0%
The lower aliphatic alcohols surplus;
Described camphor can be one or both in natural camphor or the synthetic camphor;
Described borneol can be one or both in positive borneol or the isocamphol;
Described nitrotoluene is one or both in mononitrotoluene or the dinitrotoluene (DNT);
Described Fluorenone compounds is at least a in 9-Fluorenone or the phenodiazine Fluorenone;
Described lower aliphatic alcohols is that carbon chain lengths is the Fatty Alcohol(C12-C14 and C12-C18) of C2～C4;
At least a in the preferred ethylene glycol of described lower aliphatic alcohols, ethanol or the propyl alcohol;
The preparation method of the ignition dope of described high efficiency, oil saving, comprise following steps: the Fluorenone compounds of mass percent 0.05～2.0% and the nitrotoluene of mass percent 0.05～2.0% are dissolved in the lower aliphatic alcohols, mix with the camphor of mass percent 80～99.5% and the borneol of mass percent 0.3～12% then, fully mixing obtains high-efficiency oil-saving agent;
The application of described high-efficiency oil-saving agent is that described high-efficiency oil-saving agent is made an addition in the fuel oil, and rate of economizing gasoline can be up to 30%;
Described fuel oil is preferably gasoline or diesel oil;
Described high-efficiency oil-saving agent is applied in the gasoline, and the ratio of adding 1 gram high-efficiency oil-saving agent according to 10～50L gasoline makes an addition to described oil-saving agent in the gasoline.
Principle of the present invention is: when fuel oil burns in airtight cylinder, oil of mirbane and Fluorenone compounds play the effect of catalytic activity, oxidation rate is accelerated, fuel oil is fully burnt, and camphor, borneol and Fluorenone compounds can be regulated the octane value of gasoline, improve the anti-knocking property and the combustionproperty of fuel oil, its rate of economizing gasoline can be up to 30%.
The present invention has following advantage and effect with respect to prior art
(1) oil-saving agent of the present invention is the active ignition dope of organic oxygen-containing base with camphor, borneol, oil of mirbane, Fluorenone compounds etc., and the oil-saving effect of fuel oil is obvious, and fuel-saving efficiency can be up to 30%;
(2) oil-saving agent of the present invention can make fuel oil fully burn, and reduces objectionable impurities and smog in the vehicle exhaust;
(3) do not use metal-salt as promoting agent in the high-efficiency oil-saving agent of the present invention, do not stay residue after fuel oil fully burns, help prolonging the life-span of engine;
(4) high-efficiency oil-saving agent of the present invention is a solid additive, is convenient to transportation, stores, and be soluble in the fuel oil, and adding proportion is little, does not change the physical propertiess such as viscosity, color of fuel oil; And this high-efficiency oil-saving agent safety can improve the anti-knocking property of fuel oil.
(5) preparation method of the present invention is simple, and cost is low, is with a wide range of applications.
Description of drawings
Fig. 1 is the prepared thermogravimetric curve of high-efficiency oil-saving agent in air atmosphere of embodiment 1.
Embodiment
The present invention is described in further detail below in conjunction with embodiment and accompanying drawing, but embodiments of the present invention are not limited thereto.
Embodiment 1
(1) preparation high-efficiency oil-saving agent: 0.1g 9-Fluorenone and 0.05g mononitrotoluene are dissolved in the 0.05g ethylene glycol, and 99.5g artificial camphor and 0.3g synthetic borneol mix then, and fully mixing obtains high-efficiency oil-saving agent.With this high-efficiency oil-saving agent compacting in flakes, every 1g.
(2) residual of high-efficiency oil-saving agent detects: high-efficiency oil-saving agent is placed thermal gravimetric analyzer, and in air atmosphere, thermal gravimetric analyzer heats up the high-efficiency oil-saving agent degradation curve that obtains with the speed of 20 ℃/min.As can be seen from Figure 1, when temperature arrived 175 ℃, the prepared oil-saving agent of present embodiment decomposed fully, does not have residual.
(3) detection of rate of economizing gasoline: use Shanghai Volkswagen's Passat 1.8T automobile to be testing vehicle, add gasoline 50L, travel, exercise after 1 hour, the record oil consumption with the speed of 90km/h; Then add 1 (1g) and 4 (4g) oil-saving agents respectively, add gasoline 50L, travel (returning by former road) with the speed of 90km/h, exercise after 1 hour, the record oil consumption is calculated rate of economizing gasoline, and is as shown in table 1:
Table 1
Embodiment 2
(1) preparation high-efficiency oil-saving agent: 0.05g 9-Fluorenone and 2g dinitrotoluene (DNT) are dissolved in the 2.45g ethylene glycol, and 85g artificial camphor and 10.5g synthetic borneol mix then, and fully mixing obtains high-efficiency oil-saving agent.With this high-efficiency oil-saving agent compacting in flakes, every 1g.
(2) residual of high-efficiency oil-saving agent detects: detect step with embodiment 1 step (2), according to detected result as can be known when temperature arrives 175 ℃, the high-efficiency oil-saving agent decomposition fully that present embodiment is prepared.
(3) detection of rate of economizing gasoline: detect step with embodiment 1 step (3), as shown in table 2:
Table 2
Embodiment 3
(1) preparation high-efficiency oil-saving agent: with 2g 1,8-phenodiazine-9-Fluorenone and 2g dinitrotoluene (DNT) are dissolved in the 4g ethanol, and 80g natural camphor and 12g synthetic borneol mix then, and fully mixing obtains high-efficiency oil-saving agent.With this high-efficiency oil-saving agent compacting in flakes, every 1g.
(2) residual of high-efficiency oil-saving agent detects: detect step with embodiment 1 step (2), according to detected result as can be known when temperature arrives 175 ℃, the high-efficiency oil-saving agent decomposition fully that present embodiment is prepared.
(3) detection of rate of economizing gasoline: detect step with embodiment 1 step (3), as shown in table 3:
Table 3
Embodiment 4
(1) preparation high-efficiency oil-saving agent: with 1g 1,8-phenodiazine-9-Fluorenone and 2g mononitrotoluene are dissolved in the 2g propyl alcohol, and 87g artificial camphor and 8g synthetic borneol mix then, and fully mixing obtains high-efficiency oil-saving agent.With this high-efficiency oil-saving agent compacting in flakes, every 1g.
(2) residual of high-efficiency oil-saving agent detects: detect step with embodiment 1 step (2), according to detected result as can be known when temperature arrives 175 ℃, the high-efficiency oil-saving agent decomposition fully that present embodiment is prepared.
(3) detection of rate of economizing gasoline: detect step with embodiment 1 step (3), as shown in table 4:
Table 4
Embodiment 5
(1) preparation high-efficiency oil-saving agent: with 0.8g 1,8-phenodiazine-9-Fluorenone and 0.7g mononitrotoluene are dissolved in the 1.5g propyl alcohol, and 93g artificial camphor and 4g synthetic borneol mix then, and fully mixing obtains high-efficiency oil-saving agent.With this high-efficiency oil-saving agent compacting in flakes, every 1g.
(2) residual of high-efficiency oil-saving agent detects: detect step with embodiment 1 step (2), according to detected result as can be known when temperature arrives 175 ℃, the high-efficiency oil-saving agent decomposition fully that present embodiment is prepared.
(3) detection of rate of economizing gasoline: detect step with embodiment 1 step (3), as shown in table 5:
Table 5
The foregoing description is a preferred implementation of the present invention; but embodiments of the present invention are not restricted to the described embodiments; other any do not deviate from change, the modification done under spirit of the present invention and the principle, substitutes, combination, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (10)
1. high-efficiency oil-saving agent is characterized in that being grouped into by following one-tenth by mass percentage:
Camphor 80～99.5%
Borneol 0.3～12%
Nitrotoluene 0.05～2.0%
Fluorenone compounds 0.05～2.0%
The lower aliphatic alcohols surplus;
Described lower aliphatic alcohols is that carbon chain lengths is the Fatty Alcohol(C12-C14 and C12-C18) of C2～C4.
2. high-efficiency oil-saving agent according to claim 1 is characterized in that: described camphor is one or both in natural camphor or the synthetic camphor.
3. high-efficiency oil-saving agent according to claim 1 is characterized in that: described borneol is one or both in positive borneol or the isocamphol.
4. high-efficiency oil-saving agent according to claim 1 is characterized in that: described nitrotoluene is one or both in mononitrotoluene or the dinitrotoluene (DNT).
5. high-efficiency oil-saving agent according to claim 1 is characterized in that: described Fluorenone compounds is at least a in 9-Fluorenone or the phenodiazine Fluorenone.
6. high-efficiency oil-saving agent according to claim 1 is characterized in that: described lower aliphatic alcohols is at least a in ethylene glycol, ethanol or the propyl alcohol.
7. the preparation method of the ignition dope of each described high efficiency, oil saving of claim 1～6, it is characterized in that comprising following steps: the Fluorenone compounds of mass percent 0.05～2.0% and the nitrotoluene of mass percent 0.05～2.0% are dissolved in the lower aliphatic alcohols, mix with the camphor of mass percent 80～99.5% and the borneol of mass percent 0.3～12% then, fully mixing obtains high-efficiency oil-saving agent.
8. the application of the ignition dope of each described high efficiency, oil saving of claim 1～6 is characterized in that: described high-efficiency oil-saving agent is made an addition in the fuel oil.
9. application according to claim 8 is characterized in that: described fuel oil is gasoline or diesel oil.
10. application according to claim 9 is characterized in that: described high-efficiency oil-saving agent is applied in the gasoline, and the ratio of adding 1 gram high-efficiency oil-saving agent according to 10～50L gasoline makes an addition to described high-efficiency oil-saving agent in the gasoline.
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| CN2010101779931A CN101845338B (en) | 2010-05-21 | 2010-05-21 | High-efficiency oil-saving agent, preparation method and application thereof |
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| CN2010101779931A CN101845338B (en) | 2010-05-21 | 2010-05-21 | High-efficiency oil-saving agent, preparation method and application thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812865A (en) * | 2021-01-11 | 2021-05-18 | 南通腾展新能源科技有限公司 | Fuel oil power agent |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3925031A (en) * | 1970-07-23 | 1975-12-09 | Eugenio G Villacampa | Fuel and oil additive |
| CN1368539A (en) * | 2001-02-05 | 2002-09-11 | 美国环境能源燃料有限责任公司 | Fuel additives |
-
2010
- 2010-05-21 CN CN2010101779931A patent/CN101845338B/en not_active Expired - Fee Related
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3925031A (en) * | 1970-07-23 | 1975-12-09 | Eugenio G Villacampa | Fuel and oil additive |
| CN1368539A (en) * | 2001-02-05 | 2002-09-11 | 美国环境能源燃料有限责任公司 | Fuel additives |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112812865A (en) * | 2021-01-11 | 2021-05-18 | 南通腾展新能源科技有限公司 | Fuel oil power agent |
| CN112812865B (en) * | 2021-01-11 | 2023-07-14 | 南通鑫纳尔油品有限公司 | Fuel oil power agent |
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| CN101845338B (en) | 2012-11-14 |
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Granted publication date: 20121114 Termination date: 20130521 |