CN101759364A - Manufacturing method of medical high white material molded glass bottle - Google Patents

Manufacturing method of medical high white material molded glass bottle Download PDF

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Publication number
CN101759364A
CN101759364A CN200810237814A CN200810237814A CN101759364A CN 101759364 A CN101759364 A CN 101759364A CN 200810237814 A CN200810237814 A CN 200810237814A CN 200810237814 A CN200810237814 A CN 200810237814A CN 101759364 A CN101759364 A CN 101759364A
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Prior art keywords
glass bottle
high white
medical high
molded glass
material molded
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CN200810237814A
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CN101759364B (en
Inventor
张军
苏玉才
弋康锋
杜少君
燕婉婷
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Shandong Pharmaceutical Glass Co Ltd
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Shandong Pharmaceutical Glass Co Ltd
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Abstract

The invention relates to a manufacturing method of a medical high white material molded glass bottle, belonging to the technical field of medical glass packaging and comprising the raw material formula of the medical high white material molded glass bottle. The invention is characterized in that the raw material formula is composed of the following raw materials by weight percentage: 40% of glass cullet and 60% of mixed batch, and the mixed batch is composed of the following raw materials by weight percentage: 51-54% of quartz sand, 8-10% of feldspar, 7-9% of calcite, 1-2% of fluorspar, 14-16% of calcined soda, 5-8% of dolomite, 0.65-0.81% of common salt and the balance of selenium powder and cobalt powder, wherein the selenium powder and the cobalt powder are mixed in any proportion. The use of the formula system can significantly reduce the melting temperature of a furnace and energy consumption and increase the appearance quality and the physical and chemical properties of the product at the same time.

Description

The method for making of medical high white material molded glass bottle
Technical field
The invention belongs to pharmaceutical glass packing technique field, particularly a kind of medical high white material molded glass bottle and method for making.
Background technology
When glasswork is being produced, the difference of raw material has just determined pharmaceutical glass Products Quality quality, raw material can be divided into general white material, height material, super-white marerial and brilliant white material in vain, directly has influence on the transparency and the brittleness of glasswork, and the glasswork quality that good more raw material production is come out is good more.Present domestic pharmaceutical glass all adopts this prescription invention main purpose of soda-lime-silica glass formula system component to improve homemade pharmaceutical glass quality from the prescription source, by strict CONTROL PROCESS process, strengthens the glass cullet usage quantity, improves melting efficiency, cuts down the consumption of energy.
" high white material produce some know from experience " (Yu Guoming " glass and enamel " the 3rd phase in 1999) introduced the control of selection atmosphere of selection, the fuel of raw material during producing extra white glass for bottles and pots is produced, finings and discoloring agent.The disclosed content of the document is quoted at this as prior art.
This method wants high to the quartz sand specification of quality, the fusing point height, and fuel consumption is big, the cost height.
Summary of the invention
The purpose of this invention is to provide a kind of medical high white material molded glass bottle and method for making thereof.
The following technical scheme of the concrete employing of the present invention, that is:
A kind of method for making of medical high white material molded glass bottle comprises the composition of raw materials of described medical high white material molded glass bottle it is characterized in that described composition of raw materials is made up of following weight percent raw material: glass cullet 40%, admixtion 60%;
Described admixtion is made up of following raw materials by weight percent:
Quartz sand 51~54%
Feldspar 8~10%
Calcite 7~12%
Fluorite 1~2%
Soda ash 14~16%
Rhombspar 5~8%
Salt 0.65~0.81%
Selenium powder, cobalt powder surplus.
Wherein, selenium powder, cobalt powder mix with arbitrary proportion.
Medical high white material molded glass of the present invention adopts scorification glass method for making to adopt the method for making of prior art substantially, and its basic engineering is:
Glass batch → mixing → raw material is levigate → high-temperature fusion → moulding → annealing → check → packing warehouse-in.
Difference from prior art is:
Described burden process is raw material to be cooperated evenly Fe in the described raw material 2O 3Content is not more than 3 ‰, and water content is 3%-5%, and raw material cooperates uniformity coefficient greater than 96%;
Described fusion operation temperature of fusion is 1420-1460 ℃, and O/R value is 4-12.
The invention has the beneficial effects as follows:
1) applicant finds, the too high whiteness that can influence glass of the moisture in the raw material.Its mechanism is that moisture can quicken the volatilization of S and Se when high temperature melts system.Simultaneously, if Fe 2O 3Content is greater than 3 ‰, and along with the prolongation of production time, glass can be in the vertical direction layering, and the bottom variable color influences the glass whiteness.
2) this prescription glass melting temperature is reduced to about 1400 ℃ for 1500~1600 ℃ by the molten system temperature of conventional formulation, and is compared with prior art, capable of saving fuel more than 35%.
3) the invention reside in the more traditional glass formula technology in whiteness, transparency, intensity, reduction glass melting temperature aspect that improves the pharmaceutical glass Bottle ﹠ Can new breakthrough is arranged.
4) product that adopts this prescription to make, quality meets standard GB 2640-90 regulation fully, and main quality index all is up to state standards.
Embodiment
Embodiment
1) composition of raw materials: glass cullet 40 weight parts, admixtion 60 weight parts, wherein, admixtion is according to the cooperation of following table.
Table 1: admixtion formula table.Unit: weight part
Figure G2008102378141D0000021
Figure G2008102378141D0000031
2) preparation method: batching is selected from each prescription of embodiment 1-3
Raw material is mixed to join in the kiln, carries out high temperature melting, in forming of glass equipment, be shaped then, anneal at last, check, qualified back packing warehouse-in at 1400 ℃.
The invention reside in the more traditional glass formula technology in whiteness, transparency, intensity, reduction glass melting temperature aspect that improves the pharmaceutical glass Bottle ﹠ Can new breakthrough is arranged.This prescription glass melting temperature is reduced to about 1400 ℃ for 1500~1600 ℃ by the molten system temperature of conventional formulation, and fuel economy is more than 30%.The product that adopts this prescription to make, quality meets standard GB 2640-90 regulation fully, and main quality index all is up to state standards.

Claims (2)

1. the method for making of a medical high white material molded glass bottle comprises the composition of raw materials of described medical high white material molded glass bottle it is characterized in that described composition of raw materials is made up of following weight percent raw material: glass cullet 40%, admixtion 60%;
Described admixtion is made up of following raw materials by weight percent:
Quartz sand 51~54%
Feldspar 8~10%
Calcite 7~9%
Fluorite 1~2%
Soda ash 14~16%
Rhombspar 5~8%
Salt 0.65~0.81%
Selenium powder, cobalt powder surplus
Wherein, selenium powder and cobalt powder mix with arbitrary proportion.
2. according to the described medical high white material molded glass bottle of claim 1, it is characterized in that the method for making of described medical high white material molded glass bottle comprises burden process, fusion operation,
Described burden process is raw material to be cooperated evenly Fe in the described raw material 2O 3Content is not more than 3 ‰, and water content is 3%-5%, and raw material cooperates uniformity coefficient greater than 96%;
Described fusion operation temperature of fusion is 1420-1460 ℃, and O/R value is 4-12.
CN2008102378141A 2008-12-02 2008-12-02 Manufacturing method of medical high white material molded glass bottle Active CN101759364B (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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CN101759364A true CN101759364A (en) 2010-06-30
CN101759364B CN101759364B (en) 2011-11-16

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Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102503081A (en) * 2011-09-23 2012-06-20 杭州爱佳玻璃制品有限公司 Production method for automatically machining borosilicate glass series feeding bottles
CN102690061A (en) * 2012-06-05 2012-09-26 广东健诚高科玻璃制品股份有限公司 Method for producing high-whiteness glass ceramic product
CN102826755A (en) * 2012-09-20 2012-12-19 张家港市俊锋玻璃制品有限公司 Manufacturing method of high-clarity glass bottle
CN102826754A (en) * 2012-09-20 2012-12-19 张家港市俊锋玻璃制品有限公司 Formulation of high-clarity glass bottle
CN103319088A (en) * 2013-06-20 2013-09-25 德清才府玻璃股份有限公司 Fluoride-free environment-friendly glass formula
CN103482869A (en) * 2013-08-26 2014-01-01 吴江光华玻璃厂 Porcelain white glass formula
CN103482870A (en) * 2013-08-26 2014-01-01 吴江光华玻璃厂 Porcelain white glass and production technique thereof
CN104529160A (en) * 2014-11-28 2015-04-22 宁波长利风玻璃制品有限公司 Super white material glass ball and production process thereof
CN105271743A (en) * 2015-10-19 2016-01-27 何书敏 Formula and production method of pharmaceutical neutral borosilicate glass tube
CN106587609A (en) * 2016-12-12 2017-04-26 天豪玻璃制品集团有限公司 Method for producing glass by using recycled glass bottles
CN109250912A (en) * 2018-12-10 2019-01-22 江苏孚日玻璃科技有限公司 A kind of automatically cleaning cosmetics vial and its production technology
CN109336386A (en) * 2018-11-28 2019-02-15 四川华晶玻璃有限公司 A kind of pure white material glass and its production technology
CN109399924A (en) * 2018-11-28 2019-03-01 四川华晶玻璃有限公司 A kind of high white material glass and its production technology
CN109534678A (en) * 2019-01-22 2019-03-29 山东景耀玻璃集团有限公司 A kind of low cost common white material glass and preparation method
CN111777328A (en) * 2020-07-13 2020-10-16 许民诚 Efficient environment-friendly glass bottle blowing process
CN111925118A (en) * 2020-06-29 2020-11-13 福建华兴玻璃有限公司 Preparation formula for producing high-whiteness glass by recycling printed cullet

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1282621C (en) * 2003-07-25 2006-11-01 阿城市大明玻璃制品有限公司 Formulation for preparing high-class polyether bottle using varicolored cullet
CN101148317A (en) * 2007-08-22 2008-03-26 东营力诺玻璃制品有限责任公司 Formula of medicinal neutral borosilicate glass

Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102503081A (en) * 2011-09-23 2012-06-20 杭州爱佳玻璃制品有限公司 Production method for automatically machining borosilicate glass series feeding bottles
CN102690061A (en) * 2012-06-05 2012-09-26 广东健诚高科玻璃制品股份有限公司 Method for producing high-whiteness glass ceramic product
CN102826755B (en) * 2012-09-20 2014-08-13 张家港市俊锋玻璃制品有限公司 Manufacturing method of high-clarity glass bottle
CN102826755A (en) * 2012-09-20 2012-12-19 张家港市俊锋玻璃制品有限公司 Manufacturing method of high-clarity glass bottle
CN102826754A (en) * 2012-09-20 2012-12-19 张家港市俊锋玻璃制品有限公司 Formulation of high-clarity glass bottle
CN103319088A (en) * 2013-06-20 2013-09-25 德清才府玻璃股份有限公司 Fluoride-free environment-friendly glass formula
CN103319088B (en) * 2013-06-20 2015-12-23 德清才府玻璃股份有限公司 A kind of fluorin environment protection glass
CN103482869A (en) * 2013-08-26 2014-01-01 吴江光华玻璃厂 Porcelain white glass formula
CN103482869B (en) * 2013-08-26 2015-09-23 吴江光华玻璃厂 Porcelain white glass is filled a prescription
CN103482870A (en) * 2013-08-26 2014-01-01 吴江光华玻璃厂 Porcelain white glass and production technique thereof
CN103482870B (en) * 2013-08-26 2016-01-20 吴江光华玻璃厂 A kind of porcelain white glass and production technique thereof
CN104529160A (en) * 2014-11-28 2015-04-22 宁波长利风玻璃制品有限公司 Super white material glass ball and production process thereof
CN105271743A (en) * 2015-10-19 2016-01-27 何书敏 Formula and production method of pharmaceutical neutral borosilicate glass tube
CN106587609A (en) * 2016-12-12 2017-04-26 天豪玻璃制品集团有限公司 Method for producing glass by using recycled glass bottles
CN109399924A (en) * 2018-11-28 2019-03-01 四川华晶玻璃有限公司 A kind of high white material glass and its production technology
CN109336386A (en) * 2018-11-28 2019-02-15 四川华晶玻璃有限公司 A kind of pure white material glass and its production technology
CN109250912A (en) * 2018-12-10 2019-01-22 江苏孚日玻璃科技有限公司 A kind of automatically cleaning cosmetics vial and its production technology
CN109534678A (en) * 2019-01-22 2019-03-29 山东景耀玻璃集团有限公司 A kind of low cost common white material glass and preparation method
CN111925118A (en) * 2020-06-29 2020-11-13 福建华兴玻璃有限公司 Preparation formula for producing high-whiteness glass by recycling printed cullet
CN111777328A (en) * 2020-07-13 2020-10-16 许民诚 Efficient environment-friendly glass bottle blowing process
CN111777328B (en) * 2020-07-13 2021-07-20 福建长城华兴玻璃有限公司 Efficient environment-friendly glass bottle blowing process

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