CN101798472A - Black and blue disperse dye composition - Google Patents
Black and blue disperse dye composition Download PDFInfo
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- CN101798472A CN101798472A CN201010133539A CN201010133539A CN101798472A CN 101798472 A CN101798472 A CN 101798472A CN 201010133539 A CN201010133539 A CN 201010133539A CN 201010133539 A CN201010133539 A CN 201010133539A CN 101798472 A CN101798472 A CN 101798472A
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Abstract
The invention discloses a black and blue disperse dye composition which comprises the components by weight percent: at least one 30-70% of dye monomer A shown in formula (1), at least one 15-40% of dye monomer B shown in formula (2), at least one 5-50% of dye monomer C shown in formula (3) and at least one 5-50% of dye monomer D shown in formula (4). The disperse dye composition has wide application scope of pH value, good compatibility, strong dye depth property, high color yield, good uniformity, and good sublimation fastness, washing fastness and fastness to sunlight; more importantly, the black and blue disperse dye composition has low price and convenient use, and makes up the defects of compatibility, dye depth property and tiger color of black and blue disperse dye spliced by disperse orange 288 model.
Description
Technical field
The present invention relates to black, the blue disperse dye composition of a kind of environment-friendly type, be applicable to the dyeing and the stamp of terylene and BLENDED FABRIC thereof.
Background technology
Environment-friendly type is black in the market, blue serial dispersed dye, generally by DISPERSE ORANGE 30 200 288#, 63 DISPERSE Violet 63 93:1 and EX-SF DISPERSE BLUE EX-SF 300 291:3 form, though one of them component DISPERSE ORANGE 30 200 288# of this composition is the environmental protection dyestuff, remedied the deficiency of DISPERSE ORANGE 30 200 76#, and cost is also on the low side many than the DISPERSE ORANGE 30 200 61# of same environmental protection, but the shortcoming of DISPERSE ORANGE 30 200 288# is exactly a compatibleness, depth, opacifying property not as good as DISPERSE ORANGE 30 200 76# and DISPERSE ORANGE 30 200 61#, and look more serious the third of the twelve Earthly Branches, to look requirement in the third of the twelve Earthly Branches high-grade import trevira relatively, can only use the black of DISPERSE ORANGE 30 200 61# assembly, blue disperse dye composition.But the cost black, blue disperse dye composition that DISPERSE ORANGE 30 200 61# pieces together is too high, seeks that a not only environmental protection, performance are not only good, cost but low deceive, blue disperse dye composition, extremely urgent.
Summary of the invention
The invention provides a kind of environmental protection, depth, all black preferably, the blue disperse dye composition of look in opacifying property, third of the twelve Earthly Branches, remedied that DISPERSE ORANGE 30 200 288# pieces together blackly, blue disperse dye compatibleness, depth, the third of the twelve Earthly Branches look deficiency.This disperse dye composition pH value applied widely, compatibleness is good, and depth is strong, the dye yield height, homogeneity is good, and sublimation fastness, washing fastness, light fastness are all good, and this low price black, blue disperse dye composition of what is more important is easy to use.
A kind of black, blue disperse dye composition comprises by weight percentage:
30%～70% at least a dye monomer A as the formula (1):
X
1Be H, halogen, NO
2Or CN;
R
1, R
2Independent separately is C
1～C
4Alkyl;
R
3, R
4Independent separately is C
1～C
4Alkyl or be C
1～C
4A hydrogen in the alkyl is replaced by phenyl ring, alkoxyl group, CN or is CH
2CH=CH
2Or be the alkyloyloxyethyl alkyl;
15%～40% at least a dye monomer B as the formula (2):
X
2, X
3Independent separately is H, halogen, NO
2Or CN;
R
5Be C
1～C
4Alkyl;
R
6, R
7Independent separately is C
1～C
4Alkyl or C
1～C
4A hydrogen in the alkyl is replaced by phenyl ring, alkoxyl group, CN or be the alkyloyloxyethyl alkyl or be CH
2CH=CH
2
5%～50% at least a dye monomer C as the formula (3):
X
3, X
4Independent separately is H, halogen, CN or NO
2
5%～50% at least a dye monomer D as the formula (4):
X
5, X
6Independent separately is H, halogen, CN or NO
2
Described dye monomer A preferably is made up of following one or more compositions,
Described dye monomer B preferably is made up of following one or more compositions,
Described dye monomer C preferably is made up of following one or more compositions,
Described dye monomer D preferably is made up of following one or more compositions,
Black, blue disperse dye composition of the present invention is preferably 35%～55% at least a dye monomer A as the formula (1), 20%～35% at least a dye monomer B as the formula (2), 6%～30% at least a dye monomer C as the formula (3), 6%～30% at least a dye monomer D as the formula (4).
Black, blue disperse dye composition of the present invention generally needs to add auxiliary agent during application.Described auxiliary agent is dispersed dye dispersion agent, diffusant and tensio-active agents thereof etc. commonly used when composite. preferably include one of following or its mixture: naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, alkyl naphthalene sulfonic acid formaldehyde condensation products.As condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF), naphthalene sulfonic acidformaldehyde condensation product (dispersing agent NNO), benzyl naphthalene sulfonic formaldehyde condensation compound (dispersing agent CNF), sodium lignosulfonate (xylogen 85A, 83A) etc.Usually, auxiliary agent is 1.5～3.2: 1 with the ratio of former dyestuff weight.
Black, blue disperse dye composition of the present invention can prepare with following method: after the former dyestuff of dye monomer is mixed in proportion, in the presence of auxiliary agent, water or other tensio-active agent, carry out corpusculed with pulverizers such as sand mill or shredders, then spraying drying.Above-mentioned dye monomer all can adopt the commercially available prod.
Black, blue disperse dye composition of the present invention can be aqueous, paste behind the corpusculed, can be powdery, particulate state after the spraying drying.Black, blue disperse dye composition of the present invention is an environment-friendly type, because of its depth is good, opacifying property strong, can reduce dye dosage, improves the utilization ratio of dyestuff; Because of its dye yield height, exhaustion rate height, the sewage in the time of can reducing dyeing; The intermiscibility of the each component when dyeing because of it, equalization, compatibleness are all good, the scope of application of pH value is extremely wide, so use more convenient.And black, blue disperse dye group low price of the present invention, the third of the twelve Earthly Branches, look few, and sublimation fastness, washing fastness, light fastness are all good.
Embodiment
The invention will be further described below in conjunction with embodiment, but protection scope of the present invention is not limited to this.
Embodiment 1～18
According to data shown in the table 1, with dye monomer A, dye monomer B, dye monomer C, dye monomer D by certain proportioning and condensation compound of methyl naphthalene sulfonic acid and formaldehyde (Dispersant MF), naphthalene sulfonic acidformaldehyde condensation product (dispersing agent NNO), sodium lignosulfonate (xylogen 85A, 83A) add water piece together mix after, grind dispersion with sand milling, carry out spraying drying then.
Wherein (1-1) among the dye monomer A can select the C.I.DISP BLUE 291:1# that Zhejiang Province Runtu intercalated Co., Ltd produces for use; (1-2) the C.I.DISP BLUE 291:2# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; Be 2 (1-3), 4-dinitrochlorobenzene amine diazotization and 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N-ethyl-N-allyl group aniline coupling makes; Be 2 (1-4), 4-dinitrochlorobenzene amine diazotization and 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N-ethyl-N-cyanoethyl aniline coupling makes; Be 2 (1-5), 4-dinitrochlorobenzene amine diazotization and 2-methoxyl group-5-acetylaminohydroxyphenylarsonic acid N-benzyl-N-cyanoethyl aniline coupling makes; (1-6) the C.I.DISP BLUE 291# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (1-7) the C.I.DISP BLUE 301# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (1-8) the C.I.DISP BLUE 79# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce.
Wherein (2-1) among the dye monomer B can select the C.I.DISP VIOLET 93# that Zhejiang Province Runtu intercalated Co., Ltd produces for use; (2-2) the C.I.DISP VIOLET 93:1# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-3) the C.I.DISP BLUE 183:1# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-4) the C.I.DISP BLUE 165:1# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-5) the C.I.DISP BLUE 165# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-6) the C.I.DISPVIOLET 63# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-7) the C.I.DISP VIOLET33# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (2-8) the C.I.DISP VIOLET 77# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce.
Wherein (3-1) among the dye monomer C can select the C.I.DISP ORANGE 288# that Zhejiang Province Runtu intercalated Co., Ltd produces for use; (3-2) the C.I.DISP ORANGE 30:2# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce; (3-3) the C.I.DISP ORANGE 298# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce.
Wherein (4-1) among the dye monomer D can select the C.I.DISP ORANGE 279# that Zhejiang Province Runtu intercalated Co., Ltd produces for use; (4-2) the C.I.DISP ORANGE 278# that can select for use Zhejiang Province Runtu intercalated Co., Ltd to produce.
Table 1:
The composition that disperse dye composition and 45% (weight) EX-SF DISPERSE BLUE EX-SF 300 291:1,30% (weight) 63 DISPERSE Violet 63 93# that the foregoing description is made, 25% (weight) DISPERSE ORANGE 30 200 288# piece together system carries out the performance comparison test, and testing method is as follows:
Respectively get the dispersed dye that 0.5 gram embodiment 1～20 makes, water is mixed with the dispersed dye suspension that concentration is 1g/500ml respectively, the suspension of getting 10ml, 50ml, 80ml mixes with the water of 90ml, 50ml, 20ml, regulate dye bath pH to 5 with acetic acid, be warmed up to 60 ℃ then, put into the 2g trevira simultaneously respectively and carry out high-temperature pressure dyeing, in 35 minutes, be warmed up to 130 ℃, be incubated 30 minutes, sampling when being cooled to 80 ℃.
Observe cloth specimen coloured light and adopt GB/T2400-1980, GB/T2397-2003, GB/T3921-1997, GB/T3920-1997, GB/T5718-1997 to measure its dyefastness.Measurement result sees Table 2.
Table 2
| The embodiment title | Compatibleness | Lifting force | Washing fastness | Crock fastness | Sublimation fastness (180 ℃) |
| Embodiment 1 | ??A | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 2 | ??A-B | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 3 | ??A | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 4 | ??A-B | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 5 | ??A-B | ??A - | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 6 | ??A-B | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 7 | ??A | ??A - | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 8 | ??A-B | ??A-B | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 9 | ??A-B | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 10 | ??A | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 11 | ??A | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 12 | ??A-B | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 13 | ??A | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 14 | ??A - | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 15 | ??A | ??A - | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 16 | ??A | ??A - | ??4-5 | ??4-5 | ??4-5 |
| The embodiment title | Compatibleness | Lifting force | Washing fastness | Crock fastness | Sublimation fastness (180 ℃) |
| Embodiment 17 | ??A | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 18 | ??A - | ??A | ??4-5 | ??4-5 | ??4-5 |
| Embodiment 19 | ??A | ??A | ??4 | ??4-5 | ??4-5 |
| Embodiment 20 | ??A | ??A | ??4-5 | ??4-5 | ??4-5 |
| Comparative Examples | ??B | ??B | ??4-5 | ??4-5 | ??4-5 |
Claims (6)
1. black, blue disperse dye composition by weight percentage, comprising:
30%～70% at least a dye monomer A as the formula (1):
X
1Be H, halogen, NO
2Or CN;
R
1, R
2Independent separately is C
1～C
4Alkyl;
R
3, R
4Independent separately is C
1～C
4Alkyl or be C
1～C
4A hydrogen in the alkyl is replaced by phenyl ring, alkoxyl group, CN or is CH
2CH=CH
2Or be the alkyloyloxyethyl alkyl;
15%～40% at least a dye monomer B as the formula (2):
X
2, X
3Independent separately is H, halogen, NO
2Or CN;
R
5Be C
1～C
4Alkyl;
R
6, R
7Independent separately is C
1～C
4Alkyl or C
1～C
4A hydrogen in the alkyl is replaced by phenyl ring, alkoxyl group, CN or be the alkyloyloxyethyl alkyl or be CH
2CH=CH
2
5%～50% at least a dye monomer C as the formula (3):
X
3, X
4Independent separately is H, halogen, CN or NO
2
5%～50% at least a dye monomer D as the formula (4):
X
5, X
6Independent separately is H, halogen, CN or NO
2
2. black, blue disperse dye composition as claimed in claim 1, it is characterized in that: described dye monomer A is made up of following one or more compositions,
3. black, blue disperse dye composition as claimed in claim 1, it is characterized in that: described dye monomer B is made up of following one or more compositions,
4. black, blue disperse dye composition as claimed in claim 1, it is characterized in that: described dye monomer C is made up of following one or more compositions,
5. black, blue disperse dye composition as claimed in claim 1, it is characterized in that: described dye monomer D is made up of following one or more compositions,
6. black, blue disperse dye composition as claimed in claim 1, it is characterized in that: by weight percentage, comprise: 35%～55% at least a dye monomer A as the formula (1), 20%～35% at least a dye monomer B as the formula (2), 6%～30% at least a dye monomer C as the formula (3), 6%～30% at least a dye monomer D as the formula (4).
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|---|---|---|---|
| CN201010133539.6A CN101798472B (en) | 2010-03-26 | 2010-03-26 | Black and blue disperse dye composition |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201010133539.6A CN101798472B (en) | 2010-03-26 | 2010-03-26 | Black and blue disperse dye composition |
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|---|---|
| CN101798472A true CN101798472A (en) | 2010-08-11 |
| CN101798472B CN101798472B (en) | 2014-01-15 |
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|---|---|---|---|
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| CN101948633A (en) * | 2010-08-24 | 2011-01-19 | 浙江闰土股份有限公司 | Environment-friendly quick dyeing disperse dye composition |
| CN102153890A (en) * | 2011-02-24 | 2011-08-17 | 绍兴县精细化工有限公司 | Disperse dye composition |
| CN102153888A (en) * | 2011-02-24 | 2011-08-17 | 浙江万丰化工有限公司 | Disperse dye compound |
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| CN102702790B (en) * | 2012-06-07 | 2014-06-18 | 江苏之江化工有限公司 | Disperse black azo dye mixture |
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| CN105733307B (en) * | 2014-12-10 | 2018-09-07 | 上海安诺其集团股份有限公司 | A kind of preparation method of disperse dye composition |
| CN105733306B (en) * | 2014-12-10 | 2018-09-07 | 上海安诺其集团股份有限公司 | A kind of application of disperse dye composition |
| CN105733303A (en) * | 2014-12-10 | 2016-07-06 | 上海安诺其集团股份有限公司 | A disperse dye composition |
| CN105733306A (en) * | 2014-12-10 | 2016-07-06 | 上海安诺其集团股份有限公司 | Application of disperse dye composition |
| CN105733307A (en) * | 2014-12-10 | 2016-07-06 | 上海安诺其集团股份有限公司 | Preparation method of disperse dye composition |
| CN105733303B (en) * | 2014-12-10 | 2018-09-07 | 上海安诺其集团股份有限公司 | A kind of disperse dye composition |
| CN105131648A (en) * | 2015-07-03 | 2015-12-09 | 浙江亿得化工有限公司 | Novel composite black disperse dye |
| CN106479220A (en) * | 2015-08-24 | 2017-03-08 | 杭州福莱蒽特精细化工有限公司 | A kind of dark blue to black disperse dye composition |
| CN106479221A (en) * | 2015-08-24 | 2017-03-08 | 杭州福莱蒽特精细化工有限公司 | A kind of dark blue to black disperse dye mixture |
| CN106479220B (en) * | 2015-08-24 | 2018-09-25 | 杭州福莱蒽特精细化工有限公司 | It is a kind of dark blue to black disperse dye composition |
| CN106479221B (en) * | 2015-08-24 | 2018-12-11 | 杭州福莱蒽特精细化工有限公司 | It is a kind of dark blue to black disperse dye mixture |
| CN111117289A (en) * | 2019-11-29 | 2020-05-08 | 浙江龙盛染料化工有限公司 | Blue-to-black disperse dye composition and dye product |
| CN111117289B (en) * | 2019-11-29 | 2022-07-19 | 浙江龙盛染料化工有限公司 | Blue-to-black disperse dye composition and dye product |
| CN112646390A (en) * | 2020-12-07 | 2021-04-13 | 绍兴市上虞金冠化工有限公司 | Dark blue to black disperse dye composition and dye product |
| CN112646390B (en) * | 2020-12-07 | 2022-10-28 | 绍兴市上虞金冠化工有限公司 | Dark blue to black disperse dye composition and dye product |
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