CN101844947B - Trace element water-soluble fertilizer and preparation method thereof - Google Patents
Trace element water-soluble fertilizer and preparation method thereof Download PDFInfo
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- CN101844947B CN101844947B CN201010153679XA CN201010153679A CN101844947B CN 101844947 B CN101844947 B CN 101844947B CN 201010153679X A CN201010153679X A CN 201010153679XA CN 201010153679 A CN201010153679 A CN 201010153679A CN 101844947 B CN101844947 B CN 101844947B
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Abstract
The invention relates to a trace element water-soluble fertilizer and a preparation method thereof, which are applied in the field of agriculture and forestry production. The trace element water-soluble fertilizer is characterized by comprising the following components in percentage by weight: 13 to 20 percent of ammonium carbonate, 8 to 10 percent of monopotassium phosphate, 19 to 35 percent of potassium sulfate, 15 to 33 percent of ferrous sulfate, 1.5 to 2.0 percent of copper sulfate, 1.9 to 2.5 percent of zinc sulfate, 1.6 to 1.9 percent of manganese sulfate, 2.3 to 2.6 percent of boric acid, 0.1 to 0.2 percent of sodium molybdate, 13 to 17 percent of magnesium sulfate, 1.5 to 2.0 percent of pericarpium juglandis, 2.0 to 2.5 percent of rhubarb, 1.5 to 1.8 percent of fineleaf schizonepeta herb and 1.0 to 1.4 percent of peganum harmala. The preparation method comprises the following steps of: 1, evaporating and dehydrating the ammonium carbonate, monopotassium phosphate, potassium sulfate, ferrous sulfate, copper sulfate, zinc sulfate, manganese sulfate, boric acid, sodium molybdate and magnesium sulfate at the temperature of between 110 and 180 DEG C respectively to keep the water content below 1.5 percent, and crushing the components into fine powder respectively; 2, crushing the pericarpium juglandis, rhubarb, fineleaf schizonepeta herb and the peganum harmala into fine powder, boiling the fine powder for 1 to 2 hours by adding water, squeezing the mixture, and taking juice to form Chinese medicinal juice; and 3, mixing the treated raw materials in a ratio, and winnowing and crushing the mixture to obtain the trace element water-soluble fertilizer.
Description
Technical field
The present invention relates to a kind of trace element water-soluble fertilizer and preparation method.
Background technology
What in agriculture prodn, use extensively and in a large number at present is chemical fertilizer, and it is few that organic fertilizer uses.Organic and inorganic fertilizer variety is various, but is mostly simple substance or two materialization fertilizer.The usage quantity of chemical fertilizer increases year by year; The mu consumption reaches the 80-150 kilogram; The consequence of a large amount of use chemical fertilizer is to make the structure of soil nutrient imbalance soil suffer serious destruction, causes nutritional deficiency disease generally to be taken place, and agricultural product quality is reduced; Influence HUMAN HEALTH, the nitrate salt that remains in the agricultural-food directly is detrimental to health and life security.Go back polluted-water simultaneously, destroy ecotope.A kind of water-soluble fertilizer was once arranged, and mostly the former foliage fertilizer that is named as is that chemical hormone processes, very big to human harm, disabled at present.
The content of invention
The objective of the invention is to overcome existing fertilizer defective provides a kind of to the needs of crop growthing development to various nutrients, the improving crop quality, improve trace element water-soluble fertilizer disease-resistant and that immunizing power, minimizing are polluted of preparation various trace elements.
Technical scheme of the present invention is: the characteristics of this trace element water-soluble fertilizer are in its component, to contain by weight percentage: volatile salt 13～20%; Potassium primary phosphate 8～10%; Vitriolate of tartar 19～35%; Ferrous sulfate 15～33%; Copper sulfate 1.5～2.0%; Zinc sulfate 1.9～2.5%; Manganous sulfate 1.6～1.9%; Boric acid 2.3～2.6%; Sodium orthomolybdate 0.1～0.2%; Sal epsom 13～17%; Exocarpium Juglandis Immaturum 1.5～2.0%; Rheum officinale 2.0～2.5%; Schizonepeta 1.5～1.8%; Herba pegani harmalae 1.0～1.4%.
Preparing method of the present invention is: its characteristics are: step 1; With volatile salt (by weight percentage; All material proportionings of relating among following this paper; All be weight percentage) 13～20%, potassium primary phosphate 8～10%, vitriolate of tartar 19～35%, ferrous sulfate 15～33%, copper sulfate 1.5～2.0%, zinc sulfate 1.9～2.5%, manganous sulfate 1.6～1.9%, boric acid 2.3～2.6%, Sodium orthomolybdate 0.1～0.2%, sal epsom 13～17% be respectively 110～180 ℃ of high temperature evaporations dehydrations; Make its water cut be lower than 1.5%, pulverize separately becomes fine powder; Step 2 is ground into fine powder with Exocarpium Juglandis Immaturum 1.5～2.0%, rheum officinale 2.0～2.5%, schizonepeta 1.5～1.8%, Herba pegani harmalae 1.0～1.4%, adds poach and presses extracting juice in 1～2 hour and became Chinese medicine juice; Step 3, by said mixed, compound is pulverized through selection by winnowing and is formed with above-mentioned treated raw material.
Another characteristics of the present invention are in the described step 2, and medicinal powder is crossed 80 mesh sieves before poach, and medicine when Chinese medicine adds poach juice/water ratio is 1: 10; The Chinese medicine juice of processing concentrates, and concentrated patent medicine/the juice ratio is 1: 1, promptly obtains 1 kilogram of concoction with 1 kilogram of medicinal powder.
Another characteristics of the present invention are that the raw materials mix process described in the described step 3 can also be: get ferrous sulfate powder, the mixing of sal epsom powder, get Chinese medicine juice and be sprayed on the aforementioned powder mix, further mix is even again, is a material; Getting sulfuric acid copper powder, sulfuric acid zinc powder, sulfuric acid manganese powder, boric acid powder, Sodium orthomolybdate powder and mix, is No. two material; Getting volatile salt powder, potassium dihydrogen phosphate, kalium slfuricum powder and mix, is No. three material; With behind material and No. two material mixings, add No. three material again and get thick batch mixing with the mixer thorough mixing, slightly air separation disintegrator is ground into 200-250 order fine powder and forms on the batch mixing.
The present invention has following advantage and effect: 1, can satisfy the needs of crop growthing development to nutrient.Conventional fertilizing method generally is the mixing fertilizer of processing with chemical fertilizer of simple substance or 2-3 kind chemical fertilizer, and mostly foliage fertilizer is the chemical industry hormone, thereby its nutrient is all not enough, all can not satisfy the needs of crop.The present invention explores the needs of crop through for many years put into practice (trade name of the present invention " multiple green bell "); Formulated according to the needed necessary trace element of crop growth; Solved the defective of conventional fertilizer nutritional deficiency, can satisfy the needs of crop growthing development nutrient.2, can improve the photosynthesis of crop.Because the present invention contains various trace elements, and the photosynthetic main frame of crop is a chloroplast(id), the formation of chloroplast(id) needs multiple nutrient element, and the present invention contains the element of chloroplast(id) needs just, so the present invention can improve the photosynthesis of crop.3, the resistance against diseases and the immunizing power of ability enhancing crop.Trace element is the important substance that improves crop resistance, is strengthening the photosynthetic cell concn that increases simultaneously, dwindles the iuntercellular lock, improves the cambium vigor, can stop the germ invasion effectively.So the resistance against diseases and the immunizing power of the present invention's ability enhancing crop.Facts have proved that the present invention has the good effect of pressing down that resists to wheat class, legume crop rust.4, has the effect that improves crop quality and raising the output.The quality that the crop organism forms depends on various nutritive substances such as protein, VITAMINs, carbohydrate and the mineral substance that it includes, and these materials depend on the quality of fertilizer.Facts have proved that the present invention can improve content of effective in the crop, and can increase production 15-30%.5, method of manufacture is simple, cost is low.
Embodiment
Respectively 110～180 ℃ of high temperature evaporation dehydrations, make its water cut be lower than 1.5% in volatile salt, potassium primary phosphate, vitriolate of tartar, ferrous sulfate, copper sulfate, zinc sulfate, manganous sulfate, boric acid, Sodium orthomolybdate, sal epsom, pulverize separately becomes fine powder, and is subsequent use.
Embodiment 1: get Exocarpium Juglandis Immaturum 2.0%, rheum officinale 2.5%, schizonepeta 1.8%, Herba pegani harmalae 1.4% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 19%, sal epsom powder 15%, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.7%, sulfuric acid zinc powder 2.2%, sulfuric acid manganese powder 1.7%, boric acid 2.5%, Sodium orthomolybdate 0.2%, mixing is No. two material; Get volatile salt 18%, potassium primary phosphate 8%, vitriolate of tartar 24%, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 2: get Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2%, schizonepeta 1.5%, Herba pegani harmalae 1% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 19%, sal epsom powder 15%, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.7%, sulfuric acid zinc powder 2.0%, sulfuric acid manganese powder 1.7%, boric acid 2.5%, Sodium orthomolybdate 0.1%, mixing is No. two material; Get volatile salt 18%, potassium primary phosphate 10%, vitriolate of tartar 24%, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 3: get Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2%, schizonepeta 1.5%, Herba pegani harmalae 1% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 17.6%, sal epsom powder 13%, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.5%, sulfuric acid zinc powder 1.9%, sulfuric acid manganese powder 1.6%, boric acid 2.3%, Sodium orthomolybdate 0.1%, mixing is No. two material; Get volatile salt 13%, potassium primary phosphate 8%, vitriolate of tartar 35%, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 4, get Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2%, schizonepeta 1.5%, Herba pegani harmalae 1% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 33%, sal epsom powder 13%, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.8%, sulfuric acid zinc powder 1.9%, sulfuric acid manganese powder 1.6%, boric acid 2.6%, Sodium orthomolybdate 0.1%, mixing is No. two material; Get volatile salt 13%, potassium primary phosphate 8%, vitriolate of tartar 19%, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 5: get Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2%, schizonepeta 1.5%, Herba pegani harmalae 1% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 15%, sal epsom powder 15.6%, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.5%, sulfuric acid zinc powder 1.9%, sulfuric acid manganese powder 1.6%, boric acid 2.3%, Sodium orthomolybdate 0.1%, mixing is No. two material; Get volatile salt 13%, potassium primary phosphate 8%, vitriolate of tartar 35%, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 6: get Exocarpium Juglandis Immaturum 2.0%, rheum officinale 2.5%, schizonepeta 1.8%, Herba pegani harmalae 1.4% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 16.1, sal epsom powder 17, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 2.0, sulfuric acid zinc powder 2.5, sulfuric acid manganese powder 1.9, boric acid 2.6, Sodium orthomolybdate 0.2, mixing is No. two material; Get volatile salt 20, potassium primary phosphate 10, vitriolate of tartar 20, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 7: get Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2.0%, schizonepeta 1.5%, Herba pegani harmalae 1.0% and be ground into fine powder, added poach 1～2 hour, press extracting juice and become Chinese medicine juice.Get ferrous sulfate powder 23, sal epsom powder 15, mixing is got Chinese medicine juice and is sprayed on the above-mentioned powder mix, and further mix is even again, is a material; Get sulfuric acid copper powder 1.5, sulfuric acid zinc powder 1.9, sulfuric acid manganese powder 1.6, boric acid 2.3, Sodium orthomolybdate 0.1, mixing is No. two material; Get volatile salt 15, potassium primary phosphate 8.6, vitriolate of tartar 25, mixing is No. three material; With material and No. two material mixings, add material No. three again, insert mixer and fully mix and become thick batch mixing, slightly batch mixing gets into air separation disintegrator again and is ground into 200-250 order fine powder, promptly obtains product of the present invention.
Embodiment 8: volatile salt 13%, potassium primary phosphate 8%, vitriolate of tartar 30%, ferrous sulfate 22.6%, copper sulfate 1.5%, zinc sulfate 1.9%, manganous sulfate 1.6%, boric acid 2.3%, Sodium orthomolybdate 0.1%, sal epsom 13% are dewatered at 110～180 ℃ of high temperature evaporations respectively; Make its water cut be lower than 1.5%, pulverize separately becomes fine powder; Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2.0%, schizonepeta 1.5%, Herba pegani harmalae 1.0% are ground into fine powder, add poach and pressed extracting juice in 1～2 hour and became Chinese medicine juice; By said mixed, compound is pulverized through selection by winnowing and is formed with above-mentioned treated raw material.
Embodiment 9: volatile salt 13%, potassium primary phosphate 8%, vitriolate of tartar 24.6%, ferrous sulfate 28%, copper sulfate 1.5%, zinc sulfate 1.9%, manganous sulfate 1.6%, boric acid 2.3%, Sodium orthomolybdate 0.1%, sal epsom 13% are dewatered at 110～180 ℃ of high temperature evaporations respectively; Make its water cut be lower than 1.5%, pulverize separately becomes fine powder; Exocarpium Juglandis Immaturum 1.5%, rheum officinale 2.0%, schizonepeta 1.5%, Herba pegani harmalae 1.0% are ground into fine powder, add poach and pressed extracting juice in 1～2 hour and became Chinese medicine juice; By said mixed, compound is pulverized through selection by winnowing and is formed with above-mentioned treated raw material.
Substances content among the above embodiment all is weight percentage.Among the above embodiment, Exocarpium Juglandis Immaturum, rheum officinale, schizonepeta, Herba pegani harmalae all are ground into fine powder, and before poach, medicinal powder is crossed 80 mesh sieves; When Chinese medicine added poach juice, medicine/water ratio was 1: 10; The Chinese medicine juice of processing concentrates, and concentrated patent medicine/the juice ratio is 1: 1, promptly obtains 1 kilogram of concoction with 1 kilogram of medicinal powder.
Claims (4)
1. a trace element water-soluble fertilizer is characterized in that in its component, containing by weight percentage: volatile salt 13～20%, potassium primary phosphate 8～10%, vitriolate of tartar 19～35%, ferrous sulfate 15～33%, copper sulfate 1.5～2.0%, zinc sulfate 1.9～2.5%, manganous sulfate 1.6～1.9%, boric acid 2.3～2.6%, Sodium orthomolybdate 0.1～0.2%, sal epsom 13～17%, Exocarpium Juglandis Immaturum 1.5～2.0%, rheum officinale 2.0～2.5%, schizonepeta 1.5～1.8%, Herba pegani harmalae 1.0～1.4%.
2. the preparation method of a trace element water-soluble fertilizer; It is characterized in that by weight percentage: step 1; Volatile salt 13～20%, potassium primary phosphate 8～10%, vitriolate of tartar 19～35%, ferrous sulfate 15～33%, copper sulfate 1.5～2.0%, zinc sulfate 1.9～2.5%, manganous sulfate 1.6～1.9%, boric acid 2.3～2.6%, Sodium orthomolybdate 0.1～0.2%, sal epsom 13～17% are dewatered at 110～180 ℃ of high temperature evaporations respectively; Make its water cut be lower than 1.5%, pulverize separately becomes fine powder; Step 2 is ground into fine powder with Exocarpium Juglandis Immaturum 1.5～2.0%, rheum officinale 2.0～2.5%, schizonepeta 1.5～1.8%, Herba pegani harmalae 1.0～1.4%, adds poach and presses extracting juice in 1～2 hour and became Chinese medicine juice; Step 3, by said mixed, compound is pulverized through selection by winnowing and is formed with above-mentioned treated raw material.
3. the preparation method of a kind of trace element water-soluble fertilizer as claimed in claim 2 is characterized in that in the described step 2, medicinal powder is crossed 80 mesh sieves before poach, and medicine when Chinese medicine adds poach juice/water ratio is 1: 10; The Chinese medicine juice of processing concentrates, and concentrated patent medicine/the juice ratio is 1: 1, promptly obtains 1 kilogram of concoction with 1 kilogram of medicinal powder.
4. like the preparation method of claim 2 or 3 described a kind of trace element water-soluble fertilizers; It is characterized in that the raw materials mix process described in the described step 3 can also be: get ferrous sulfate powder, the mixing of sal epsom powder; Getting Chinese medicine juice is sprayed on the aforementioned powder mix; Further mix is even again, is a material; Getting sulfuric acid copper powder, sulfuric acid zinc powder, sulfuric acid manganese powder, boric acid powder, Sodium orthomolybdate powder and mix, is No. two material; Getting volatile salt powder, potassium dihydrogen phosphate, kalium slfuricum powder and mix, is No. three material; With behind material and No. two material mixings, add No. three material again and get thick batch mixing with the mixer thorough mixing, slightly air separation disintegrator is ground into 200-250 order fine powder and forms on the batch mixing.
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