CN101781489A - Method for producing interior wall healthcare latex paint by using lavender natural extract - Google Patents

Method for producing interior wall healthcare latex paint by using lavender natural extract Download PDF

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Publication number
CN101781489A
CN101781489A CN200910217200A CN200910217200A CN101781489A CN 101781489 A CN101781489 A CN 101781489A CN 200910217200 A CN200910217200 A CN 200910217200A CN 200910217200 A CN200910217200 A CN 200910217200A CN 101781489 A CN101781489 A CN 101781489A
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China
Prior art keywords
stirring
low speed
emulsion
herba lysimachiae
quintessence oil
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Granted
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CN200910217200A
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CN101781489B (en
Inventor
王海林
胥帅
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Shandong hannuo Baojia energy Polytron Technologies Inc
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WEIFANG THREE POWER GROUP CO Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/54Improvements relating to the production of bulk chemicals using solvents, e.g. supercritical solvents or ionic liquids

Abstract

The invention relates to a method for producing an interior wall healthcare latex paint by using lavender natural extract, which comprises the following steps: A) mixing surface-active agent, lavender essential oil and sustained-release agent, and stirring the mixture at a low speed at 20-30 DEG C for 20 minutes; B) keeping stirring at the low speed, adding the mixture obtained in step A) evenly into latex, and stirring for 10 minutes; C) adding water, titanium pigment, filling material and partial additives in accordance with formula quantity into a new agitation tank, and stirring at a high speed for 20 minutes; D) sending the materials obtained in step C) into a sand mill to grind until the fineness of the granule is less than 30mu m, and lowering the materials temperature below 30 DEG C; E) keeping stirring at the low speed, adding the mixture obtained in step B) slowly into the materials obtained in step D); and F) keeping stirring at the low speed, adding the surplus additives, and adjusting to get the expected viscosity, thus obtaining the product. The product has healthcare efficacy.

Description

A kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint
Technical field
The present invention relates to a kind of method that the natural essential oil that extracts in the lavandula angustifolia is used to produce interior wall healthcare latex paint, belong to the fine chemical technology field.
Background technology
Lavandula angustifolia is that Labiatae, lavandula angustifolia belong to perennial shrub, originates in Mediterranean Zone.The lavandula angustifolia in China Xinjiang is also very famous.Though lavandula angustifolia name " grass " has cane to do, and is opening hepatic Xiao Hua on the tip, flower shape such as wheat spike, fragrance elegant in smell, salubrious sweet belongs to the rhythm fragrance of a flower clearly.
Common Herba Lysimachiae foenumgraeci quintessence oil is owing to complicated component, and effect is also a lot, and very high through the Herba Lysimachiae foenumgraeci quintessence oil purity of supercritical CO 2 extraction, the effect scope reduces relatively, and effect increases.High-quality Herba Lysimachiae foenumgraeci quintessence oil be utilize lavandula angustifolia fresh inflorescence after wet distillation, utilize supercritical CO 2 under suitable extracting pressure, temperature, time and CO2 flow condition, to make again.The Herba Lysimachiae foenumgraeci quintessence oil yield is generally 3.5%-4.8%.Optimized process conditions is extracting pressure 20MPa, 30 ℃ of temperature, CO2 flow 22L/h, extraction time 100min.The Herba Lysimachiae foenumgraeci quintessence oil purity height that makes under this condition, content mainly contain phantol, lavandula angustifolia alcohol, phanteine, acetate lavandula angustifolia ester etc. more than 96%.Its main effect has: pain relieving, anti-inflammatory, decongest and swelling, bring high blood pressure down, sharp neural calm, ease off the pressure, alleviate melancholy uneasyly, Cure for insomnia helps body and mind relaxed and comfortable.Because it can stabilize mood, so not normal psychological condition is had positive effect.Can purify, pacify soul, alleviate indignation and beaten sensation, make the people can face life even-tempered and good-humouredly.Because so its energy centre of equilibrium nerve is helpful to alarmed and dejected state.Also have significantly tranquil and the function of releiving, there be goodish easypro putting to console to the insomniac with spirit, unlike the series products of sleeping peacefully, the lavender essential oil used on work and daytime, not only do not have any too lax influence, can also provide calm and balance, stable and efficient job morale is provided, hot-temperedly advance or moody temper has goodish effect for pacifying.
Though the development of emulsion paint has only the history in more than 50 year, compare with other coating and to have many advantages, safety and environmental protection, easy construction, dried coating film is fast, good permeability, water-tolerant.Because these advantages people of emulsion paint generally adopt in indoor and outdoor decoration, make emulsion paint obtain tremendous development in recent years, along with the raising of people's living standard and the continuous development of emulsion paint technology, develop some function emulsion paints now again, as: mildew-proof latex paint, radon-screening emulsion paint, improve Air quality emulsion paint, absorbing carbon dioxide emulsion paint etc.These function emulsion paints can satisfy under people's varying environment and the different condition situation and use, but people want to produce the emulsion paint with health-care effect always for a long time, but fail to find suitable, sophisticated method.
Summary of the invention
At the deficiency that prior art exists, technical problem to be solved by this invention is, a kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint is provided, and produces the emulsion paint with health-care effect.
For solving the problems of the technologies described above, the technical solution used in the present invention is that a kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint comprises following content:
A, tensio-active agent, Herba Lysimachiae foenumgraeci quintessence oil, sustained release dosage are joined in the container by formula ratio, under 20-30 ℃ of temperature, stirring at low speed 20 minutes, stirring velocity is no more than 100r/min;
B, emulsion is joined in another container, the mixture that under stirring at low speed the A step is made evenly adds, and stirs 10 minutes, and stirring velocity is no more than 100r/min;
C, in new stirred pot, adding entry, titanium dioxide, filler, part of auxiliary by formula ratio, high-speed stirring 20 minutes, stirring velocity is not less than 1000r/min;
D, the material that the C step is made advance sand mill and are ground to below the fineness 30um; Ground temperature of charge is dropped to below 30 ℃;
E, the Herba Lysimachiae foenumgraeci quintessence oil that mixes that the B step is made and emulsion slowly join under stirring at low speed in the ground material that the D step makes;
F, be no more than in speed under the stirring at low speed of 100r/min and add formula ratio residue auxiliary agent, be transferred to suitable viscosity, be packaged to be product;
The composition of described each material and shared weight part thereof are:
Water, 258; Herba Lysimachiae foenumgraeci quintessence oil, 5; Tensio-active agent, 2; Sustained release dosage, 3; Dispersion agent, 6; Defoamer, 5; 50% aqueous thickener solution, 15; Flow agent, 6; Titanium dioxide, 180; Filler, 260; Emulsion 260.
Above-mentioned emulsion is the self-crossing emulsion of solid content more than 55%.
Above-mentioned Herba Lysimachiae foenumgraeci quintessence oil is the highly purified Herba Lysimachiae foenumgraeci quintessence oil of the fresh inflorescence of lavandula angustifolia through wet distillation and supercritical CO 2 extraction acquisition, and purity is more than 96%.
The above-mentioned utilization in the method that lavender natural extract produces interior wall healthcare latex paint, used Herba Lysimachiae foenumgraeci quintessence oil must be the highly purified Herba Lysimachiae foenumgraeci quintessence oil that obtains through the supercritical CO 2 abstraction technique, common on the market Herba Lysimachiae foenumgraeci quintessence oil complicated component, effect difference.Herba Lysimachiae foenumgraeci quintessence oil must and tensio-active agent, sustained release dosage thorough mixing, to reach slow release effect.Selected emulsion need be that emulsion particle diameter is little, the emulsion that solid content is high, and also stirring velocity is low, and temperature also will be controlled well.The addition of Herba Lysimachiae foenumgraeci quintessence oil must be an amount of, it can stabilize mood an amount of Herba Lysimachiae foenumgraeci quintessence oil, so not normal psychological condition is had positive effect, can purify, pacify soul, can alleviate indignation and beaten sensation, make the people can face life even-tempered and good-humouredly.Because so its energy centre of equilibrium nerve is helpful to alarmed and dejected state.Also have significantly tranquil and the function of releiving, there be goodish easypro putting to console to the insomniac with spirit, Herba Lysimachiae foenumgraeci quintessence oil used on work and daytime, not only do not have any too lax influence, calm and balance can also be provided, provide stable and effective job morale, hot-temperedly advance or moody temper has goodish effect, can increase work efficiency for pacifying.
The method of utilizing lavender natural extract to produce interior wall healthcare latex paint of the present invention, it makes the emulsion paint with health-care effect for the highly purified Herba Lysimachiae foenumgraeci quintessence oil through wet distillation and the acquisition of supercritical CO 2 abstraction technique is added in the emulsion paint with special process.Make emulsion paint behind decorating house, Oleum lavandula angustifolia can slow release, utilize Herba Lysimachiae foenumgraeci quintessence oil pain relieving, anti-inflammatory, decongest and swelling, bring high blood pressure down, sharp neural calm, ease off the pressure, alleviate effects such as melancholy uneasiness, thereby reach Cure for insomnia, alleviate stress, the effect of increasing work efficiency.
Raw material involved in the present invention is the usual commercially available technical pure commodity raw material that uses of the industry, is the raw material that the industry is known.
The present invention does not relate to specific equipment, and related detection method is industry customary way.
Embodiment
The present invention is described in more detail below in conjunction with embodiment.
Embodiment 1
A kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint comprises following content:
A, 2 parts in tensio-active agent, 5 parts of Herba Lysimachiae foenumgraeci quintessence oils, sustained release dosage are joined in the container for 3 parts, under 20-30 ℃ of temperature, stirring at low speed 20 minutes, stirring velocity is no more than 100r/min;
B, the self-crossing emulsion of 260 parts of solid contents more than 55% joined in another container, the mixture that under stirring at low speed the A step is made evenly adds, and stirs 10 minutes, and stirring velocity is no more than 100r/min;
C, in new stirred pot, add 258 parts of water, 180 parts of titanium dioxides, 260 parts of fillers, 6 parts of dispersion agents, 5 parts of defoamers, 6 parts of flow agents, 5 part of 50% aqueous thickener solution, high-speed stirring 20 minutes, stirring velocity is not less than 1000r/min;
D, the material that the C step is made advance sand mill and are ground to below the fineness 30um; Ground temperature of charge is dropped to below 30 ℃;
E, the Herba Lysimachiae foenumgraeci quintessence oil that mixes that the B step is made and emulsion slowly join under stirring at low speed in the ground material that the D step makes;
F, be no more than in speed under the stirring at low speed of 100r/min and add 10 part of 50% aqueous thickener solution again, be transferred to suitable viscosity, be packaged to be product.
The composition of described each material of present embodiment and shared weight part thereof are: water, 258; Herba Lysimachiae foenumgraeci quintessence oil, 5; Tensio-active agent, 2; Sustained release dosage, 3; Dispersion agent, 6; Defoamer, 5; 50% aqueous thickener solution, 15; Flow agent, 6; Titanium dioxide, 180; Filler, 260; Emulsion 260.
Embodiment 2
A kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint comprises following content:
A, 2 parts in tensio-active agent, 5 parts of Herba Lysimachiae foenumgraeci quintessence oils, sustained release dosage are joined in the container for 3 parts, under 20-30 ℃ of temperature, stirring at low speed 20 minutes, stirring velocity is no more than 100r/min;
B, the self-crossing emulsion of 260 parts of solid contents more than 55% joined in another container, the mixture that under stirring at low speed the A step is made evenly adds, and stirs 10 minutes, and stirring velocity is no more than 100r/min;
C, in new stirred pot, add 258 parts of water, 180 parts of titanium dioxides, 260 parts of fillers, 6 parts of dispersion agents, 5 parts of defoamers, 6 parts of flow agents, high-speed stirring 20 minutes, stirring velocity is not less than 1000r/min;
D, the material that the C step is made advance sand mill and are ground to below the fineness 30um; Ground temperature of charge is dropped to below 30 ℃;
E, the Herba Lysimachiae foenumgraeci quintessence oil that mixes that the B step is made and emulsion slowly join under stirring at low speed in the ground material that the D step makes;
F, be no more than in speed under the stirring at low speed of 100r/min and add 15 part of 50% aqueous thickener solution again, be transferred to suitable viscosity, be packaged to be product.
The composition of described each material of present embodiment and shared weight part thereof are: water, 258; Herba Lysimachiae foenumgraeci quintessence oil, 5; Tensio-active agent, 2; Sustained release dosage, 3; Dispersion agent, 6; Defoamer, 5; 50% aqueous thickener solution, 15; Flow agent, 6; Titanium dioxide, 180; Filler, 260; Emulsion 260.
Embodiment 3
A kind of method of utilizing lavender natural extract to produce interior wall healthcare latex paint comprises following content:
A, 2 parts in tensio-active agent, 5 parts of Herba Lysimachiae foenumgraeci quintessence oils, sustained release dosage are joined in the container for 3 parts, under 20-30 ℃ of temperature, stirring at low speed 20 minutes, stirring velocity is no more than 100r/min;
B, the self-crossing emulsion of 260 parts of solid contents more than 55% joined in another container, the mixture that under stirring at low speed the A step is made evenly adds, and stirs 10 minutes, and stirring velocity is no more than 100r/min;
C, in new stirred pot, add 258 parts of water, 180 parts of titanium dioxides, 260 parts of fillers, 6 parts of dispersion agents, 3 parts of defoamers, 3 parts of flow agents, 5 part of 50% aqueous thickener solution, high-speed stirring 20 minutes, stirring velocity is not less than 1000r/min;
D, the material that the C step is made advance sand mill and are ground to below the fineness 30um; Ground temperature of charge is dropped to below 30 ℃;
E, the Herba Lysimachiae foenumgraeci quintessence oil that mixes that the B step is made and emulsion slowly join under stirring at low speed in the ground material that the D step makes;
F, be no more than in speed under the stirring at low speed of 100r/min and add 10 part of 50% aqueous thickener solution again, 2 parts of defoamers, 3 parts of flow agents are transferred to suitable viscosity, are packaged to be product.
The composition of described each material of present embodiment and shared weight part thereof are: water, 258; Herba Lysimachiae foenumgraeci quintessence oil, 5; Tensio-active agent, 2; Sustained release dosage, 3; Dispersion agent, 6; Defoamer, 5; 50% aqueous thickener solution, 15; Flow agent, 6; Titanium dioxide, 180; Filler, 260; Emulsion 260.
The lavender natural extract that utilizes of the various embodiments described above is produced in the interior wall healthcare latex paint method, and Herba Lysimachiae foenumgraeci quintessence oil must be the highly purified Herba Lysimachiae foenumgraeci quintessence oil that obtains through the supercritical CO 2 abstraction technique, common on the market Herba Lysimachiae foenumgraeci quintessence oil complicated component, effect difference.Herba Lysimachiae foenumgraeci quintessence oil must and tensio-active agent, sustained release dosage thorough mixing, to reach slow release effect.Selected emulsion need be that emulsion particle diameter is little, the emulsion that solid content is high, and also stirring velocity is low, and temperature also will be controlled well.The addition of Herba Lysimachiae foenumgraeci quintessence oil must be an amount of, it can stabilize mood an amount of Herba Lysimachiae foenumgraeci quintessence oil, so not normal psychological condition is had positive effect, can purify, pacify soul, can alleviate indignation and beaten sensation, make the people can face life even-tempered and good-humouredly.Because so its energy centre of equilibrium nerve is helpful to alarmed and dejected state.Also have significantly tranquil and the function of releiving, there be goodish easypro putting to console to the insomniac with spirit, Herba Lysimachiae foenumgraeci quintessence oil used on work and daytime, not only do not have any too lax influence, calm and balance can also be provided, provide stable and effective job morale, hot-temperedly advance or moody temper has goodish effect, can increase work efficiency for pacifying.Therefore the interior wall healthcare latex paint that utilizes lavender natural extract to produce not only can use in family's interior decoration, also can use in the office space.
In the various embodiments described above, in emulsion paint, add Herba Lysimachiae foenumgraeci quintessence oil and auxiliary agent after, every performance index of emulsion paint all do not influence, and can cover other taste in the emulsion paint, make emulsion paint that fragrance just be arranged after uncapping.In use really can the centre of equilibrium nerve, make the people reduce uneasiness, the spirit of releiving is very helpful to insomniac and long-term brain worker, can use in indoor any environment.Because Herba Lysimachiae foenumgraeci quintessence oil adds through special process, strict in process of production control production technique, wherein the release of Herba Lysimachiae foenumgraeci quintessence oil effective constituent is controlled, makes the health-care effect of emulsion paint can reach 3-5.

Claims (3)

1. method of utilizing lavender natural extract to produce interior wall healthcare latex paint comprises following content:
A, tensio-active agent, Herba Lysimachiae foenumgraeci quintessence oil, sustained release dosage are joined in the container by formula ratio, under 20-30 ℃ of temperature, stirring at low speed 20 minutes, stirring velocity is no more than 100r/min;
B, emulsion is joined in another container, the mixture that under stirring at low speed the A step is made evenly adds, and stirs 10 minutes, and stirring velocity is no more than 100r/min;
C, in new stirred pot, adding entry, titanium dioxide, filler, part of auxiliary by formula ratio, high-speed stirring 20 minutes, stirring velocity is not less than 1000r/min;
D, the material that the C step is made advance sand mill and are ground to below the fineness 30um; Ground temperature of charge is dropped to below 30 ℃;
E, the Herba Lysimachiae foenumgraeci quintessence oil that mixes that the B step is made and emulsion slowly join under stirring at low speed in the ground material that the D step makes;
F, be no more than in speed under the stirring at low speed of 100r/min and add formula ratio residue auxiliary agent, be transferred to suitable viscosity, be packaged to be product;
The composition of described each material and shared weight part thereof are:
Water, 258; Herba Lysimachiae foenumgraeci quintessence oil, 5; Tensio-active agent, 2; Sustained release dosage, 3; Dispersion agent, 6; Defoamer, 5; 50% aqueous thickener solution, 15; Flow agent, 6; Titanium dioxide, 180; Filler, 260; Emulsion 260.
2. the method for utilizing lavender natural extract to produce interior wall healthcare latex paint according to claim 1, it is characterized in that: described emulsion is the self-crossing emulsion of solid content more than 55%.
3. the method for utilizing lavender natural extract to produce interior wall healthcare latex paint according to claim 1, it is characterized in that: described Herba Lysimachiae foenumgraeci quintessence oil is the highly purified Herba Lysimachiae foenumgraeci quintessence oil of the fresh inflorescence of lavandula angustifolia through wet distillation and supercritical CO 2 extraction acquisition, and purity is more than 96%.
CN2009102172001A 2009-12-31 2009-12-31 Method for producing interior wall healthcare latex paint by using lavender natural extract Expired - Fee Related CN101781489B (en)

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CN103709842A (en) * 2012-09-29 2014-04-09 上海绿色建材研究中心有限公司 Herbal essence health paint and preparation method thereof
CN103965711A (en) * 2014-05-16 2014-08-06 蒋宏宝 Insecticidal environment-friendly emulsion paint
CN104177949A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Anion environment-friendly latex paint containing sweet marjoram natural extract
CN104177950A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Negative ion antibacterial latex paint containing folium artemisiae argyi extract
CN104177903A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Lavender-scent anion internal wall putty and preparation method thereof
CN104177948A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Long-acting antibacterial emulsion paint containing ambergris extract
CN104212272A (en) * 2014-08-20 2014-12-17 中山艺展装饰工程有限公司 Antibacterial and environment-friendly lavender interior wall latex paint
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CN103709842B (en) * 2012-09-29 2016-01-20 上海绿色建材研究中心有限公司 A kind of Herbal essence health paint and preparation method thereof
CN103965711A (en) * 2014-05-16 2014-08-06 蒋宏宝 Insecticidal environment-friendly emulsion paint
CN104177903A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Lavender-scent anion internal wall putty and preparation method thereof
CN104177948A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Long-acting antibacterial emulsion paint containing ambergris extract
CN104212272A (en) * 2014-08-20 2014-12-17 中山艺展装饰工程有限公司 Antibacterial and environment-friendly lavender interior wall latex paint
CN104231709A (en) * 2014-08-20 2014-12-24 中山艺展装饰工程有限公司 Green environment-friendly long-acting antibacterial putty and preparation method
CN104177949A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Anion environment-friendly latex paint containing sweet marjoram natural extract
CN104212272B (en) * 2014-08-20 2017-02-08 河北晨阳工贸集团有限公司 Antibacterial and environment-friendly lavender interior wall latex paint
CN104177950A (en) * 2014-08-20 2014-12-03 中山艺展装饰工程有限公司 Negative ion antibacterial latex paint containing folium artemisiae argyi extract
CN111094473A (en) * 2017-07-11 2020-05-01 陶氏环球技术有限责任公司 Aqueous dispersion and aqueous coating composition comprising the same
WO2019010629A1 (en) 2017-07-11 2019-01-17 Dow Global Technologies Llc Aqueous dispersion and aqueous coating composition comprising the same
US11505716B2 (en) 2017-07-11 2022-11-22 Dow Global Technologies Llc Aqueous dispersion and aqueous coating composition comprising the same
CN111094473B (en) * 2017-07-11 2021-05-07 陶氏环球技术有限责任公司 Aqueous dispersion and aqueous coating composition comprising the same
CN107760161A (en) * 2017-10-31 2018-03-06 安徽腾龙泵阀制造有限公司 A kind of magnetic force pump case Special heat dissipating coating
CN110305543A (en) * 2018-03-27 2019-10-08 上海泛亚生命科技有限公司 A kind of natural plant incense atmosphere functional paint
CN109370293A (en) * 2018-10-15 2019-02-22 西安金海礁建筑节能科技有限公司 The plant essence water and preparation method thereof of the water-soluble finishing product of dilution
CN112341874A (en) * 2020-11-30 2021-02-09 吉安天晟新材料有限公司 Preparation method and application of coating containing compound plant extracted essential oil

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