CN101732208A - Application of Chinese medicinal composition in preparation of oil-controlling shampoo - Google Patents
Application of Chinese medicinal composition in preparation of oil-controlling shampoo Download PDFInfo
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Abstract
The invention provides application of a Chinese medicinal composition in the preparation of oil-controlling shampoo, wherein the Chinese medicinal composition is prepared by extracting 0.25 to 8 weight parts of arborvitae leaf, 0.25 to 8 weight parts of common cnidium fruit, 0.25 to 8 weight parts of delavay soapberry pericarp seed and 0.25 to 8 weight parts of common rabdosia.
Description
Technical field
The present invention relates to the daily cosmetics technical field, be specifically related to a kind of Chinese medicine, natural drug oil-controlling shampoo.
Background technology
The people who much has oily hair is arranged, and it is thin that hair quality all compares the children.If whole head all is an oil oil, hair just seems not angry and lacks flexibility, and is plain.And can bring symptoms such as dandruff, pruritus, select to adopt oil-controlling shampoo to come control head to initiate oil so have the people of oily hair.Present shampoo on the market, of a great variety, function is also had nothing in common with each other, and the selection of multiple hair-protecting health-care is provided for people.But present most shampoo more or less all contains the chemical substance of synthetic, and with ZPT (pyrrolidine copper zinc), climbazole etc., maintenance also has essence, antibacterial, antiseptic etc. with silicone oil and cationic polymer as removing scurf and relieving itching.Though these chemical substances have played positive effect, still there are some side effect.
Traditional dandruff-controlling shampoo is to add anti-dandruff dose of function of giving removing scurf and relieving itching on the basis of common shampoo, these anti-dandruff dose is the chemosynthesis product, cause that to removing fungus dandruff has certain effect, the dandruff that hypersteatosis is caused comes off, only dandruff can be removed, and the reason that produces dandruff can not be fundamentally eliminated.The shampoo that also has some to claim to be pure Chinese medicine, but result of use is not very desirable.In recent years, cosmetics are at the trend development of beginning to " going back to nature ", begun one's study and contained the shampoo of Chinese medicine additive, make it have safety non-toxic, nonirritant again, but hair care and nourishing, relieving itching and removing dandruff, but, mainly there is the deficiency of two aspects with regard to the present existing shampoo that contains Chinese medicine additive: the one, the effect of the Chinese medicinal ingredients of adding is single at present, is the auxotype shampoo of generating and nourishing hair mostly, they are two years old, contain in the shampoo manufacturing process of Chinese medicine, mostly Chinese medicine additive adopts is to decoct or the method for infusion makes medicine juice, and the former makes the loss of property of medicine composition bigger, the latter's complex process, difficulty is big, and described method makes medicine juice to contain concentration little, and is poor with the compatibility of other component of shampoo.
The application's patent applicant has applied for " a kind of Chinese medicine shampoo of relieving itching and removing dandruff " (application number is 200910094201.1) on March 13rd, 2009, is the application for a patent for invention file of 101496783A referring to publication number.Claimed this Chinese medicine composition and preparation method thereof is found in clinical trial subsequently that this shampoo has to control oily effect preferably, and through patent retrieval, is not found that any document discloses the control functional oil of this compositions.
Summary of the invention
For overcoming the deficiencies in the prior art, solve problems such as scalp pomade, dandruff are many, scalp itch, the invention provides a kind of a kind of new purposes of Chinese medicine composition, i.e. application in preparing oil-controlling shampoo.
The invention provides the application of a kind of Chinese medicine composition in the preparation oil-controlling shampoo, it is characterized in that said composition is by the Cacumen Platycladi of 0.25-8 weight portion, the Fructus Cnidii of 0.25-8 weight portion, the Semen Sapindi Delavayi of 0.25-8 weight portion, the Herba Rabdosiae glaucocalycis of 0.25-8 weight portion, make the conventional shampoo substrate that adds the 68-99 weight portion behind the Chinese medicine extract again and make through extracting.
The invention provides the application of a kind of Chinese medicine composition in the preparation oil-controlling shampoo, it is characterized in that said composition is by the Cacumen Platycladi of 0.25-8 weight portion, the Fructus Cnidii of 0.25-8 weight portion, the Semen Sapindi Delavayi of 0.25-8 weight portion, the Herba Rabdosiae glaucocalycis of 0.25-8 weight portion, make the water that adds the 68-99 weight portion behind the Chinese medicine extract again and make through extracting.
Chinese medicine extract in the shampoo of the present invention can be made by two kinds of methods:
Method one takes by weighing Cacumen Platycladi, Fructus Cnidii, Semen Sapindi Delavayi, Herba Rabdosiae glaucocalycis 4 flavor medical materials by weight, adds 5-10 water doubly, decocts two to three mixing, filters, filtrate is concentrated into 1/20 of original volume, adds ethanol to containing alcohol amount 60-80%, places, filter, concentrate, vacuum drying gets Chinese medicine extract;
Method two extracts 4 flavor medical materials respectively earlier by purgation:
Cacumen Platycladi: take by weighing the Cacumen Platycladi medical material by weight, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, medicinal residues add 65% alcohol reflux twice, and each 2 hours, the decocting liquid behind medicinal liquid and the extraction volatile oil merged, filter, decompression recycling ethanol gets concentrated solution, put coldly, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, wait to adsorb the back water flushing that finishes, the ethanol elution of reuse 80% is collected eluent, reclaim ethanol, concentrate, lyophilization gets Cacumen Platycladi extract;
Fructus Cnidii: take by weighing the Fructus Cnidii medical material by weight, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, and reclaim under reduced pressure concentrates, and lyophilization gets Fructus cnidii extract;
Semen Sapindi Delavayi: take by weighing the Semen Sapindi Delavayi medical material by weight, water boiling and extraction three times, each 2 hours, filter, reclaim under reduced pressure water concentrates, and lyophilization gets the Semen Sapindi Delavayi extract;
Herba Rabdosiae glaucocalycis: take by weighing the Herba Rabdosiae glaucocalycis medical material by weight, add 85% alcohol reflux twice, filter, decompression recycling ethanol gets concentrated solution, puts cold, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, waits to adsorb the back water flushing that finishes, the ethanol elution of reuse 80%, collect eluent, decompression recycling ethanol concentrates, lyophilization gets Herba Rabdosiae glaucocalycis extract;
After obtaining each medicinal substances extract respectively, mix promptly getting Chinese medicine extract.
Method for making one: shampoo substrate disodiumedetate is dissolved with suitable quantity of water, add polyoxyethylenated alcohol sodium sulfate, place on 80 ℃ of water-baths after the heating for dissolving, add cocamido propyl betaine, add emulsified silicone oil and Pearl Concentrate behind the mix homogeneously, fully mix, promptly get phase 1; The Chinese medicine extract that above-mentioned two kinds of any one methods of method are made fully dissolves with propylene glycol in addition, promptly gets phase 2; Phase 2 is added uniform mixing in the phase 1, and add cationic guar gum, citric acid, Kai Song and essence, add water to ormal weight and get final product.
Method for making two: will add the sodium bicarbonate of 100 mesh sieves after the fusion of effervescent tablet substrate polyethylene glycol 6000, mix homogeneously, pulverize the cooling back, crosses 100 mesh sieves, add all through blended Chinese medicine extract, tartaric acid, the soluble starch of 100 mesh sieves, tabletting promptly gets effervescent tablet.Add in the entry during use and dissolve.
Method for making three: with the Chinese medicine extract that drying obtains, be dissolved in water or the dry extract extract powder is contained in the paper bag, make medicated bag, add entry during use, medicated bag is immersed to dissolve in the water get final product.
By new clinical experiment, contrasted the Test Summary of the present composition and commercially available shampoo, the result shows that the present invention has the purposes of preparation oil-controlling shampoo.
One, test objective
Seborrhea hair quality and dandruff are many by choosing, the crowd of hair pruritus (men and women does not limit), difference design experiment group (trial edition invention plant component shampoo) and matched group (commercially available shampoo on probation), and using method is identical with number of times.Observe " controlling oily effect ", " anti-dandruff effect ", " antipruritic effect " of two groups of crowds' use front and back, so that compare control oil, the anti-dandruff and antipruritic effect of the plant component shampoo of the present invention's trial-production.
Two, EXPERIMENTAL DESIGN
Test goes into to organize crowd's age: 18～60 years old; Sex: the men and women does not limit.
Adopt the mode of going into group at random to observe.
Case load: 160 examples, wherein: test group 120 examples, matched group 40 examples.
Group technology: adopt random fashion to enter test group or matched group.
Three, the group situation is gone in test
Actual several 161 examples of the total example of test of participating in.Test group wherein: 121 examples, matched group: 40 examples, go into that the group situation sees Table 1, table 2 for two groups.
Table 1 is participated in two groups of experimenter's sex statistics
Table 2 is participated in experimenter's age distribution table
Four, experimental observation result and conclusion
(1) " controlling oily effect " effective percentage of test group is 83.15%, and the effective percentage of matched group is 68.42%, and the control oil effect of test group obviously is better than matched group.
(2) " anti-dandruff effect " effective percentage of test group is 81.70%, and the effective percentage of matched group is 82.05%, illustrates that the anti-dandruff effect and the matched group of test group is suitable.
(3) " antipruritic effect " effective percentage of test group is 81.33%, and the effective percentage of matched group is 74.29%, and the antipruritic effect of test group is better than matched group.
The result of the test statistical data sees Table 3.
Two kinds of shampoo contrasts of table 3 trial effect statistical table
Illustrate:
Amount to selected 161 examples on probation, go into group respectively: " the present invention " shampoo test group 121 examples 1. on probation; 2. commercially available shampoo matched group 40 examples on probation.
Effective percentage calculates " effect is fine ", " effective " two item number certificates.
Typical case's example on probation:
Mrs Yang, 41 years old, the technical cadre was the seborrhea hair quality, and because operating pressure is big, hair turns to be yellow gradually, attenuates before 10 years, and bull is considered to be worth doing at ordinary times, and three days do not wash is the head pruritus agitation.According to the using method of plant shampoo agent of the present invention, used once every 2-3 days, when using for the second time continuously, just feel that dandruff obviously reduces, the head pruritus sx, the seborrhea phenomenon is obviously improved; When using the 5th time, dandruff, head pruritus transference cure, it is obvious to control oily effect; Used three months continuously front and back, and hair is blackening gradually, and hair quality is greatly improved.
Mr. Wang, 34 years old, the packer, the seborrhea hair quality is itched constantly, slight alopecia, and a large amount of dandruffs are arranged.According to three times on probation weekly, two weeks on probation, uses plant shampoo agent of the present invention after, feel that obviously hair quality improves, the dandruff disappearance, alopecia obviously reduces, the head pruritus symptom is thoroughly improved.
Mr. Niu, 50 years old, the political work cadre, neutral oiliness hair quality partially, dandruff is many especially at ordinary times, the head pruritus serious symptom.After using plant shampoo agent of the present invention five times, feel that obviously oily hair has improvement, dandruff disappears substantially, the head pruritus transference cure.
The specific embodiment:
Embodiment 1:
Cacumen Platycladi, Fructus Cnidii, Semen Sapindi Delavayi, Herba Rabdosiae glaucocalycis 4 flavor medical materials are respectively got 5 weight portions and added 5-10 water doubly, decoct two to three mixing, filter, filtrate is concentrated into 1/20 of original volume, add ethanol to containing alcohol amount 60-80%, place, filter, concentrate, vacuum drying gets Chinese medicine extract, and is standby;
Get shampoo substrate 80 weight portions commonly used, comprise: propylene glycol 20.1 weight portions, cationic guar gum 0.3 weight portion, citric acid 0.1 weight portion, cocamido propyl betaine 3 weight portions, polyoxyethylenated alcohol sodium sulfate 10 weight portions, emulsified silicone oil 3 weight portions, Pearl Concentrate 1.5 weight portions, disodiumedetate 0.2 weight portion, triumphant loose 0.05 weight portion, essence 0.5 weight portion, water 41.25 weight portions
Method for making: 1. disodiumedetate is dissolved with suitable quantity of water, add polyoxyethylenated alcohol sodium sulfate, place on 80 ℃ of water-baths after the heating for dissolving, add cocamido propyl betaine, add emulsified silicone oil and Pearl Concentrate behind the mix homogeneously, fully mix, promptly get phase 1.
2. other fully dissolves the Chinese medicine extract of above-mentioned gained with aqueous solution of propylene glycol, promptly gets phase 2.
3. phase 2 is added uniform mixing in the phase 1, and add cationic guar gum, citric acid, Kai Song and essence, add the water mixing and get final product.The shampoo of preparation has the control functional oil.
Embodiment 2:
Respectively 4 flavor medical materials are extracted by purgation earlier:
Cacumen Platycladi: take by weighing Cacumen Platycladi 1 weight portion, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, medicinal residues add 65% alcohol reflux twice, and each 2 hours, the decocting liquid behind medicinal liquid and the extraction volatile oil merged, filter decompression recycling ethanol, concentrated solution, put coldly, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, wait to adsorb the back water flushing that finishes, the ethanol elution of reuse 80% is collected eluent, reclaim ethanol, concentrate, lyophilization gets Cacumen Platycladi extract;
Fructus Cnidii: take by weighing Fructus Cnidii medical material 1 weight portion, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, and reclaim under reduced pressure concentrates, and lyophilization gets Fructus cnidii extract;
Semen Sapindi Delavayi: take by weighing Semen Sapindi Delavayi medical material 1 weight portion, water boiling and extraction three times, each 2 hours, filter, reclaim under reduced pressure water concentrates, and lyophilization gets the Semen Sapindi Delavayi extract;
Herba Rabdosiae glaucocalycis: take by weighing Herba Rabdosiae glaucocalycis medical material 1 weight portion, add 85% alcohol reflux twice, filter, decompression recycling ethanol, concentrated solution is put cold, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, waits to adsorb the back water flushing that finishes, the ethanol elution of reuse 80%, collect eluent, decompression recycling ethanol concentrates, lyophilization gets Herba Rabdosiae glaucocalycis extract;
After obtaining each medicinal substances extract respectively, mix promptly getting Chinese medicine extract, standby.
Get shampoo substrate 96 weight portions commonly used, comprising: propylene glycol 7 weight portions, Oleum Cocois oxalic acid amide 3 weight portions, monoalkyl phosphoric acid esters 7 weight portions, polyoxyethylenated alcohol sodium sulfate 10 weight portions, alkyl polyglucoside 2 weight portions, Pearl Concentrate 1.5 weight portions, disodiumedetate 0.2 weight portion, triumphant loose 0.05 weight portion, essence 0.5 weight portion, water 64.75 weight portions
Method for making: 1. disodiumedetate is dissolved with suitable quantity of water, add polyoxyethylenated alcohol sodium sulfate, place on 80 ℃ of water-baths after the heating for dissolving, add monoalkyl phosphoric acid esters, add alkyl polyglucoside and Pearl Concentrate behind the mix homogeneously, fully mix, promptly get phase 1.
2. other fully dissolves the extract of above-mentioned gained with aqueous solution of propylene glycol, promptly gets phase 2.3. phase 2 is added uniform mixing in the phase 1, and add Oleum Cocois oxalic acid amide, Kai Song and essence, add the water mixing and get final product.The shampoo of preparation has the control functional oil.
Embodiment 3:
Cacumen Platycladi, Fructus Cnidii, Semen Sapindi Delavayi, Herba Rabdosiae glaucocalycis 4 flavor medical materials are respectively got 5 weight portions and added 5-10 water doubly, decoct two to three mixing, filter, filtrate is concentrated into 1/20 of original volume, adds ethanol to containing alcohol amount 60-80%, places, filter, concentrate, vacuum drying gets Chinese medicine extract, and the water dissolution that adds 80 weight portions gets final product.The shampoo of preparation has the control functional oil.
Embodiment 4:
Respectively 4 flavor medical materials are extracted by purgation earlier:
Cacumen Platycladi: take by weighing Cacumen Platycladi 8 weight portions, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, medicinal residues add 65% alcohol reflux twice, and each 2 hours, the decocting liquid behind medicinal liquid and the extraction volatile oil merged, filter decompression recycling ethanol, concentrated solution, put coldly, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, wait to adsorb the back water flushing that finishes, the ethanol elution of reuse 80% is collected eluent, reclaim ethanol, concentrate, lyophilization gets Cacumen Platycladi extract;
Fructus Cnidii: take by weighing Fructus Cnidii medical material 8 weight portions, steam distillation extracts and got volatile oil in 3 hours, and device is preserved standby in addition; Decocting liquid filters, and reclaim under reduced pressure concentrates, and lyophilization gets Fructus cnidii extract;
Semen Sapindi Delavayi: take by weighing Semen Sapindi Delavayi medical material 8 weight portions, water boiling and extraction three times, each 2 hours, filter, reclaim under reduced pressure water concentrates, and lyophilization gets the Semen Sapindi Delavayi extract;
Herba Rabdosiae glaucocalycis: take by weighing Herba Rabdosiae glaucocalycis medical material 8 weight portions, add 85% alcohol reflux twice, filter, decompression recycling ethanol, concentrated solution is put cold, filter, filtrate is directly gone up the D-101 macroporous adsorptive resins, waits to adsorb the back water flushing that finishes, the ethanol elution of reuse 80%, collect eluent, decompression recycling ethanol concentrates, lyophilization gets Herba Rabdosiae glaucocalycis extract;
After obtaining each medicinal substances extract respectively, mix promptly getting Chinese medicine extract, standby.
Get effervescent tablet substrate 68 weight portions, comprising: tartaric acid 15 weight portions, sodium bicarbonate 15 weight portions, soluble starch 28 weight portions, polyethylene glycol 6000 10 weight portions.
Method for making: 1. will add the sodium bicarbonate of 100 mesh sieves after the polyethylene glycol 6000 fusion, mix homogeneously, pulverize the cooling back, crosses 100 mesh sieves, adds all through blended Chinese medicine extract, tartaric acid, the soluble starch of 100 mesh sieves, and tabletting promptly gets effervescent tablet.Add in the entry during use and dissolve, the shampoo of preparation has the control functional oil.
Embodiment 5:
Cacumen Platycladi, Fructus Cnidii, Semen Sapindi Delavayi, Herba Rabdosiae glaucocalycis 4 flavor medical materials are respectively got 5 weight portions and added 5-10 water doubly, decoct two to three mixing, filter, filtrate is concentrated into 1/20 of original volume, add ethanol to containing alcohol amount 60-80%, place, filter, concentrate, vacuum drying gets Chinese medicine extract, and the dry extract extract powder is contained in the paper bag, makes medicated bag, the water that adds 80 weight portions during use gets final product dissolving in the medicated bag immersion water.The shampoo of preparation has the control functional oil.
Claims (2)
1. the application of Chinese medicine composition in the preparation oil-controlling shampoo, it is characterized in that said composition is by the Cacumen Platycladi of 0.25-8 weight portion, the Fructus Cnidii of 0.25-8 weight portion, the Semen Sapindi Delavayi of 0.25-8 weight portion, the Herba Rabdosiae glaucocalycis of 0.25-8 weight portion, make the conventional shampoo substrate that adds the 68-99 weight portion behind the Chinese medicine extract again and make through extracting.
2. the application of Chinese medicine composition in the preparation oil-controlling shampoo, it is characterized in that said composition is by the Cacumen Platycladi of 0.25-8 weight portion, the Fructus Cnidii of 0.25-8 weight portion, the Semen Sapindi Delavayi of 0.25-8 weight portion, the Herba Rabdosiae glaucocalycis of 0.25-8 weight portion, make the water that adds the 68-99 weight portion behind the Chinese medicine extract again and make through extracting.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012077120A3 (en) * | 2010-12-09 | 2013-07-04 | Y&B Mother's Choice Ltd. | Natural formulations |
| US9474283B2 (en) | 2010-12-09 | 2016-10-25 | Y&B Mother's Choice Ltd. | Formulations comprising saponins and uses thereof |
| US10117827B2 (en) | 2013-12-08 | 2018-11-06 | Y&B Mother's Choice Ltd. | Preparations for suppressing or attenuating ocular irritancy |
| US10434058B2 (en) | 2010-12-09 | 2019-10-08 | Y&B Mother's Choice Ltd. | Natural formulations |
| CN111658580A (en) * | 2020-06-23 | 2020-09-15 | 广西和桂集团有限公司 | Hair growth and/or hair blackening essence containing various peptides and plant extracts and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1819816A (en) * | 2005-04-11 | 2006-08-16 | 孟悦华 | Chinese medicinal preparation for removing dandruff and production thereof |
| CN101357201A (en) * | 2008-09-16 | 2009-02-04 | 杨运金 | Multipurpose traditional Chinese medicine and preparation method thereof |
| CN101496783B (en) * | 2009-03-13 | 2010-10-06 | 云南省药物研究所 | Chinese medicine shampoo for relieving itching and removing dandruff |
-
2010
- 2010-01-20 CN CN201010039190XA patent/CN101732208B/en active Active
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2012077120A3 (en) * | 2010-12-09 | 2013-07-04 | Y&B Mother's Choice Ltd. | Natural formulations |
| US9474283B2 (en) | 2010-12-09 | 2016-10-25 | Y&B Mother's Choice Ltd. | Formulations comprising saponins and uses thereof |
| US10064881B2 (en) | 2010-12-09 | 2018-09-04 | Y&B Mother's Choice Ltd. | Natural formulations |
| US10434058B2 (en) | 2010-12-09 | 2019-10-08 | Y&B Mother's Choice Ltd. | Natural formulations |
| US10117827B2 (en) | 2013-12-08 | 2018-11-06 | Y&B Mother's Choice Ltd. | Preparations for suppressing or attenuating ocular irritancy |
| CN111658580A (en) * | 2020-06-23 | 2020-09-15 | 广西和桂集团有限公司 | Hair growth and/or hair blackening essence containing various peptides and plant extracts and preparation method thereof |
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| Publication number | Publication date |
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| CN101732208B (en) | 2011-07-20 |
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