CN101818095B - Concentrated solution for fully mechanized mining hydraulic support electrohydraulic control system - Google Patents
Concentrated solution for fully mechanized mining hydraulic support electrohydraulic control system Download PDFInfo
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- CN101818095B CN101818095B CN2010101756111A CN201010175611A CN101818095B CN 101818095 B CN101818095 B CN 101818095B CN 2010101756111 A CN2010101756111 A CN 2010101756111A CN 201010175611 A CN201010175611 A CN 201010175611A CN 101818095 B CN101818095 B CN 101818095B
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- 238000005065 mining Methods 0.000 title claims abstract description 35
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 17
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 33
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 32
- 239000003795 chemical substances by application Substances 0.000 claims description 31
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 30
- 238000003756 stirring Methods 0.000 claims description 30
- 239000003921 oil Substances 0.000 claims description 28
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 20
- YNAVUWVOSKDBBP-UHFFFAOYSA-N Morpholine Chemical compound C1COCCN1 YNAVUWVOSKDBBP-UHFFFAOYSA-N 0.000 claims description 20
- BXWNKGSJHAJOGX-UHFFFAOYSA-N hexadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCO BXWNKGSJHAJOGX-UHFFFAOYSA-N 0.000 claims description 16
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- VEHVJXQNSCCNSB-UHFFFAOYSA-N morpholin-4-ium;benzoate Chemical compound C1COCCN1.OC(=O)C1=CC=CC=C1 VEHVJXQNSCCNSB-UHFFFAOYSA-N 0.000 claims description 12
- 235000013311 vegetables Nutrition 0.000 claims description 12
- -1 Polyoxyethylene Polymers 0.000 claims description 11
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 claims description 11
- 239000012964 benzotriazole Substances 0.000 claims description 11
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 claims description 11
- 229910000020 calcium bicarbonate Inorganic materials 0.000 claims description 11
- VTYYLEPIZMXCLO-UHFFFAOYSA-L calcium carbonate Substances [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 11
- 235000010216 calcium carbonate Nutrition 0.000 claims description 11
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 10
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 10
- 239000010695 polyglycol Substances 0.000 claims description 10
- 229920000151 polyglycol Polymers 0.000 claims description 10
- 239000011591 potassium Substances 0.000 claims description 10
- 229910052700 potassium Inorganic materials 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 10
- JRMUNVKIHCOMHV-UHFFFAOYSA-M tetrabutylammonium bromide Chemical compound [Br-].CCCC[N+](CCCC)(CCCC)CCCC JRMUNVKIHCOMHV-UHFFFAOYSA-M 0.000 claims description 10
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 8
- ZEMPKEQAKRGZGQ-AAKVHIHISA-N 2,3-bis[[(z)-12-hydroxyoctadec-9-enoyl]oxy]propyl (z)-12-hydroxyoctadec-9-enoate Chemical compound CCCCCCC(O)C\C=C/CCCCCCCC(=O)OCC(OC(=O)CCCCCCC\C=C/CC(O)CCCCCC)COC(=O)CCCCCCC\C=C/CC(O)CCCCCC ZEMPKEQAKRGZGQ-AAKVHIHISA-N 0.000 claims description 7
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 7
- 229910052710 silicon Inorganic materials 0.000 claims description 7
- 239000010703 silicon Substances 0.000 claims description 7
- 239000005995 Aluminium silicate Substances 0.000 claims description 6
- 229910021532 Calcite Inorganic materials 0.000 claims description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims description 6
- WYTGDNHDOZPMIW-RCBQFDQVSA-N alstonine Natural products C1=CC2=C3C=CC=CC3=NC2=C2N1C[C@H]1[C@H](C)OC=C(C(=O)OC)[C@H]1C2 WYTGDNHDOZPMIW-RCBQFDQVSA-N 0.000 claims description 6
- 235000012211 aluminium silicate Nutrition 0.000 claims description 6
- 239000000440 bentonite Substances 0.000 claims description 6
- 229910000278 bentonite Inorganic materials 0.000 claims description 6
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 6
- 239000004359 castor oil Substances 0.000 claims description 6
- 235000019438 castor oil Nutrition 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 6
- 239000010439 graphite Substances 0.000 claims description 6
- 229910002804 graphite Inorganic materials 0.000 claims description 6
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 6
- 239000011777 magnesium Substances 0.000 claims description 6
- 229910052749 magnesium Inorganic materials 0.000 claims description 6
- 238000002360 preparation method Methods 0.000 claims description 6
- 238000007127 saponification reaction Methods 0.000 claims description 6
- 239000000454 talc Substances 0.000 claims description 6
- 235000012222 talc Nutrition 0.000 claims description 6
- 229910052623 talc Inorganic materials 0.000 claims description 6
- 239000003245 coal Substances 0.000 abstract description 10
- 229910052751 metal Inorganic materials 0.000 abstract description 6
- 239000002184 metal Substances 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 5
- 238000004140 cleaning Methods 0.000 abstract description 4
- 238000001914 filtration Methods 0.000 abstract description 4
- 238000011161 development Methods 0.000 abstract description 3
- 229910052799 carbon Inorganic materials 0.000 abstract description 2
- 239000000460 chlorine Substances 0.000 abstract description 2
- 229910052801 chlorine Inorganic materials 0.000 abstract description 2
- 238000005260 corrosion Methods 0.000 abstract description 2
- 230000007797 corrosion Effects 0.000 abstract description 2
- 239000004530 micro-emulsion Substances 0.000 abstract description 2
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 abstract 1
- 230000001050 lubricating effect Effects 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 description 23
- 235000011187 glycerol Nutrition 0.000 description 9
- 235000019197 fats Nutrition 0.000 description 7
- 230000005540 biological transmission Effects 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- LPXPTNMVRIOKMN-UHFFFAOYSA-M sodium nitrite Chemical compound [Na+].[O-]N=O LPXPTNMVRIOKMN-UHFFFAOYSA-M 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 239000007764 o/w emulsion Substances 0.000 description 4
- 239000003208 petroleum Substances 0.000 description 4
- WWYDYZMNFQIYPT-UHFFFAOYSA-N ru78191 Chemical compound OC(=O)C(C(O)=O)C1=CC=CC=C1 WWYDYZMNFQIYPT-UHFFFAOYSA-N 0.000 description 4
- 229920002545 silicone oil Polymers 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 3
- 102000004895 Lipoproteins Human genes 0.000 description 3
- 108090001030 Lipoproteins Proteins 0.000 description 3
- 239000002480 mineral oil Substances 0.000 description 3
- 230000002335 preservative effect Effects 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 235000010288 sodium nitrite Nutrition 0.000 description 3
- 235000015112 vegetable and seed oil Nutrition 0.000 description 3
- 239000008158 vegetable oil Substances 0.000 description 3
- ICLYJLBTOGPLMC-KVVVOXFISA-N (z)-octadec-9-enoate;tris(2-hydroxyethyl)azanium Chemical compound OCCN(CCO)CCO.CCCCCCCC\C=C/CCCCCCCC(O)=O ICLYJLBTOGPLMC-KVVVOXFISA-N 0.000 description 2
- 238000005299 abrasion Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 235000010446 mineral oil Nutrition 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 229940117013 triethanolamine oleate Drugs 0.000 description 2
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 description 1
- 101100309447 Caenorhabditis elegans sad-1 gene Proteins 0.000 description 1
- 208000005623 Carcinogenesis Diseases 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 244000057114 Sapium sebiferum Species 0.000 description 1
- 235000005128 Sapium sebiferum Nutrition 0.000 description 1
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 239000002199 base oil Substances 0.000 description 1
- JODXHCAANAWXKR-UHFFFAOYSA-N benzene;morpholine Chemical compound C1COCCN1.C1=CC=CC=C1 JODXHCAANAWXKR-UHFFFAOYSA-N 0.000 description 1
- 230000036952 cancer formation Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000504 carcinogenesis Toxicity 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 239000008157 edible vegetable oil Substances 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 description 1
- 235000010234 sodium benzoate Nutrition 0.000 description 1
- 239000004299 sodium benzoate Substances 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 229960004418 trolamine Drugs 0.000 description 1
- 235000019871 vegetable fat Nutrition 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000003911 water pollution Methods 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
The invention provides energy-saving environment-friendly water-based concentrated solution for a fully mechanized mining hydraulic support electrohydraulic control system under a coal mine, which is applied to different water qualities such as total hardness, sulfate radicals, chlorine radicals, bicarbonate radicals and the like through concentration ratio adjustments. The concentrated solution greatly improves lubricating property, rust resistance, corrosion resistance, sealability and cleaning and filtering characteristics of the fully mechanized mining hydraulic support electrohydraulic control system under the coal mine, has a function of repairing a metal frictional wear surface, prolongs the service life of equipment, changes a frictional interface, avoids pollutions, prevents original emulsified oil and microemulsion from polluting water resources of a mining area, and saves nonrenewable oil resources, so the concentrated solution is an energy-saving and environment-friendly substitute upgrading product, and simultaneously the concentrated solution meets national and international low-carbon economic development general requirements on energy saving and emission reduction, and has predominant economic benefits and social benefits.
Description
Technical field:
The present invention relates to the lubricated transmission system used additives of coal mine machinery hydraulic support, particularly a kind of concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system.
Background technology:
Hydraulic support is one of main equipment of comprehensive mining machinery coal mining production, the motion of support is to stop in the system that the pipeline and the controlling elements of a fixed structure are formed by pressure liquid to flow, thereby realize the transmission and the conversion of energy, this pressure fluid is commonly referred to as driving medium, and hydraulic transmission medium is the important composition part in the hydraulic efficiency system.The coal mine hydraulic supporting driving medium, the overwhelming majority is the hydraulic support oil in water emulsion, and oil in water emulsion is main raw material with the refined mineral oil, and it is formulated to add other additives again, and it need consume the bulk petroleum resource, and cost is also high.Major part still is base oil with mineral oil up to now, although advantages such as the extensive availability of vegetables oil and environmental sounds, it is not finding broad applicability aspect the high performance hydraulic support as yet.On the other hand, because coal mine hydraulic supporting directly discharges in the down-hole after using with transmission fluid, cause the severe contamination of a large amount of greasy dirts to subsurface environment.Granted publication has some inhibiter, lubricant, tensio-active agent and the configuration of other additives to form number for the patent of invention of CN 1036527C discloses a kind of concentrated transmission liquid for coal mine hydraulic supporting.Concrete composition has triethanolamine oleate, sulphonated oil, 1-1-Hydroxy Benzotriazole, ethylene glycol, EDTA, potassium hydroxide, butyl glycol ether, silicone emulsion.At first, owing to replaced oil in water emulsion with sulphonated oil in this product, though saved petroleum resources to a certain extent, reduced environmental pollution, but along with the continuous progress of coal mine hydraulic supporting with drive technology, and the continuous development of hydraulic transmission medium, its kind is increasing, and the over-all properties that this product carries out in the colliery using in fully mechanized mining hydraulic support electrohydraulic control system performance, can not meet the demands to aspects such as metal rub resistance wearing and tearing at for example energy-conserving and environment-protective, oilness, rust-preventing characteristic, preservative property, stopping property, cleaning and filtering.Concentrated solution for fully mechanized mining hydraulic support electrohydraulic control system can not just put undue emphasis on some individual event performance, and what the concentrated solution of high-quality fully mechanized mining hydraulic support electrohydraulic control system showed is a kind of over-all properties.Secondly, raw materials such as triethanolamine oleate give out peculiar smell in the saponification process, make the underground work environment be subjected to serious infringement, and waste liquid can cause water pollution in down-the hole treatment.Equally for example disclosed technical scheme does not all overcome above-mentioned technical problem among CN1042375A, CN1046752A, CN87101044A, US4686058 and the WO9324601 etc.
Publication number is that the document of CN101029273A discloses a kind of liquefied concentrate for hydraulic stand, and concrete prescription is water, sodium sulfonate, trolamine, tween, benzotriazole, disodium ethylene diamine tetraacetate, OS-15, Sodium Nitrite, Sodium Benzoate, kilfoam.Though solved to a certain extent that the conventional emulsification oil-proofness of hydraulic support in the prior art is poor, cost height, lack of material, problem that environmental-protecting performance is low, but this product contains Sodium Nitrite, trolamines etc. have carcinogenesis to human body, jeopardize underground labour's health.
Summary of the invention:
When preparation is used for the fully mechanized mining hydraulic support electrohydraulic control system concentrated solution, can not put undue emphasis on some individual event performance.In fact, the performance of the concentrated solution of high-quality fully mechanized mining hydraulic support electrohydraulic control system is a kind of over-all properties.The overall target of concentrated solution well could satisfy the good operation of present fully mechanized mining hydraulic support electrohydraulic control system.In order to overcome the problem that exists in the above-mentioned technology that solves, the inventor after having carried out a large amount of experiments, has developed product of the present invention through research and exploration.The invention provides a kind of both energy-conserving and environment-protective, safety and Health again, simultaneously in security, oilness, rust-preventing characteristic, preservative property, stopping property, cleaning and filtering, aspects such as metal rub resistance wearing and tearing are had a kind of concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system of comprehensive premium properties.
The present invention adopts vegetables oil or Vegetable oil lipoprotein or vegetable tallow proxy-mineral oil on the basis of existing technology, has saved petroleum-based energy, has reduced environmental pollution.Vegetable oil lipoprotein is the compound that is formed by lipid acid and glycerine chemical combination, is distributed widely in occurring in nature, from the fat general designation Vegetable oil lipoprotein of plant seed, pulp and other extracting section gained.Can be divided into oil and fat two classes by the proterties vegetables oil, usually calling oil for the liquid person at normal temperatures; Normal temperature is called fat for solid and semi-solid person down.Be divided into edible vegetable oil and fat and industrial plant grease two big classes by purposes.The greasy purposes of industrial plant is very extensive, is the main raw material of industrial goods such as soap, paint, printing ink, rubber, process hides, weaving, candle, lubricating oil, synthetic resins, makeup and medicine.In addition, the present invention is without carcinogenic substances such as Sodium Nitrites, energy-conserving and environment-protective, safety and Health.The present invention has also further adopted the anti-wear agent that metal frictional abrasion surface is had repairing effect, mainly be to have adopted: with respect to the gross weight of anti-wear agent, the component of anti-wear agent and content are the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight %, the rhombspar of 10 weight %.Go back oil-containing inorganic corrosion inhibitor for example Calcium hydrogen carbonate and benzoic acid morpholine etc. in the component of the present invention.The benzoic acid morpholine is acid of benzene morpholine or phenylmalonate again, and its CAS registration number is 2613-89-0, and molecular formula is C
9H
8O
4, molecular weight is 180.16, English name is phenyl-propanedioicacid or Phenylmalonic acid.The CAS registration number of water-soluble silicon oil is 63148-62-9.According to actual needs, the present invention optionally uses pour point reducer, antioxidant, detergent-dispersant additive, friction negative catalyst, oiliness improver, extreme pressure agent, foam reducing composition, metal passivator, emulsifying agent, rust-preventive agent, additives such as demulsifying agent.
A kind of concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system of the present invention contains following component, and the weight percentage sum of each component is 100%, and each compositions in weight percentage is respectively:
Vegetables oil 5-8%,
Mass percentage concentration is 30% sodium hydroxide 5-8%,
EDTA 4-8％，
Dimeracid potassium 1-3%,
Diethanolamine 5-7%,
Mass percentage concentration is 50% potassium hydroxide 5-10%,
Benzotriazole 2-5%,
Polyoxyethylene hexadecyl alcohol or polyoxyethylenated castor oil fat 5-8%,
Sad 1-3%,
Polyglycol ether 10%,
Glycerol 10%,
Morpholine 1-2%,
Water-soluble silicon oil 0.1-1%,
Tetrabutyl amonium bromide 0.3-0.5%,
Sanitas 1-2%,
Anti-wear agent 5-10%,
Surplus is a water;
The component of described anti-wear agent is: with respect to the gross weight of anti-wear agent, each component of anti-wear agent is respectively the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight % and the rhombspar of 10 weight %; Described sanitas is Calcium hydrogen carbonate powder and benzoic acid morpholine thing, and described Calcium hydrogen carbonate powder and benzoic acid morpholine are 1: 1 by mass ratio; Described vegetables oil is a Viscotrol C.
This preparation method who is used for the concentrated solution of fully mechanized mining hydraulic support electrohydraulic control system is: (1) is according to separately weight percent, get described vegetables oil, mass percentage concentration and be 30% sodium hydroxide, in reactor, mix, stirring saponification reaction 4 hours less than 70 ℃ down; (2) add entry, EDTA, dimeracid potassium, diethanolamine, morpholine, benzotriazole, glycerol and Tetrabutyl amonium bromide according to separately weight percent then, in 50-60 ℃ of stirring reaction 1-2 hour; (3) adding anti-wear agent, mass percentage concentration are 50% potassium hydroxide, sad and sanitas, continue to keep 50-60 ℃ and stir 1 hour; (4) adding polyoxyethylene hexadecyl alcohol or polyoxyethylenated castor oil fat keeps 50-60 ℃ to stir 20-30 minute; (5) adding polyglycol ether keeps 50-60 ℃ to stir 10-20 minute; (6) last adding water soluble silicone oil, 20-40 ℃ of following the stirring promptly obtained the described concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system in 30 minutes.
Embodiment
Embodiment 1
The concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system contains following component, and the weight percentage sum of each component is 100%, and each compositions in weight percentage is respectively:
Viscotrol C 5%,
Mass percentage concentration is 30% sodium hydroxide 5%,
EDTA 4％，
Dimeracid potassium 1%,
Diethanolamine 5%,
Mass percentage concentration is 50% potassium hydroxide 5%,
Benzotriazole 2%,
Polyoxyethylene hexadecyl alcohol 5%,
It is sad 1%,
Polyglycol ether 10%,
Glycerol 10%,
Morpholine 1%,
Water-soluble silicon oil 0.1%,
Tetrabutyl amonium bromide 0.3%,
Sanitas 1%,
Anti-wear agent 5%,
Surplus is a water;
The component of described anti-wear agent is: with respect to the gross weight of anti-wear agent, each component of anti-wear agent is respectively the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight % and the rhombspar of 10 weight %; Described sanitas is Calcium hydrogen carbonate powder and benzoic acid morpholine thing, and described Calcium hydrogen carbonate powder and benzoic acid morpholine are 1: 1 by mass ratio.
This preparation method who is used for the concentrated solution of fully mechanized mining hydraulic support electrohydraulic control system is: (1) is according to separately weight percent, get described Viscotrol C, mass percentage concentration and be 30% sodium hydroxide, in reactor, mix, stirring saponification reaction 4 hours less than 70 ℃ down; (2) add entry, EDTA, dimeracid potassium, diethanolamine, morpholine, benzotriazole, glycerol and Tetrabutyl amonium bromide according to separately weight percent then, in 50 ℃ of stirring reactions 1 hour; (3) adding anti-wear agent, mass percentage concentration are 50% potassium hydroxide, sad and sanitas, continue to keep 60 ℃ and stir 1 hour; (4) adding polyoxyethylene hexadecyl alcohol keeps 50 ℃ to stir 20-30 minute; (5) adding polyglycol ether keeps 50 ℃ to stir 10 minutes; (6) last adding water soluble silicone oil, 20 ℃ of following stirrings promptly obtained the described concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system in 30 minutes.
Embodiment 2
A kind of concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system contains following component, and the weight percentage sum of each component is 100%, and each compositions in weight percentage is respectively:
Viscotrol C 8%,
Mass percentage concentration is 30% sodium hydroxide 8%,
EDTA 8％，
Dimeracid potassium 3%,
Diethanolamine 7%,
Mass percentage concentration is 50% potassium hydroxide 10%,
Benzotriazole 5%,
Polyoxyethylenated castor oil fat 8%,
It is sad 3%,
Polyglycol ether 10%,
Glycerol 10%,
Morpholine 2%,
Water-soluble silicon oil 1%,
Tetrabutyl amonium bromide 0.5%,
Sanitas 2%,
Anti-wear agent 10%,
Surplus is a water;
The component of described anti-wear agent is: with respect to the gross weight of anti-wear agent, each component of anti-wear agent is respectively the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight % and the rhombspar of 10 weight %; Described sanitas is Calcium hydrogen carbonate powder and benzoic acid morpholine thing, and described Calcium hydrogen carbonate powder and benzoic acid morpholine are 1: 1 by mass ratio.
This preparation method who is used for the concentrated solution of fully mechanized mining hydraulic support electrohydraulic control system is: (1) is according to separately weight percent, get described vegetables oil, mass percentage concentration and be 30% sodium hydroxide, in reactor, mix, stirring saponification reaction 4 hours less than 70 ℃ down; (2) add entry, EDTA, dimeracid potassium, diethanolamine, morpholine, benzotriazole, glycerol and Tetrabutyl amonium bromide according to separately weight percent then, in 60 ℃ of stirring reaction 1-2 hours; (3) adding anti-wear agent, mass percentage concentration are 50% potassium hydroxide, sad and sanitas, continue to keep 60 ℃ and stir 1 hour; (4) adding polyoxyethylenated castor oil fat keeps 60 ℃ to stir 30 minutes; (5) adding polyglycol ether keeps 60 ℃ to stir 20 minutes; (6) last adding water soluble silicone oil, 40 ℃ of following stirrings promptly obtained the described concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system in 30 minutes.
Embodiment 3
A kind of concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system contains following component, and the weight percentage sum of each component is 100%, and each compositions in weight percentage is respectively:
Viscotrol C 6%,
Mass percentage concentration is 30% sodium hydroxide 7%,
EDTA 5％，
Dimeracid potassium 2%,
Diethanolamine 6%,
Mass percentage concentration is 50% potassium hydroxide 6%,
Benzotriazole 4%,
Polyoxyethylene hexadecyl alcohol 6%,
It is sad 2%,
Polyglycol ether 10%,
Glycerol 10%,
Morpholine 1.5%,
Water-soluble silicon oil 0.8%,
Tetrabutyl amonium bromide 0.4%,
Sanitas 1.5%,
Anti-wear agent 6%,
Surplus is a water;
The component of described anti-wear agent is: with respect to the gross weight of anti-wear agent, each component of anti-wear agent is respectively the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight % and the rhombspar of 10 weight %; Described sanitas is Calcium hydrogen carbonate powder and benzoic acid morpholine thing, and described Calcium hydrogen carbonate powder and benzoic acid morpholine are 1: 1 by mass ratio; Described vegetables oil is a Viscotrol C.
This preparation method who is used for the concentrated solution of fully mechanized mining hydraulic support electrohydraulic control system is: (1) is according to separately weight percent, get described vegetables oil, mass percentage concentration and be 30% sodium hydroxide, in reactor, mix, stirring saponification reaction 4 hours less than 70 ℃ down; (2) add entry, EDTA, dimeracid potassium, diethanolamine, morpholine, benzotriazole, glycerol and Tetrabutyl amonium bromide according to separately weight percent then, in 45 ℃ of stirring reactions 1.5 hours; (3) adding anti-wear agent, mass percentage concentration are 50% potassium hydroxide, sad and sanitas, continue to keep 45 ℃ and stir 1 hour; (4) adding polyoxyethylene hexadecyl alcohol keeps 45 ℃ to stir 25 minutes; (5) adding polyglycol ether keeps 45 ℃ to stir 15 minutes; (6) last adding water soluble silicone oil, 30 ℃ of following stirrings promptly obtained the described concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system in 30 minutes.
The water base concentrated solution of the energy-conserving and environment-protective of fully mechanized mining hydraulic support electrohydraulic control system special use under the coal mine provided by the invention, apply to different water quality by the concentration ratio adjusting, total hardness for example, sulfate radical, the chlorine root, the water quality that bicarbonate radical content difference is bigger etc., greatly improved the oilness of fully mechanized mining hydraulic support electrohydraulic control system under the coal mine, rust-preventing characteristic, preservative property, stopping property, cleaning and filtering, metal frictional abrasion surface there is a kind of repairing effect, prolong service life of equipment, change characteristics such as frictional interface, avoided former oil in water emulsion, microemulsion is to the pollution of mine water resource, non-renewable petroleum resources have been saved, be the alternative upgrading products of a kind of not only energy-conservation but also environmental protection, also meet simultaneously the low-carbon economy development general requirement of country and international energy-saving and emission-reduction, have superior economic benefit and social benefit.
The result that performance and every index of three kinds of products among the embodiment 1-3 are tested according to MT76-2002 and MAJY09-006-07 testing standard all meets national requirements and industry production safety requirements.Now embodiment 2 products obtained therefroms are detected through national security production Beijing mine working equipment and mining oil product inspection center, the result all meets the requirements, and test result is as showing 1-3:
National security production Beijing mine working equipment and mining oil product inspection center detected result table 1
National security production Beijing mine working equipment and mining oil product inspection center detected result table 2
National security production Beijing mine working equipment and mining oil product inspection center detected result table 3
Claims (2)
1. a concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system contains following component, and the weight percentage sum of each component is 100%, it is characterized in that each compositions in weight percentage is respectively:
Vegetables oil 5-8%,
Mass percentage concentration is 30% sodium hydroxide 5-8%,
EDTA 4-8％，
Dimeracid potassium 1-3%,
Diethanolamine 5-7%,
Mass percentage concentration is 50% potassium hydroxide 5-10%,
Benzotriazole 2-5%,
Polyoxyethylene hexadecyl alcohol or polyoxyethylenated castor oil fat 5-8%,
Sad 1-3%,
Polyglycol ether 10%,
Glycerol 10%,
Morpholine 1-2%,
Water-soluble silicon oil 0.1-1%,
Tetrabutyl amonium bromide 0.3-0.5%,
Sanitas 1-2%,
Anti-wear agent 5-10%,
Surplus is a water;
The component of described anti-wear agent is: with respect to the gross weight of anti-wear agent, each component of anti-wear agent is respectively the serpentine of 40 weight %, the magnesium base bentonite of 10 weight %, the calcite of 10 weight %, the talcum of 10 weight %, the aphanitic graphite of 10 weight %, the kaolin of 10 weight % and the rhombspar of 10 weight %; Described sanitas is Calcium hydrogen carbonate powder and benzoic acid morpholine thing, and described Calcium hydrogen carbonate powder and benzoic acid morpholine are 1: 1 by mass ratio;
The preparation method of described concentrated solution is: (1) gets described vegetables oil, mass percentage concentration according to weight percent is 30% sodium hydroxide, mixes in reactor, is stirring saponification reaction 4 hours down less than 70 ℃; (2) add entry, EDTA, dimeracid potassium, diethanolamine, morpholine, benzotriazole, glycerol and Tetrabutyl amonium bromide according to the weight percent of each component then, in 50-60 ℃ of stirring reaction 1-2 hour; (3) add anti-wear agent then, mass percentage concentration is 50% potassium hydroxide, sad and sanitas, continue to keep 50-60 ℃ to stir 1 hour; (4) adding polyoxyethylene hexadecyl alcohol or polyoxyethylenated castor oil fat again keeps 50-60 ℃ to stir 20-30 minute; (5) adding polyglycol ether then keeps 50-60 ℃ to stir 10-20 minute; (6) add water-soluble silicon oil at last, 20-40 ℃ of following the stirring promptly obtained the described concentrated solution that is used for fully mechanized mining hydraulic support electrohydraulic control system in 30 minutes.
2. concentrated solution according to claim 1 is characterized in that: described vegetables oil is a Viscotrol C.
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| CN102618366B (en) * | 2012-03-09 | 2013-10-30 | 广西大学 | Lubricant composition for fuel gas generator of ship gas turbine |
| CN102911799B (en) * | 2012-10-25 | 2014-03-26 | 高碑店市中煤神海科技发展有限公司 | Cleaning agent for electrohydraulic control system of fully-mechanized mining hydraulic support and preparation method thereof |
| CN102925268A (en) * | 2012-11-07 | 2013-02-13 | 福建中佰川生物润滑剂有限公司 | Cleaning concentrate hydraulic fluid and preparation method thereof |
| CN103305327B (en) * | 2013-07-10 | 2014-08-13 | 哈尔滨紫杉油脂有限责任公司 | Preparation method of emulsified oil for hydraulic support |
| CN103387869B (en) * | 2013-08-09 | 2015-01-14 | 焦作市广聚矿用制品有限公司 | Emulsified oil for coal mine hydraulic support and preparation method thereof |
| CN104673431A (en) * | 2013-11-28 | 2015-06-03 | 深圳市富兰克科技有限公司 | Alkaline electrolyte-containing mine support hydraulic fluid |
| CN105838494B (en) * | 2016-04-29 | 2019-09-24 | 榆林市金世源矿用油品有限公司 | A kind of hydraulic support environment-friendly type concentrate and preparation method thereof |
| CN107557132B (en) * | 2017-06-28 | 2021-02-02 | 煤炭科学技术研究院有限公司 | Green efficient concentrated solution for hydraulic support system and preparation method thereof |
| CN107723081A (en) * | 2017-09-30 | 2018-02-23 | 新疆现代石油化工股份有限公司 | Hydraulic support oil emulsion and preparation method thereof |
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| CN108048182B (en) * | 2017-12-18 | 2021-05-07 | 煤炭科学技术研究院有限公司 | Composite functional additive for emulsified oil for hydraulic support and preparation method |
| CN109337750A (en) * | 2018-11-02 | 2019-02-15 | 浙江师范大学 | A kind of hard water resistance hydraulic support emulsion of novel environment-friendly and its production method |
| CN110499146B (en) * | 2019-09-02 | 2021-05-11 | 淄博爱科工矿机械有限公司 | High-performance environment-friendly anti-freezing solution for hydraulic support and preparation method thereof |
| CN111088096B (en) * | 2019-12-30 | 2022-02-18 | 河北科技大学 | Graphene oxide grafted modified oleic soap, concentrated solution for hydraulic support, preparation method and application |
| CN111253996B (en) * | 2020-03-06 | 2022-04-26 | 薛友生 | Biodegradable fully-mechanized mining support electro-hydraulic control concentrated solution and hydraulic fluid containing same |
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| EP0062891A1 (en) * | 1981-04-13 | 1982-10-20 | Basf Wyandotte Corporation | Thickened-water based hydraulic fluids |
| GB9221841D0 (en) * | 1992-10-17 | 1992-12-02 | Castrol Ltd | Industrial oils |
| CN1036527C (en) * | 1994-08-26 | 1997-11-26 | 巢剑崙 | Concentrated transmission liquid for coal mine hydraulic supporting |
| JP4598907B2 (en) * | 1999-04-16 | 2010-12-15 | Ｊｘ日鉱日石エネルギー株式会社 | Hydraulic fluid composition |
| CN101029273B (en) * | 2007-02-15 | 2010-05-26 | 大同云雁石化有限公司 | Liquefied concentrate for hydraulic stand |
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